EP0121916B1 - Feuille d'enregistrement pour stylet à projection d'encre - Google Patents

Feuille d'enregistrement pour stylet à projection d'encre Download PDF

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Publication number
EP0121916B1
EP0121916B1 EP84103846A EP84103846A EP0121916B1 EP 0121916 B1 EP0121916 B1 EP 0121916B1 EP 84103846 A EP84103846 A EP 84103846A EP 84103846 A EP84103846 A EP 84103846A EP 0121916 B1 EP0121916 B1 EP 0121916B1
Authority
EP
European Patent Office
Prior art keywords
recording
coating
silicon dioxide
ink
recording paper
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
EP84103846A
Other languages
German (de)
English (en)
Other versions
EP0121916A3 (en
EP0121916A2 (fr
Inventor
Hiroyo Central Research Laboratory Oshima
Yutaka Central Research Laboratory Kojima
Yukio Central Research Laboratory Kobayashi
Takashi Central Research Laboratory Omori
Koichi Central Research Laboratory Nagai
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jujo Paper Co Ltd
Original Assignee
Jujo Paper Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jujo Paper Co Ltd filed Critical Jujo Paper Co Ltd
Publication of EP0121916A2 publication Critical patent/EP0121916A2/fr
Publication of EP0121916A3 publication Critical patent/EP0121916A3/de
Application granted granted Critical
Publication of EP0121916B1 publication Critical patent/EP0121916B1/fr
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
    • B41M5/00—Duplicating or marking methods; Sheet materials for use therein
    • B41M5/50—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording
    • B41M5/52—Macromolecular coatings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
    • B41M5/00—Duplicating or marking methods; Sheet materials for use therein
    • B41M5/50—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording
    • B41M5/502—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording characterised by structural details, e.g. multilayer materials
    • B41M5/508—Supports
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H19/00—Coated paper; Coating material
    • D21H19/36—Coatings with pigments
    • D21H19/38—Coatings with pigments characterised by the pigments
    • D21H19/40—Coatings with pigments characterised by the pigments siliceous, e.g. clays
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
    • B41M5/00—Duplicating or marking methods; Sheet materials for use therein
    • B41M5/50—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording
    • B41M5/52—Macromolecular coatings
    • B41M5/5218—Macromolecular coatings characterised by inorganic additives, e.g. pigments, clays
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
    • B41M5/00—Duplicating or marking methods; Sheet materials for use therein
    • B41M5/50—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording
    • B41M5/52—Macromolecular coatings
    • B41M5/5254—Macromolecular coatings characterised by the use of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds, e.g. vinyl polymers
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/24—Structurally defined web or sheet [e.g., overall dimension, etc.]
    • Y10T428/24802—Discontinuous or differential coating, impregnation or bond [e.g., artwork, printing, retouched photograph, etc.]
    • Y10T428/24893—Discontinuous or differential coating, impregnation or bond [e.g., artwork, printing, retouched photograph, etc.] including particulate material
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/27—Web or sheet containing structurally defined element or component, the element or component having a specified weight per unit area [e.g., gms/sq cm, lbs/sq ft, etc.]
    • Y10T428/273—Web or sheet containing structurally defined element or component, the element or component having a specified weight per unit area [e.g., gms/sq cm, lbs/sq ft, etc.] of coating
    • Y10T428/277—Cellulosic substrate
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31971—Of carbohydrate
    • Y10T428/31993—Of paper

