EP1371496A2 - Gegenstand aus Glas oder Keramik mit aufgebrachtem Aufdruck - Google Patents
Gegenstand aus Glas oder Keramik mit aufgebrachtem Aufdruck Download PDFInfo
- Publication number
- EP1371496A2 EP1371496A2 EP03076729A EP03076729A EP1371496A2 EP 1371496 A2 EP1371496 A2 EP 1371496A2 EP 03076729 A EP03076729 A EP 03076729A EP 03076729 A EP03076729 A EP 03076729A EP 1371496 A2 EP1371496 A2 EP 1371496A2
- Authority
- EP
- European Patent Office
- Prior art keywords
- glass
- digital image
- digital
- ceramic
- printing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Images
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F24—HEATING; RANGES; VENTILATING
- F24C—DOMESTIC STOVES OR RANGES ; DETAILS OF DOMESTIC STOVES OR RANGES, OF GENERAL APPLICATION
- F24C15/00—Details
- F24C15/10—Tops, e.g. hot plates; Rings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M1/00—Inking and printing with a printer's forme
- B41M1/26—Printing on other surfaces than ordinary paper
- B41M1/34—Printing on other surfaces than ordinary paper on glass or ceramic surfaces
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M3/00—Printing processes to produce particular kinds of printed work, e.g. patterns
- B41M3/008—Sequential or multiple printing, e.g. on previously printed background; Mirror printing; Recto-verso printing; using a combination of different printing techniques; Printing of patterns visible in reflection and by transparency; by superposing printed artifacts
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
- B41M5/0041—Digital printing on surfaces other than ordinary paper
- B41M5/0047—Digital printing on surfaces other than ordinary paper by ink-jet printing
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
- B41M5/0041—Digital printing on surfaces other than ordinary paper
- B41M5/007—Digital printing on surfaces other than ordinary paper on glass, ceramic, tiles, concrete, stones, etc.
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M7/00—After-treatment of prints, e.g. heating, irradiating, setting of the ink, protection of the printed stock
- B41M7/009—After-treatment of prints, e.g. heating, irradiating, setting of the ink, protection of the printed stock using thermal means, e.g. infrared radiation, heat
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/24—Structurally defined web or sheet [e.g., overall dimension, etc.]
- Y10T428/24802—Discontinuous or differential coating, impregnation or bond [e.g., artwork, printing, retouched photograph, etc.]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/24—Structurally defined web or sheet [e.g., overall dimension, etc.]
- Y10T428/24802—Discontinuous or differential coating, impregnation or bond [e.g., artwork, printing, retouched photograph, etc.]
- Y10T428/24926—Discontinuous or differential coating, impregnation or bond [e.g., artwork, printing, retouched photograph, etc.] including ceramic, glass, porcelain or quartz layer
Definitions
- the invention relates to an object, at least partially consisting of Glass or glass ceramic with a non-digital printing technique Imprint.
- Decorated glass ceramic cooktops e.g. CERAN glass ceramic cooktops
- the Decoration or the markings are applied by screen printing.
- Screen printing is now a proven method, especially for glass printing Printing process, which is particularly economical with large lot sizes is used.
- it can be used on glass objects relatively thick and so that opaque layers can be realized in one printing process.
- the disadvantage is however, that individual decors and / or labels are economical cannot be realized with this method.
- the object of the invention is achieved in that the glass or the glass ceramic has at least one surface area that is in digital Printing technology generated print image (hereinafter briefly called digital image) is.
- digital printing on the one hand and not digital printing technology on the other hand can have their respective advantages of the individual processes can be combined.
- the digital image makes it possible Object to give an individual character or additional, only on to contain information related to this subject or content.
- the digital image can be changed bit by bit, making a greatest possible flexibility is achieved.
- the non-digitally generated print image can be applied in a conventional manner, for example by screen printing become. Technically mature processes are used here, by means of which complex decors with good quality can be created.
- the digital technology can in particular be used to Barcode, a number code, a matrix code and / or a 2-D barcode to print the object. These digital prints can be customized in Scanners can be read out.
- the Digital image formed from a ceramic color preferably by means of a ceramic toner is generated.
- the ceramic color can then in particular be permanently burned into the surface of the glass or glass ceramic.
- a design is also conceivable in which it is provided that the digital image at least partially using a plastic-based printing ink, preferably using a toner with a thermoplastic or thermosetting plastic matrix is generated.
