DE102005047424A1 - Phosphatierlösung mit Wasserstoffperoxid und chelatbildenden Carbonsäuren - Google Patents

Phosphatierlösung mit Wasserstoffperoxid und chelatbildenden Carbonsäuren Download PDF

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Publication number
DE102005047424A1
DE102005047424A1 DE102005047424A DE102005047424A DE102005047424A1 DE 102005047424 A1 DE102005047424 A1 DE 102005047424A1 DE 102005047424 A DE102005047424 A DE 102005047424A DE 102005047424 A DE102005047424 A DE 102005047424A DE 102005047424 A1 DE102005047424 A1 DE 102005047424A1
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DE
Germany
Prior art keywords
phosphating
hydrogen peroxide
acid
ions
phosphating solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
DE102005047424A
Other languages
German (de)
English (en)
Inventor
Jan-Willem Brouwer
Jerzy-Tadeusz Wawrzyniak
Jens Dr. Krömer
Maximilian Dr. Schönherr
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Original Assignee
Henkel AG and Co KGaA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Priority to DE102005047424A priority Critical patent/DE102005047424A1/de
Priority to PCT/EP2006/008063 priority patent/WO2007039015A1/de
Priority to CN2006800364618A priority patent/CN101278075B/zh
Priority to EP06776869A priority patent/EP1929070A1/de
Priority to RU2008116542/02A priority patent/RU2428518C2/ru
Publication of DE102005047424A1 publication Critical patent/DE102005047424A1/de
Priority to US12/055,984 priority patent/US20090071573A1/en
Priority to ZA200802778A priority patent/ZA200802778B/xx
Ceased legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
    • C23C22/08—Orthophosphates
    • C23C22/18—Orthophosphates containing manganese cations
    • C23C22/188—Orthophosphates containing manganese cations containing also magnesium cations
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
    • C23C22/08—Orthophosphates
    • C23C22/12—Orthophosphates containing zinc cations
    • C23C22/16—Orthophosphates containing zinc cations containing also peroxy-compounds
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
    • C23C22/08—Orthophosphates
    • C23C22/12—Orthophosphates containing zinc cations
    • C23C22/17—Orthophosphates containing zinc cations containing also organic acids
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
    • C23C22/36—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates
    • C23C22/364—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates containing also manganese cations
    • C23C22/365—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates containing also manganese cations containing also zinc and nickel cations

Landscapes

  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Chemical Treatment Of Metals (AREA)
  • Preventing Corrosion Or Incrustation Of Metals (AREA)
DE102005047424A 2005-09-30 2005-09-30 Phosphatierlösung mit Wasserstoffperoxid und chelatbildenden Carbonsäuren Ceased DE102005047424A1 (de)

Priority Applications (7)

Application Number Priority Date Filing Date Title
DE102005047424A DE102005047424A1 (de) 2005-09-30 2005-09-30 Phosphatierlösung mit Wasserstoffperoxid und chelatbildenden Carbonsäuren
PCT/EP2006/008063 WO2007039015A1 (de) 2005-09-30 2006-08-16 Phosphatierlösung mit wasserstoffperoxid und chelatbildenden carbonsäuren
CN2006800364618A CN101278075B (zh) 2005-09-30 2006-08-16 含过氧化氢和螯合羧酸的磷化液
EP06776869A EP1929070A1 (de) 2005-09-30 2006-08-16 Phosphatierlösung mit wasserstoffperoxid und chelatbildenden carbonsäuren
RU2008116542/02A RU2428518C2 (ru) 2005-09-30 2006-08-16 Раствор фосфатирования с перекисью водорода и хелатообразующими карбоновыми кислотами
US12/055,984 US20090071573A1 (en) 2005-09-30 2008-03-26 Phosphating solution with hydrogen peroxide and chelating carboxylic acids
ZA200802778A ZA200802778B (en) 2005-09-30 2008-03-28 Phosphatising solution with hydrogen peroxide and chelating carboxylic acids

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102005047424A DE102005047424A1 (de) 2005-09-30 2005-09-30 Phosphatierlösung mit Wasserstoffperoxid und chelatbildenden Carbonsäuren

Publications (1)

Publication Number Publication Date
DE102005047424A1 true DE102005047424A1 (de) 2007-04-05

Family

ID=37668277

Family Applications (1)

Application Number Title Priority Date Filing Date
DE102005047424A Ceased DE102005047424A1 (de) 2005-09-30 2005-09-30 Phosphatierlösung mit Wasserstoffperoxid und chelatbildenden Carbonsäuren

Country Status (7)

