DE2844942A1 - Verfahren zur herstellung von monodispersen photographischen silberhalogenidemulsionen - Google Patents
Verfahren zur herstellung von monodispersen photographischen silberhalogenidemulsionenInfo
- Publication number
- DE2844942A1 DE2844942A1 DE19782844942 DE2844942A DE2844942A1 DE 2844942 A1 DE2844942 A1 DE 2844942A1 DE 19782844942 DE19782844942 DE 19782844942 DE 2844942 A DE2844942 A DE 2844942A DE 2844942 A1 DE2844942 A1 DE 2844942A1
- Authority
- DE
- Germany
- Prior art keywords
- silver halide
- salt
- solution
- crystals
- rhodium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 229910052709 silver Inorganic materials 0.000 title claims description 45
- 239000004332 silver Substances 0.000 title claims description 45
- 239000000839 emulsion Substances 0.000 title claims description 30
- 238000004519 manufacturing process Methods 0.000 title description 4
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 title description 3
- -1 silver halide Chemical class 0.000 claims description 48
- 239000013078 crystal Substances 0.000 claims description 35
- 239000000243 solution Substances 0.000 claims description 23
- 150000003283 rhodium Chemical class 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 16
- 230000006911 nucleation Effects 0.000 claims description 11
- 238000010899 nucleation Methods 0.000 claims description 11
- 229910052703 rhodium Inorganic materials 0.000 claims description 7
- 239000010948 rhodium Substances 0.000 claims description 7
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 claims description 7
- 239000007791 liquid phase Substances 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 6
- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 claims description 6
- 239000002612 dispersion medium Substances 0.000 claims description 5
- 150000004820 halides Chemical class 0.000 claims description 5
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 150000003839 salts Chemical class 0.000 claims description 4
- 239000000084 colloidal system Substances 0.000 claims description 3
- 230000001681 protective effect Effects 0.000 claims description 3
- 239000012266 salt solution Substances 0.000 claims description 3
- 229910052783 alkali metal Inorganic materials 0.000 claims 2
- 150000001340 alkali metals Chemical class 0.000 claims 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims 1
- BWYMLYMBQPWYCL-UHFFFAOYSA-N [Na].[Rh] Chemical compound [Na].[Rh] BWYMLYMBQPWYCL-UHFFFAOYSA-N 0.000 claims 1
- 210000004072 lung Anatomy 0.000 claims 1
- 239000002609 medium Substances 0.000 description 9
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 8
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 6
- 229920000159 gelatin Polymers 0.000 description 5
- 235000019322 gelatine Nutrition 0.000 description 5
- 108010010803 Gelatin Proteins 0.000 description 4
- 239000008273 gelatin Substances 0.000 description 4
- 235000011852 gelatine desserts Nutrition 0.000 description 4
- 229910001961 silver nitrate Inorganic materials 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- SWLVFNYSXGMGBS-UHFFFAOYSA-N ammonium bromide Chemical compound [NH4+].[Br-] SWLVFNYSXGMGBS-UHFFFAOYSA-N 0.000 description 3
- 235000019270 ammonium chloride Nutrition 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 239000003513 alkali Substances 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 2