- the object of the invention relating to the method is achieved in that on a further surface area of the glass or the glass ceramic in digital printing technology a digitally generated print image (hereinafter briefly digital image called) is applied.
- a digitally generated print image hereinafter briefly digital image called
- the two printing processes can be simultaneous or in time and / or space be carried out separately. If the printing processes are consecutive, then these can be separated from each other by a print media fixation his. It is also conceivable that the non-digital printing is carried out at the factory becomes. The individualization then only takes place at the end customer Digital printing. This opens up new logistical opportunities.
- the digital image can be provided for fixing the print and the non-digitally generated print image in the glass or the glass ceramic be branded together.
- the digital image in the electrophotographic or is applied by inkjet printing. It is also conceivable that the digital image is applied in a laser process, using a printing medium is applied over a large area to the glass or the glass ceramic and wherein this is then burned in locally using a laser.
- the Digital image is applied and burned into the glass or glass ceramic, and that the glass or glass ceramic is then thermally tempered becomes.
- a conceivable variant of the invention can be designed such that the digital image using a plastic based ink, preferably using a toner with a thermoplastic or thermoset plastic matrix is generated and that the digital image at a temperature in the range between 130 ° C and 200 ° C is fixed.
- Example 1 Glass ceramic cooktops
- a glass ceramic cooktop (1) is schematic in plan view shown.
- Cooking zone markings (2.1) and manufacturer logos can be seen (2.2) and decor areas (2.3), which have certain decor grids, which in comparatively large production lots with screen printing technology were.
- this cooking surface (1) has at least one additional one Surface area (3) in which individual characters or logos in Form of a digital image (4) generated in digital technology are applied.
- Ceramic colors used here are electrophotographic Process in which the ceramic color is in the form of ceramic toner is printed directly on the glass ceramic.
- the printing can be done directly after the usual screen printing process on the not yet ceramicized cooking surface or off-line on the decorated one and already ceramicized cooking surface.
- the branding then takes place in first case together with the screen-printed, possibly intermediate-dried Decorative colors or, in the second case, with an additional short penetration, the (only!) locally in the case of glass ceramics due to the zero expansion behavior can be done. It is sufficient if only the surface area (3) with the digital images (4) to a temperature of> 700 ° C (typically approx. 720 ° C) for 5 to 10 minute is heated. Basically, this also opens up new logistical opportunities, which a subsequent individualization only shortly before delivery to the end customer.
- Example 1 designs as in Example 1 can be used realize.
- the 2nd digital one is used Printing process before the tempering process. A subsequent branding after tempering the glass is no longer possible.
- Plastic based paints e.g. B. thermosetting or thermoplastic Colors
- the color can also be fixed after tempering (temperature typically between 130 and 200 ° C, depending on the plastic).
- This embodiment is front, side and / or Rear windows of motor vehicles that have a decoration in the form of revolving, mostly black colored edges, which have the best possible Should have opacity in order to conceal bonds or assembly elements.
- This edge printing is usually done in a first printing step made by screen printing.
- these disks have zones on which individual characters and codes are applied, which the later Contain the vehicle identification code or serial numbers included after assembly in the vehicle together with the chassis number of the vehicle an identification code for the vehicle result that can be used for better traceability in the event of theft.
- the manufacturing process for such individualized car windows also works here from a 2-step printing process that combines screen printing with digital Printing, in particular the electrophotographic printing process combined here.
- Such logos are, for example, fine matrix codes, in the form of a pixel field, with which relatively extensive, individual information Have it stored in the smallest space. These can now be done using special Scanner can be read out.
- the disc also contains areas in which individual room names, notes, names and department names are printed.
- the drinking milk bottles are provided with a standard decor and can be used with individualized with a specific imprint. Can be customized for example the name, weight, date of birth etc. in digital printing be applied.
Landscapes
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Combustion & Propulsion (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Printing Methods (AREA)
- Surface Treatment Of Glass (AREA)
- Developing Agents For Electrophotography (AREA)
- Laser Beam Printer (AREA)
- Combination Of More Than One Step In Electrophotography (AREA)
- Medical Preparation Storing Or Oral Administration Devices (AREA)
- Dot-Matrix Printers And Others (AREA)
- Laminated Bodies (AREA)
Abstract
Description
- Schriftzüge, wie "Private Edition - exclusive für <NAME des Endkunden, NAME der Elektro-Handelsgesellschaft oder NAME des Küchenstudios > ", "Edition..."
