FR2506630A1 - Catalyseur d'hydrogenation pour la desulfuration et l'elimination de metaux lourds - Google Patents

Catalyseur d'hydrogenation pour la desulfuration et l'elimination de metaux lourds

Info

Publication number
FR2506630A1
FR2506630A1 FR8209502A FR8209502A FR2506630A1 FR 2506630 A1 FR2506630 A1 FR 2506630A1 FR 8209502 A FR8209502 A FR 8209502A FR 8209502 A FR8209502 A FR 8209502A FR 2506630 A1 FR2506630 A1 FR 2506630A1
Authority
FR
France
Prior art keywords
heavy metals
removal
hydrogenation catalyst
sulfurization
carbon black
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR8209502A
Other languages
English (en)
Other versions
FR2506630B1 (fr
Inventor
Yoichi Kageyama
Kazuhiko Onuma
Toshihiro Kawakami
Makoto Suzuki
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Kasei Corp
Original Assignee
Mitsubishi Kasei Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from JP56084703A external-priority patent/JPS57201532A/ja
Priority claimed from JP56086116A external-priority patent/JPS57201533A/ja
Application filed by Mitsubishi Kasei Corp filed Critical Mitsubishi Kasei Corp
Publication of FR2506630A1 publication Critical patent/FR2506630A1/fr
Application granted granted Critical
Publication of FR2506630B1 publication Critical patent/FR2506630B1/fr
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/24—Chromium, molybdenum or tungsten
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/88—Molybdenum
    • B01J23/882—Molybdenum and cobalt
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/615—100-500 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/635—0.5-1.0 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/638—Pore volume more than 1.0 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/64—Pore diameter
    • B01J35/647—2-50 nm
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/66—Pore distribution
    • B01J35/69—Pore distribution bimodal
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/107—Atmospheric residues having a boiling point of at least about 538 °C

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Catalysts (AREA)

Abstract

L'INVENTION A POUR OBJET UN CATALYSEUR D'HYDROGENATION POUR LA DESULFURATION ET L'ELIMINATION DES METAUX LOURDS. IL COMPREND: A. AU MOINS UN COMPOSANT METALLIQUE CHOISI PARMI LES METAUX DES GROUPES VIA ET VIII DE LA CLASSIFICATION PERIODIQUE A TITRE DE COMPOSANT CATALYTIQUE ACTIF, ET B. UN SUPPORT POREUX EN ALUMINE ACTIVEE OBTENU EN FACONNANT UN MELANGE DE NOIR DE CARBONE ET D'UNE POUDRE D'ALUMINE ACTIVEE OU D'UN PRECURSEUR D'ALUMINE ACTIVEE, EN SECHANT CE MELANGE FACONNE ET EN LE SOUMETTANT A UNE CUISSON DANS UN COURANT GAZEUX CONTENANT DE L'OXYGENE POUR BRULER LE NOIR DE CARBONE. TRAITEMENT DES PRODUITS PETROLIERS POUR REDUIRE LES TENEURS EN SOUFRE ET LES DEBARRASSER DES METAUX LOURDS.
FR8209502A 1981-06-02 1982-06-01 Catalyseur d'hydrogenation pour la desulfuration et l'elimination de metaux lourds Expired FR2506630B1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP56084703A JPS57201532A (en) 1981-06-02 1981-06-02 Production of catalyst with active alumina carrier
JP56086116A JPS57201533A (en) 1981-06-04 1981-06-04 Hydrodesulfurizing and demetallizing catalyst

Publications (2)

Publication Number Publication Date
FR2506630A1 true FR2506630A1 (fr) 1982-12-03
FR2506630B1 FR2506630B1 (fr) 1985-07-12

Family

ID=26425686

Family Applications (1)

Application Number Title Priority Date Filing Date
FR8209502A Expired FR2506630B1 (fr) 1981-06-02 1982-06-01 Catalyseur d'hydrogenation pour la desulfuration et l'elimination de metaux lourds

Country Status (9)

Country Link
US (1) US4448896A (fr)
BE (1) BE893369A (fr)
CA (1) CA1183120A (fr)
DE (1) DE3220671A1 (fr)
DK (1) DK162723C (fr)
FR (1) FR2506630B1 (fr)
GB (1) GB2101005B (fr)
IT (1) IT1156304B (fr)
NL (1) NL189850C (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0237240A2 (fr) * 1986-02-28 1987-09-16 Nippon Oil Co. Ltd. Procédé de préparation de catalyseurs d'hydrogénation

Families Citing this family (66)