- 239000001828 Gelatine Substances 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- FOIXSVOLVBLSDH-UHFFFAOYSA-N Silver ion Chemical compound [Ag+] FOIXSVOLVBLSDH-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- SJOOOZPMQAWAOP-UHFFFAOYSA-N [Ag].BrCl Chemical compound [Ag].BrCl SJOOOZPMQAWAOP-UHFFFAOYSA-N 0.000 description 1
- CODNYICXDISAEA-UHFFFAOYSA-N bromine monochloride Chemical compound BrCl CODNYICXDISAEA-UHFFFAOYSA-N 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 239000004848 polyfunctional curative Substances 0.000 description 1
- PZSJYEAHAINDJI-UHFFFAOYSA-N rhodium(3+) Chemical class [Rh+3] PZSJYEAHAINDJI-UHFFFAOYSA-N 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/06—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein with non-macromolecular additives
- G03C1/08—Sensitivity-increasing substances
- G03C1/09—Noble metals or mercury; Salts or compounds thereof; Sulfur, selenium or tellurium, or compounds thereof, e.g. for chemical sensitising
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/015—Apparatus or processes for the preparation of emulsions
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/035—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein characterised by the crystal form or composition, e.g. mixed grain
- G03C2001/0357—Monodisperse emulsion
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C2200/00—Details
- G03C2200/06—Additive
Landscapes
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- General Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Colloid Chemistry (AREA)
- Non-Silver Salt Photosensitive Materials And Non-Silver Salt Photography (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB43073/77A GB1535016A (en) | 1977-10-17 | 1977-10-17 | Monodispersed emulsions |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2844942A1 true DE2844942A1 (de) | 1979-04-19 |
Family
ID=10427213
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19782844942 Ceased DE2844942A1 (de) | 1977-10-17 | 1978-10-16 | Verfahren zur herstellung von monodispersen photographischen silberhalogenidemulsionen |
Country Status (7)
| Country | Link |
|---|---|
| JP (1) | JPS5465521A (enrdf_load_stackoverflow) |
| BE (1) | BE871278R (enrdf_load_stackoverflow) |
| CH (1) | CH638904A5 (enrdf_load_stackoverflow) |
| DE (1) | DE2844942A1 (enrdf_load_stackoverflow) |
| FR (1) | FR2406228A2 (enrdf_load_stackoverflow) |
| GB (1) | GB1535016A (enrdf_load_stackoverflow) |
| IT (1) | IT1157371B (enrdf_load_stackoverflow) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58190943A (ja) * | 1982-04-30 | 1983-11-08 | Fuji Photo Film Co Ltd | ハロゲン化銀写真感光材料の現像方法 |
| JPS59212826A (ja) * | 1983-05-18 | 1984-12-01 | Konishiroku Photo Ind Co Ltd | ハロゲン化銀写真乳剤の製造方法 |
| JPS61245151A (ja) | 1985-04-23 | 1986-10-31 | Konishiroku Photo Ind Co Ltd | ハロゲン化銀写真感光材料 |
| JPS61250643A (ja) | 1985-04-30 | 1986-11-07 | Konishiroku Photo Ind Co Ltd | ハロゲン化銀写真感光材料 |
| JPS61250645A (ja) | 1985-04-30 | 1986-11-07 | Konishiroku Photo Ind Co Ltd | ハロゲン化銀写真感光材料 |
| DE3682128D1 (de) | 1985-07-17 | 1991-11-28 | Konishiroku Photo Ind | Photographisches silberhalogenidmaterial. |
| JP2515115B2 (ja) * | 1987-01-26 | 1996-07-10 | 富士写真フイルム株式会社 | ネガ型ハロゲン化銀写真感光材料 |
| EP0476327B1 (en) | 1990-08-20 | 1999-11-17 | Fuji Photo Film Co., Ltd. | Data-retainable photographic film product and process for producing color print |
| DE69230387T2 (de) | 1991-04-22 | 2000-06-29 | Fuji Photo Film Co., Ltd. | Photographische Silberhalogenidmaterialien und Verfahren zu ihrer Verarbeitung |
| EP0557616A1 (en) * | 1992-02-07 | 1993-09-01 | Agfa-Gevaert N.V. | A silver halide material suitable for use in a silver salt diffusion transfer process |