Definitions

  • the invention relates to a coated recording paper for ink jet recorders or for the ink spray recording method, which is suitable for recording at high speed.
  • the ink spray recording method has the advantage that it is quiet and multi-color records can be easily made. It is used in facsimile machines and for various printers.
  • the recording papers for ink-jet recording processes are divided into conventional and coated recording papers.
  • the conventional recording papers with a low degree of sizing have good ink absorbency; however, the clarity of the recording suffers from the diffusion of the ink in the sheet layer, in particular the image resolution and color density are unsatisfactory in the case of multicolor recordings. Therefore, investigations were carried out with coated recording papers with superior image resolution.
  • the coated recording papers provide superior image density and clarity because the dye of the ink in the coating is locally absorbed and does not bleed.
  • such recording papers have the disadvantage that they are not so suitable for rapid recording because of their insufficient ink absorption capacity.
  • the rapid recording by the ink jet recording method has to be improved, as in other recording methods such as the screen dot recording, electrostatic recording, heat sensitive recording, etc.
  • the recording device there is a faster one Multi-nozzle type printer using a foam jet system has already been developed.
  • the coated recording paper which has a superior image resolution, has the disadvantage that the dry state of the ink is unstable because the ink drops ejected from the nozzles after being adhered to the surface of the recording paper are absorbed inside and thereby are only apparently in a dry state.
  • problems in fast recording such as the contact of papers with each other after recording, the transfer and scratching of the ink when transported by the roller of the recording apparatus, etc., which are not found in other recording methods.
  • the invention is based on the object of providing a coated recording paper for ink jet recorders or for ink spray recording processes which is better suited for rapid recording.
  • a recording paper for ink-jet recording processes consisting of a support and at least one coating arranged thereon, which contains fine silicon oxide and a water-soluble, polymeric binder, which is characterized in that the support has a Stöckigt sizing degree of less than 4 seconds. (based on a basis weight of 60 g / m 2 ) and that the fine silicon oxide has a specific surface area of at least 200 m 2 / g, determined by the BET method, and a uniformity number n of the Rosin-Rammler distribution of at least 1, 10 owns.
  • Fine silica with a specific surface area of at least 200 m 2 / g, determined by the BET method, and with a uniformity number n of the Rosin-Rammler distribution of at least 1.10 is used as the pigment according to the invention in the coating composition.
  • the use of a pigment based on silicon dioxide as a coating material for the surface of the ink spray paper is described in JP-A-51583/1980. However, the silicon dioxide described there has different properties and is of a different nature.
  • the fine silicon dioxide selected according to the invention results in a recording paper which is superior in color density, hue, clarity and suitability for rapid recording.
  • the silicon dioxide according to the invention must meet as a first condition that it has a specific surface area of at least 200 m 2 / g.
  • a coating that contains silicon dioxide with a large specific surface area as the main component results in superior color density and clarity.
  • the silicon dioxide according to the invention must satisfy that it has a uniformity number n of the Rosin-Rammler distribution of at least 1.10.
  • a large uniformity number n means a narrow particle distribution.
  • Silicon dioxide with a large specific surface area and a narrow particle distribution results in a particularly superior ink absorption capacity.
  • the right choice of silicon dioxide gives a coating that is particularly suitable for rapid recording. In general, the coating has the structure of a dense layer of pigment and binder. It was therefore not believed that the superior absorbency that conventional ink-jet recording papers had was achievable with a coated paper.
  • a paper with a Stöckigt glue strength of less than 4 seconds (based on a basis weight of 60 g / m 2 ) is used.
  • a Stöckigt sizing degree of less than 4 seconds (based on a basis weight of 60 g / m 2 ) means that the ratio of Stöckigt sizing degree / basis weight [(seconds) / (g / M 2 )] is less than 0.07 . That is, the inkbe Part that flows through the coating easily penetrates into the carrier and is absorbed by it because the carrier has no or only a low degree of sizing.
  • ⁇ BDp n (where b and n are each a constant and n is called a uniformity number or a distribution constant), you can get a straight line. Then you draw a line parallel to this line through a point P in the RR diagram and read the exponent n on the exposed line. This way you can easily get n.
  • the effect according to the invention can also be achieved if the measured value of the particle size distribution, which is determined by the above method, is approximately regarded as a straight line.
  • silica pigments that meet the above two conditions are, for example, SILCRON ° G100, SILCRON O 600 (manufactured by Nissan Chemical Industries, Ltd.), SYLOID® 404, SYLOID® 79, SYLOID O 74 (manufactured by Fuji -Davison Chemical Ltd.), GASIL ° HP-34 (manufactured by Joseph Crossfield & Sons, Ltd.), Finesil® X27, Finesil® X37, Finesil® 79 (manufactured by Tokuyama Soda Co., Ltd.), CARPLEX ° Nr .80 (manufactured by Shionogi & Co., Ltd.) etc.
  • a water-soluble polymeric binder is suitable as the binder which is used in combination with the above-mentioned silicon dioxide pigments.
  • Polyvinyl alcohol and its derivatives are particularly desirable in terms of color density, but one can also use oxidized starch, modified starch, rubber compounds, e.g. Guar gum and the like, sodium alginate, water-soluble cellulose derivatives, e.g. Hydroxyethyl cellulose, methyl cellulose, carboxymethyl cellulose etc., water soluble proteins e.g. Soybean protein, casein and the like, water soluble polymeric compounds e.g. Polyvinyl pyrrolidone and the like.
  • a fairly large amount of pigment according to the invention is preferably used in the preparation of the coating composition, i.e. a weight ratio (expressed as a solid weight) of silicon dioxide according to the invention to water-soluble, polymeric binder of about 60-95: 40-5.
  • the silicon dioxide according to the invention can optionally be used together with other pigments, e.g. Kaolin, talc, calcium carbonate, magnesium carbonate, barium sulfate, titanium white, organic fillers and the like can be used.
  • the coating can be carried out using customary application devices, for example doctor blade spreaders, air brush spreaders, bar spreaders, roller spreaders and the like, or size presses.
  • the coating amount is preferably 3 to 15 g / m 2 on one surface of the support; too much coating leads to poor ink absorbency.
  • the ink spray recording was made with a Panafax 6000 (manufactured by Matsushita Graphic Communication Systems, Inc.).
  • a two-nozzle ink jet recording device was used to produce two-color printing with black and red inks.
  • the red ink was ejected for 10 seconds, then both red and black ink were ejected for 5 seconds, and finally a black ink was ejected for 10 seconds.
  • the respective recording width of the red and black ink was 24 mm and the overlapping recording width of red and black ink in the central area was 8 mm.
  • the reflection density of the recording surface was measured with a Macbeth densimeter, the reflection density of the red recording surface using green filter for the magenta color and of blue filter for the yellow color and the reflection density of the black recording surface using visual filter for the black color (all filters are SPI filters).
  • the reflection density (the sum) in the table was expressed as the sum of the individual reflection densities.
  • the ink absorption time of a recording paper was determined by dropping 0.0018 cm 3 of cyan ink (manufactured by Matsushita-Giken) at 20 ° C and 65% RH using 1 micron micro-injectors onto the surface of a paper and determining the absorption time of the ink .
  • the ink absorption speeds of the recording papers Nos. 1 to 3 are less than 30 seconds; so they are very fast, and their reflection densities are superior.
  • the comparative tests which have a uniformity number of less than 1.10, have a significantly lower ink absorption rate
  • the other comparative tests which have a BET-specific surface of less than 200 m 2 / g have inferior reflection densities.
  • a silica slurry (Gasil ° HP-34, manufactured by Joseph Crossfield & Sons, Ltd.) was added to 20 wt. (as a solid content) of a 15% aqueous solution of polyvinyl alcohol (degree of saponification: 100%, PVA 117, manufactured by Kuraray Co., Ltd.) to prepare a coating composition.
  • the coating composition obtained was applied to three higher-quality papers with different degrees of sizing in an amount of 6 to 8 g / m 2 to produce three recording papers.
  • the recording papers coated with the silicon dioxide according to the invention regardless of the type of base paper types, have a superior reflection density.
  • the ink absorption rate depends on the degree of sizing of the base paper, and with a degree of sizing of more than 4 seconds (based on a basis weight of 60 g / m 2 ) the coating of silicon dioxide works insufficiently.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Ink Jet Recording Methods And Recording Media Thereof (AREA)
  • Paper (AREA)
  • Duplication Or Marking (AREA)