- Firmenlogos, z. B. die von großen Einrichtungshäusern, Küchenhäusern oder Elektro-Handelsgesellschaften, die derartige Kochflächen (1) vertreiben.
- Barcodes, Zahlencodes, Matrixcodes oder 2-D-Barcodes etc. die zur Kennzeichnung der Produktionscharge, Artikelnummer odgl. dienen.
- aufgerasterte Bilder, z. B. von den Endkunden (z. B. in Verbindung mit dem Schriftzug "Familien-Edition" + Photo der Familienmitglieder, z. B. innerhalb jeder Kochzone).
- Schriftzüge in asiatischen oder arabischen Sprachen, die Sicherheitshinweise enthalten. Oft weisen derartige Schriften feine Lininezüge auf, die im Zuge der normalen Dekoration nicht fein genug gedruckt werden können.
- feine Symbole innerhalb von Funktionszonen, wie Bedienfelder innerhalb der Kochflächen (1).
- maschinenlesbare Barcodes,
- maschinenlesbare Matrixcodes,
- Ziffern und/oder Buchstaben,
- etc.
Claims (15)
- Gegenstand, zumindest teilweise bestehend aus Glas oder Glaskeramik mit einem in nicht digitaler Drucktechnik aufgebrachten Aufdruck,
dadurch gekennzeichnet, dass das Glas oder die Glaskeramik wenigstens einen Oberflächenbereich aufweist, der mit einem in digitaler Drucktechnik erzeugten Druckbild (nachfolgend kurz Digitalbild (4) genannt) versehen ist. - Gegenstand nach Anspruch 1,
dadurch gekennzeichnet, dass das Digitalbild (4) einen Schriftzug, ein Lager, ein aufgerastertes Bild und/oder ein Symbol enthält. - Gegenstand nach Anspruch 1 oder 2,
dadurch gekennzeichnet, dass das Digitalbild (4) einen Barcode, einen Zahlencode, einen Matrixcode und/oder einen 2-D-Barcode enthält. - Gegenstand nach Anspruch 2 oder 3,
dadurch gekennzeichnet, dass das Digitalbild (4) von einer keramischen Farbe gebildet, vorzugsweise mittels eines keramischen Toners erzeugt ist. - Gegenstand nach eines der Ansprüche 1 bis 4,
dadurch gekennzeichnet, dass das in nicht digitaler Drucktechnik aufgebrachte Druckbild im Tampondurck-, Offsetdruck- oder Siebdruckverfahren aufgebracht ist. - Gegenstand nach eines der Ansprüche 1 bis 5,
dadruch gekennzeichnet, dass das Digitalbild (4) in die Oberfläche des Glases oder der Glaskeramik eingebrannt ist. - Gegenstand nach eines der Ansprüche 1 bis 6,
dadurch gekennzeichnet, dass das Digitalbild (4) zumindest teilweise mittels einer Kunststoff basierten Druckfarbe, vorzugsweise mittels eines Toners mit thermoplastischer oder duromerischer Kunststoffmatrix erzeugt ist. - Verfahren zum Dekorieren eines Gegenstandes aus Glas oder Glaskeramik, wobei auf einen Oberflächenbereich des Glases oder der Glaskeramik ein Druckbild in nicht digitaler Drucktechnik aufgebracht wird,
dadurch gekennzeichnet, dass auf einen weiteren Oberflächenbereich des Glases oder der Glaskeramik in digitaler Drucktechnik ein digital erzeugtes Druckbild (nachfolgend kurz Digitalbild (4) genannt) aufgebracht wird. - Verfahren nach Anspruch 8,
dadurch gekennzeichnet, dass das Digitalbild (4) und das nicht digital erzeugte Druckbild in zeitlich und/oder räumlich getrennter Folge gedruckt werden. - Verfahren nach Anspruch 9,
dadurch gekennzeichnet, dass das Digitalbild (4) und das nicht digital erzeugte Druckbild in das Glas oder die Glaskeramik gemeinsam eingebrannt werden. - Verfahren nach Anspruch 9,
dadurch gekennzeichnet, dass das Digitalbild (4) mittels eines lokal begrenzt auf der Glaskeramikoberfläche einwirkenden Einbrandes fixiert wird. - Verfahren nach Anspruch 10 oder 11,