| JP2777949B2 (ja) | 1992-04-03 | 1998-07-23 | 富士写真フイルム株式会社 | ハロゲン化銀カラー写真感光材料 |
| JP2603189B2 (ja) * | 1993-10-27 | 1997-04-23 | コニカ株式会社 | 感光性ハロゲン化銀乳剤 |
| DE69605393T2 (de) | 1995-12-27 | 2000-04-13 | Fuji Photo Film Co., Ltd. | Hydrazin-Verbindung und diese enthaltendes photographisches Silberhalogenidmaterial |
| EP2003946A4 (en) | 2006-03-28 | 2010-11-03 | Fujifilm Corp | CONDUCTIVE FILM, MANUFACTURING METHOD THEREOF, AND TRANSPARENT ELECTROMAGNETIC SHIELDING FILM |
| WO2008038764A1 (fr) | 2006-09-28 | 2008-04-03 | Fujifilm Corporation | Écran à émission spontanée, procédé de fabrication d'un écran à émission spontanée, film conducteur transparent, dispositif électroluminescent, électrode transparente de cellule solaire et électrode transparente de papier électronique |
| JP5588597B2 (ja) | 2007-03-23 | 2014-09-10 | 富士フイルム株式会社 | 導電性材料の製造方法及び製造装置 |
| EP2009977A3 (en) | 2007-05-09 | 2011-04-27 | FUJIFILM Corporation | Electromagnetic shielding film and optical filter |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1597560A1 (de) * | 1966-12-02 | 1970-08-13 | Eastman Kodak Co | Verfahren zur Herstellung ausentwickelbarer photographischer Silberhalogenidemulsionen |
| DE2221082A1 (de) * | 1971-05-03 | 1972-11-16 | Ilford Ltd | Verfahren zur Herstellung einer Silberhalogenidemulsion |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE309974C (enrdf_load_stackoverflow) * | 1918-09-21 | |||
| GB775197A (en) * | 1954-10-08 | 1957-05-22 | Ici Ltd | Colour photographic process |
| AU2544571A (en) * | 1970-02-16 | 1972-08-17 | Eastman Kodak Company | Method of making a metal salt precipitate |
| US3901713A (en) * | 1971-06-02 | 1975-08-26 | Fuji Photo Film Co Ltd | Process for the manufacture of silver halide photographic emulsion containing iridium and rhodium |
| JPS4933781A (enrdf_load_stackoverflow) * | 1972-07-31 | 1974-03-28 | ||
| JPS585419B2 (ja) * | 1975-08-01 | 1983-01-31 | 富士写真フイルム株式会社 | ハロゲン化銀写真乳剤の製造方法 |
-
1977
- 1977-10-17 GB GB43073/77A patent/GB1535016A/en not_active Expired
-
1978
- 1978-10-11 JP JP12422078A patent/JPS5465521A/ja active Granted
- 1978-10-13 CH CH1064878A patent/CH638904A5/de not_active IP Right Cessation
- 1978-10-13 IT IT51489/78A patent/IT1157371B/it active
- 1978-10-16 DE DE19782844942 patent/DE2844942A1/de not_active Ceased
- 1978-10-16 BE BE191130A patent/BE871278R/xx not_active IP Right Cessation
- 1978-10-16 FR FR7829445A patent/FR2406228A2/fr active Granted
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1597560A1 (de) * | 1966-12-02 | 1970-08-13 | Eastman Kodak Co | Verfahren zur Herstellung ausentwickelbarer photographischer Silberhalogenidemulsionen |
| DE2221082A1 (de) * | 1971-05-03 | 1972-11-16 | Ilford Ltd | Verfahren zur Herstellung einer Silberhalogenidemulsion |
Also Published As
| Publication number | Publication date |
|---|---|
| IT1157371B (it) | 1987-02-11 |
| GB1535016A (en) | 1978-12-06 |
| FR2406228B2 (enrdf_load_stackoverflow) | 1982-04-30 |
| IT7851489A0 (it) | 1978-10-13 |
| CH638904A5 (en) | 1983-10-14 |
| FR2406228A2 (fr) | 1979-05-11 |
| JPS6133177B2 (enrdf_load_stackoverflow) | 1986-07-31 |
| BE871278R (fr) | 1979-04-17 |
| JPS5465521A (en) | 1979-05-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8128 | New person/name/address of the agent |
Representative=s name: SCHWABE, H., DIPL.-ING. SANDMAIR, K., DIPL.-CHEM. |
|
| 8110 | Request for examination paragraph 44 | ||
| AF | Is addition to no. |
Ref country code: DE Ref document number: 2221082 Format of ref document f/p: P |
|
| 8131 | Rejection |