Claims (5)

  1. Papier d'enregistrement pour procédé d'enregistrement à jet d'encre, constitué d'un substrat et d'au moins un revêtement qui est disposé sur celui-ci et qui contient du dioxyde de silicium fin et un liant polymère soluble dans l'eau, caractérisé en ce que le substrat présente un degré d'encollage Stockigt de moins de 4 s (rapporté à un grammage de 60 g/m2) et en ce que le dioxyde de silicium fin possède une surface spécifique déterminée par le procédé BET, d'au moins 200 m2/g et un nombre de constance n pour la distribution Rosin-Rammler qui est d'au moins 1,10.
  2. 2. Papier d'enregistrement selon la revendication 1, caractérisé en ce que le liant polymère soluble dans l'eau est de l'alcool polyvinylique et/ou un dérivé de l'alcool polyvinylique.
  3. 3. Papier d'enregistrement selon la revendication 1 ou 2, caractérisé en ce que le rapport en poids du dioxyde de silicium au liant polymère soluble dans l'eau se situe dans 60-95:40-5.
  4. 4. Papier d'enregistrement selon l'une des revendications 1 à 3, caractérisé en ce que la quantité de revêtement se situe dans la gamme de 3 à 15 g/m2 sur une surface du substrat.
  5. 5. Procédé de fabrication d'un papier d'enregistrement pour procédé d'enregistrement à jet d'encre, selon lequel on applique sur un substrat au moins un revêtement qui contient du dioxyde de silicium fin et un liant polymère soluble dans l'eau, caractérisé en ce que l'on utilise un substrat qui possède un degré d'encollage Stöckigt de moins de 4 s (rapporté à un grammage de 60 g/m2) et en ce qu'on utilise du dioxyde de silicium fin ayant une surface spécifique, déterminée d'après le procédé BET, d'au moins 200 m2/g et un nombre de constance n pour la distribution Rosin-Rammler qui est d'au moins 1,10.
EP84103846A 1983-04-07 1984-04-06 Feuille d'enregistrement pour stylet à projection d'encre Expired EP0121916B1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP59968/83 1983-04-07
JP58059968A JPS59185690A (ja) 1983-04-07 1983-04-07 インクジエツト記録用紙

Publications (3)

Publication Number Publication Date
EP0121916A2 EP0121916A2 (fr) 1984-10-17
EP0121916A3 EP0121916A3 (en) 1984-12-05
EP0121916B1 true EP0121916B1 (fr) 1987-01-07

Family

ID=13128474

Family Applications (1)

Application Number Title Priority Date Filing Date
EP84103846A Expired EP0121916B1 (fr) 1983-04-07 1984-04-06 Feuille d'enregistrement pour stylet à projection d'encre

Country Status (4)

Country Link
US (1) US4478910A (fr)
EP (1) EP0121916B1 (fr)
JP (1) JPS59185690A (fr)
DE (1) DE3461942D1 (fr)

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JPH0326665B2 (fr) 1991-04-11
EP0121916A3 (en) 1984-12-05
US4478910A (en) 1984-10-23
JPS59185690A (ja) 1984-10-22
EP0121916A2 (fr) 1984-10-17
DE3461942D1 (en) 1987-02-12

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