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US4624773A (en) * 1983-08-16 1986-11-25 Ashland Oil, Inc. Large pore catalysts for heavy hydrocarbon conversion
US4492626A (en) * 1984-06-11 1985-01-08 Phillips Petroleum Company Hydrofining process for hydrocarbon containing feed streams
NL8501945A (nl) * 1984-12-07 1986-07-01 Unilever Nv Katalysator geschikt voor het ontzwavelen en de bereiding van deze katalysator.
US4598060A (en) * 1985-01-28 1986-07-01 Shell Oil Company Process for the preparation of wide pore catalysts
CA1325993C (fr) * 1988-05-16 1994-01-11 Mitsui Chemicals, Incorporated Methode permettant d'eliminer le mercure contenu dans des huiles hydrocarbures
NL8901239A (nl) * 1989-05-18 1990-12-17 Meern Bv Engelhard De Katalysator voor hydrogenering en/of dehydrogenering.
CN1044337C (zh) * 1993-11-23 1999-07-28 中国石油化工总公司 一种具有双重孔氧化铝载体的制备方法
GB9415554D0 (en) * 1994-08-02 1994-09-21 Unilever Plc Cobalt on alumina catalysts
CN1055877C (zh) * 1996-03-26 2000-08-30 中国石油化工总公司抚顺石油化工研究院 大孔径氧化铝载体及其制备方法
CN1054393C (zh) 1997-07-22 2000-07-12 中国石油化工总公司 一种渣油加氢脱金属催化剂
CN1089039C (zh) * 1998-09-28 2002-08-14 中国石油化工集团公司 一种大孔氧化铝载体及其制备方法
CN1098914C (zh) * 1999-09-29 2003-01-15 中国石油化工集团公司 一种重油加氢处理催化剂载体及其制备方法
WO2001030494A1 (fr) 1999-10-27 2001-05-03 Idemitsu Kosan Co., Ltd. Catalyseur d'hydrotraitement pour huile hydrocarbonee, support pour celle-ci et procede d'hydrotraitement d'huile hydrocarbonee
CN1115388C (zh) * 2000-09-25 2003-07-23 中国石油化工股份有限公司 一种加氢保护催化剂及其制备方法
CN1296135C (zh) * 2003-09-28 2007-01-24 中国石油化工股份有限公司 一种大孔氧化铝载体及其制备方法
EP1716076B1 (fr) * 2004-01-23 2017-03-15 Very Small Particle Company Pty Ltd Procede de fabrication d'oxydes metalliques
CN100406122C (zh) * 2004-10-29 2008-07-30 中国石油化工股份有限公司 一种重、渣油加氢处理催化剂的制备方法
CN100363470C (zh) * 2004-11-30 2008-01-23 中国石油化工股份有限公司 一种渣油加氢脱金属催化剂及其制备方法
CN100421784C (zh) * 2005-04-27 2008-10-01 中国石油化工股份有限公司 一种含硅和硼的氧化铝干胶及其制备方法
MXPA05009283A (es) * 2005-08-31 2007-02-27 Mexicano Inst Petrol Procedimiento para la preparacion de una composicion catalitica para el hidroprocesamiento de fracciones del petroleo.
CN100434177C (zh) * 2005-10-31 2008-11-19 中国石油化工股份有限公司 一种氧化铝载体的制备方法
CN1966616B (zh) * 2005-11-16 2010-08-25 中国石油化工股份有限公司 一种加氢活性保护剂及其制备方法
ES2277545B1 (es) 2005-11-18 2008-06-16 Consejo Superior Investig. Cientificas Procedimiento simplificado para la preparacion de catalizadores de metales u oxidos metalicos soportados sobre materiales porosos.
DE102007011471B4 (de) 2006-03-09 2021-09-30 Shell Internationale Research Maatschappij B.V. Katalysatorkombination für die hydrierende Verarbeitung von Vakuumgasölen und/oder Visbreakergasölen
CN101239324B (zh) * 2007-02-09 2010-05-19 中国石油化工股份有限公司 高活性、高中油选择性的加氢裂化催化剂及其制备方法
CN101314139B (zh) * 2007-05-31 2010-07-21 中国石油化工股份有限公司 一种含硼复合氧化铝载体及其制备方法
CN101468322B (zh) * 2007-12-27 2010-12-01 中国石油化工股份有限公司 一种氧化铝载体及其制备方法
CN101664701B (zh) * 2008-09-04 2011-11-30 中国石油化工股份有限公司 一种氧化铝载体及其制备方法
CN101693205B (zh) * 2009-10-14 2012-04-18 长春惠工净化工业有限公司 脱二烯烃加氢保护剂的制备及应用
CN102989454B (zh) * 2011-09-09 2016-02-10 中国石油天然气股份有限公司 含双峰孔径分布载体的碳二前加氢催化剂及其制备方法
CN103055949B (zh) * 2011-10-21 2014-07-23 中国石油化工股份有限公司 一种大孔氧化铝载体的制备方法
CN103055948B (zh) * 2011-10-21 2014-10-15 中国石油化工股份有限公司 大孔氧化铝载体的制备方法
CN103055952B (zh) * 2011-10-24 2015-01-14 中国石油化工股份有限公司 一种渣油加氢处理催化剂载体及其制备方法
CN103055932B (zh) * 2011-10-24 2015-02-18 中国石油化工股份有限公司 一种渣油加氢处理催化剂及其制备方法
CN102773113B (zh) * 2012-07-17 2014-10-22 西北大学 一种煤焦油加氢脱氮催化剂及其应用
CN103785405B (zh) * 2012-11-01 2016-08-17 中国石油化工股份有限公司 一种加氢脱金属催化剂及其制备方法
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CN105621463B (zh) * 2014-10-30 2017-08-22 中国石油化工股份有限公司 一种合成大孔氧化铝的方法
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CN106140187B (zh) * 2015-04-23 2018-08-14 中国石油化工股份有限公司 一种加氢脱金属催化剂的制备方法
CN107304062B (zh) * 2016-04-21 2019-01-25 中国石油化工股份有限公司 一种氧化铝载体的制备方法
CN108620085B (zh) * 2017-03-24 2021-01-05 中国石油化工股份有限公司 改性氧化铝载体及其制备方法和负载型加氢精制催化剂
CN109277102B (zh) * 2017-07-20 2021-07-06 中国石油化工股份有限公司 加氢脱金属催化剂及其制备方法和应用
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CN109722280B (zh) 2017-10-27 2020-06-09 中国石油化工股份有限公司 一种用于加氢处理的载体、催化剂及其制备方法和应用
EP3778021A4 (fr) 2018-04-10 2021-11-17 China Petroleum & Chemical Corporation Catalyseur d'hydroraffinage, procédé de préparation associé et utilisation correspondante
CN111097458B (zh) * 2018-10-25 2022-06-07 中国石油化工股份有限公司 一种加氢脱金属催化剂及其制法
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CN114433118B (zh) * 2020-10-30 2023-06-02 中国科学院宁波材料技术与工程研究所 沸腾床加氢催化剂及煤焦油全馏分的加工方法
CN114433119B (zh) * 2020-10-30 2023-06-02 中国科学院宁波材料技术与工程研究所 重芳烃油加氢精制催化剂及重芳烃油生产btx的方法
CN114433111B (zh) * 2020-10-30 2023-08-25 宁波中金石化有限公司 一种重芳烃油加氢精制催化剂及重芳烃油加工方法
US11577235B1 (en) * 2021-08-13 2023-02-14 Chevron U.S.A. Inc. Layered catalyst reactor systems and processes for hydrotreatment of hydrocarbon feedstocks