dadurch gekennzeichnet, dass der Einbrand, der das Digitalbild (4) zumindest teilweise schaffenden keramischen Farbe bei einer Temparatur ≥ 700°C und während einer Einbranddauer ≥ 3 min erfolgt. - Verfahren nach einem der Ansprüche 8 bis 12,
dadurch gekennzeichnet, dass das Digitalbild (4) im elektrofotografischen oder im Tintenstrahldruckverfahren aufgebracht wird, oder dass das Digitalbild (4) im Laserverfahren aufgebracht wird, wobei ein Druckmedium großflächig auf das Glas oder die Glaskeramik aufgebracht wird und wobei dieses dann lokal mittels eines Lasers eingebrannt wird. - Verfahren nach einem der Ansprüche 8 bis 13,
dadurch gekennzeichnet, dass das Digitalbild (4) aufgebracht und in das Glas oder die Glaskeramik eingebrannt wird, und dass anschließend das Glas oder die Glaskeramik thermisch vorgespannt wird. - Verfahren nach einem der vorhergehenden Ansprüche,
dadurch gekennzeichnet, dass das Digitalbild (4) unter Verwendung einer Kunststoff basierten Druckfarbe, vorzugsweise mittels eines Toners mit thermoplastischer oder duromerischer Kunststoffmatrix erzeugt wird, und dass das Digitalbild (4) bei einer Temperatur im Bereich zwischen 130°C und 200°C fixiert wird.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10226561A DE10226561B4 (de) | 2002-06-14 | 2002-06-14 | Gegenstand aus Glas oder Glaskeramik und Verfahren zum Dekorieren eines Gegenstandes aus Glas oder Glaskeramik |
DE10226561 | 2002-06-14 |
Publications (3)
Publication Number | Publication Date |
---|---|
EP1371496A2 true EP1371496A2 (de) | 2003-12-17 |
EP1371496A3 EP1371496A3 (de) | 2005-08-03 |
EP1371496B1 EP1371496B1 (de) | 2010-01-06 |
Family
ID=29557827
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP03076729A Expired - Lifetime EP1371496B1 (de) | 2002-06-14 | 2003-06-04 | Gegenstand aus Glas oder Keramik mit aufgebrachtem Aufdruck |
Country Status (8)
Country | Link |
---|---|
US (2) | US20040071942A1 (de) |
EP (1) | EP1371496B1 (de) |
JP (1) | JP2004142421A (de) |
CN (2) | CN1489008A (de) |
AT (1) | ATE454271T1 (de) |
CA (1) | CA2432328A1 (de) |
DE (2) | DE10226561B4 (de) |
ES (1) | ES2337132T3 (de) |
Cited By (3)
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WO2014060918A1 (de) * | 2012-10-19 | 2014-04-24 | BSH Bosch und Siemens Hausgeräte GmbH | Verfahren zur herstellung einer kochfeldplatte, vorrichtung dafür und kochfeldplatte |
EP3170673A1 (de) * | 2015-11-13 | 2017-05-24 | Hochschule Offenburg | Digitaldruckverfahren für keramikfarben |
WO2023099677A1 (de) * | 2021-12-03 | 2023-06-08 | BSH Hausgeräte GmbH | Verfahren zur herstellung einer haushaltsgeräteplatte |
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US20080055348A1 (en) * | 2006-08-30 | 2008-03-06 | Lee Edgar Deeter | System and method for printing data carrying mark on honeycomb structures |
US20080057266A1 (en) * | 2006-08-30 | 2008-03-06 | Corning Incorporated | Marked honeycomb structures |
US20100193459A1 (en) * | 2007-04-12 | 2010-08-05 | Todd Housley | Nursing bottle with recessed storage area |
US20080251655A1 (en) * | 2007-04-12 | 2008-10-16 | Housley Todd B | Bottle Holder |
US7658294B2 (en) * | 2007-04-12 | 2010-02-09 | Todd B. Housley | Nursing bottle with cushiony exterior sidewall |
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EP2060546A1 (de) * | 2007-11-13 | 2009-05-20 | Pilkington Italia S.p.A. | Fahrzeugverglasung |
JP5029904B2 (ja) * | 2008-01-30 | 2012-09-19 | 日本精機株式会社 | 計器文字板及びその製造方法 |
ES2341410B1 (es) * | 2008-04-24 | 2011-04-12 | Creaciones Arquitectonicas Y Estudios De Logotipos, S.L. | Metodo de impresion grafica para cristales y cristal impreso obtenido. |