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FR2175762A1 (fr) * 1972-03-14 1973-10-26 Kaiser Aluminium Chem Corp
US3893947A (en) * 1973-09-10 1975-07-08 Union Oil Co Group VI-B metal catalyst preparation
FR2413323A1 (fr) * 1977-12-30 1979-07-27 American Cyanamid Co Procede de preparation de particules d'alumine rehydratable mises en forme
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EP0237240A2 (fr) * 1986-02-28 1987-09-16 Nippon Oil Co. Ltd. Procédé de préparation de catalyseurs d'hydrogénation
EP0237240A3 (fr) * 1986-02-28 1988-05-11 Nippon Oil Co. Ltd. Procédé de préparation de catalyseurs d'hydrogénation

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FR2506630B1 (fr) 1985-07-12
IT1156304B (it) 1987-02-04
DE3220671C2 (fr) 1993-07-29
DK162723C (da) 1992-05-11
IT8221618A1 (it) 1983-12-01
CA1183120A (fr) 1985-02-26
DE3220671A1 (de) 1982-12-16
NL189850C (nl) 1993-08-16
DK245782A (da) 1982-12-03
BE893369A (fr) 1982-12-01
GB2101005A (en) 1983-01-12
GB2101005B (en) 1984-09-05
IT8221618A0 (it) 1982-06-01
NL8202120A (nl) 1983-01-03
US4448896A (en) 1984-05-15
DK162723B (da) 1991-12-02

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