ES2358825B1 (es) * | 2009-05-14 | 2012-03-20 | Bsh Electrodomesticos España S.A. | Procedimiento para fabricar una superficie de cocción. |
CN101830132A (zh) * | 2010-05-17 | 2010-09-15 | 左翠霞 | 一种陶瓷报刊物及其制备方法 |
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JP2019052050A (ja) * | 2016-01-29 | 2019-04-04 | Agc株式会社 | ガラス部材およびその製造方法 |
CN107698790B (zh) | 2016-08-05 | 2023-10-03 | 法国圣戈班玻璃公司 | 用于玻璃上的薄膜及其制造方法以及车窗 |
KR102480461B1 (ko) | 2017-11-30 | 2022-12-21 | 쌩-고벵 글래스 프랑스 | 차량용 창유리의 터미널 솔더링 장치 및 방법 |
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CN110039922B (zh) * | 2019-04-28 | 2020-09-25 | 东莞市唯美陶瓷工业园有限公司 | 固定图案与喷墨图案相对应的陶瓷砖生产方法和生产线 |
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DE19921923A1 (de) * | 1999-05-12 | 2000-11-16 | Schott Glas | Verfahren und Vorrichtung zum Aufbringen von Dekors und/oder Zeichen auf Glas-, Glaskeramik- und Keramikerzeugnisse |
DE19929523A1 (de) * | 1999-06-28 | 2001-01-18 | Schott Glas | Beschichtungsmaterial sowie Herstellungsverfahren für ein Beschichtungsmaterial |
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JP2001191479A (ja) * | 2000-01-17 | 2001-07-17 | Dainippon Ink & Chem Inc | 印刷装置および該印刷装置を用いた印刷方法 |
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DE10052371A1 (de) * | 2000-10-20 | 2002-05-02 | Schott Glas | Modular aufgebaute elektrofotografische Druckvorrichtung |
DE10134374B4 (de) * | 2001-07-14 | 2008-07-24 | Schott Ag | Kochfeld mit einer Glaskeramikplatte als Kochfläche und Verfahren zur Herstellung der Glaskeramikplatte |
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-
2002
- 2002-06-14 DE DE10226561A patent/DE10226561B4/de not_active Expired - Fee Related
-
2003
- 2003-06-04 DE DE50312310T patent/DE50312310D1/de not_active Expired - Lifetime
- 2003-06-04 EP EP03076729A patent/EP1371496B1/de not_active Expired - Lifetime
- 2003-06-04 AT AT03076729T patent/ATE454271T1/de not_active IP Right Cessation
- 2003-06-04 ES ES03076729T patent/ES2337132T3/es not_active Expired - Lifetime
- 2003-06-13 US US10/462,103 patent/US20040071942A1/en not_active Abandoned
- 2003-06-13 CA CA002432328A patent/CA2432328A1/en not_active Abandoned
- 2003-06-14 CN CNA031555101A patent/CN1489008A/zh active Pending
- 2003-06-14 CN CNA2008100032191A patent/CN101290145A/zh active Pending
- 2003-06-16 JP JP2003171119A patent/JP2004142421A/ja active Pending
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2006
- 2006-03-20 US US11/384,881 patent/US20060159852A1/en not_active Abandoned
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2014060918A1 (de) * | 2012-10-19 | 2014-04-24 | BSH Bosch und Siemens Hausgeräte GmbH | Verfahren zur herstellung einer kochfeldplatte, vorrichtung dafür und kochfeldplatte |
EP3170673A1 (de) * | 2015-11-13 | 2017-05-24 | Hochschule Offenburg | Digitaldruckverfahren für keramikfarben |
WO2023099677A1 (de) * | 2021-12-03 | 2023-06-08 | BSH Hausgeräte GmbH | Verfahren zur herstellung einer haushaltsgeräteplatte |
Also Published As
Publication number | Publication date |
---|---|
EP1371496B1 (de) | 2010-01-06 |
DE10226561A1 (de) | 2004-01-08 |
EP1371496A3 (de) | 2005-08-03 |
US20040071942A1 (en) | 2004-04-15 |
JP2004142421A (ja) | 2004-05-20 |
CA2432328A1 (en) | 2003-12-14 |
ES2337132T3 (es) | 2010-04-21 |
CN101290145A (zh) | 2008-10-22 |
CN1489008A (zh) | 2004-04-14 |
DE10226561B4 (de) | 2006-12-28 |
DE50312310D1 (de) | 2010-02-25 |
US20060159852A1 (en) | 2006-07-20 |
ATE454271T1 (de) | 2010-01-15 |
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