Country Link
US (1) US20090071573A1 (zh)
EP (1) EP1929070A1 (zh)
CN (1) CN101278075B (zh)
DE (1) DE102005047424A1 (zh)
RU (1) RU2428518C2 (zh)
WO (1) WO2007039015A1 (zh)
ZA (1) ZA200802778B (zh)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2503025B1 (de) * 2011-03-22 2013-07-03 Henkel AG & Co. KGaA Mehrstufige korrosionsschützende Behandlung metallischer Bauteile, die zumindest teilweise Oberflächen von Zink oder Zinklegierungen aufweisen
CN104278261B (zh) * 2013-07-12 2017-11-07 王恩栋 用于除锈及磷化的环保型磷酸浓缩液与应用
RU2572688C1 (ru) * 2014-09-10 2016-01-20 Закрытое акционерное общество "ФК" Раствор для фосфатирования металлической поверхности
US10113070B2 (en) 2015-11-04 2018-10-30 Ppg Industries Ohio, Inc. Pretreatment compositions and methods of treating a substrate
CN109504958A (zh) * 2018-12-25 2019-03-22 宁波淡水谷金属制线有限公司 一种钢材表面酸洗磷化工艺
CN109504838A (zh) * 2018-12-25 2019-03-22 宁波淡水谷金属制线有限公司 一种钢丝热处理工艺
US20240018662A1 (en) * 2020-12-22 2024-01-18 M-M-Morant-Gmbh Chromium(vi)-free coating agent for metals
CN113817973B (zh) * 2021-09-23 2022-12-27 马鞍山钢铁股份有限公司 改善合金化镀锌热成形钢表面氧化和涂装性能的表面处理液、热成形钢板及制备方法和应用
CN113832425B (zh) * 2021-09-23 2022-12-27 马鞍山钢铁股份有限公司 一种具有优良耐黑变性能和胶粘性能的锌镁铝镀层钢板及其制备方法
CN113755777B (zh) * 2021-09-23 2023-01-24 马鞍山钢铁股份有限公司 一种环保型表面处理的镀锌钢板及其制备方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE805343C (de) * 1950-01-31 1951-05-17 American Chem Paint Co Verfahren zur Erzeugung von Phosphatueberzuegen auf Metallen, insbesondere Eisen und Stahl
DE1208599B (de) * 1959-11-27 1966-01-05 Metallgesellschaft Ag Verfahren zum Aufbringen von Phosphatueberzuegen auf Metallen
DE4013483A1 (de) * 1990-04-27 1991-10-31 Metallgesellschaft Ag Verfahren zur phosphatierung von metalloberflaechen
WO1997014821A1 (de) * 1995-10-18 1997-04-24 Henkel Kommanditgesellschaft Auf Aktien Schichtgewichtssteuerung bei hydroxylamin-beschleunigten phosphatiersystemen

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2516139A (en) * 1948-12-08 1950-07-25 American Chem Paint Co Method of and material for treating ferriferous metal surfaces with manganese phosphate coating solutions
US3307979A (en) * 1965-10-11 1967-03-07 Lubrizol Corp Phosphating solutions
US3458364A (en) * 1968-05-01 1969-07-29 Lubrizol Corp Method for phosphating ferrous metals
DE2342558C3 (de) * 1973-08-23 1982-11-11 Metallgesellschaft Ag, 6000 Frankfurt Verfahren zur Phosphatierung von Metallen
GB1415999A (en) * 1973-05-29 1975-12-03 Pyrene Chemical Services Ltd Process for forming phosphate coatings
GB1591039A (en) * 1977-05-03 1981-06-10 Pyrene Chemical Services Ltd Processes and compositions for coating metal surfaces
JPS5935681A (ja) * 1982-08-24 1984-02-27 Nippon Paint Co Ltd カチオン型電着塗装用金属表面のリン酸塩処理方法
DE3244715A1 (de) * 1982-12-03 1984-06-07 Gerhard Collardin GmbH, 5000 Köln Verfahren zur phosphatierung von metalloberflaechen sowie hierfuer geeignete badloesungen
DE3408577A1 (de) * 1984-03-09 1985-09-12 Metallgesellschaft Ag, 6000 Frankfurt Verfahren zur phosphatierung von metallen
US5236565A (en) * 1987-04-11 1993-08-17 Metallgesellschaft Aktiengesellschaft Process of phosphating before electroimmersion painting
US5268041A (en) * 1990-04-27 1993-12-07 Metallgesellschaft Ag Process for phosphating metal surfaces
DE4243214A1 (de) * 1992-12-19 1994-06-23 Metallgesellschaft Ag Verfahren zur Erzeugung von Phosphatüberzügen
US6023103A (en) * 1994-11-15 2000-02-08 Formfactor, Inc. Chip-scale carrier for semiconductor devices including mounted spring contacts
DE19511573A1 (de) * 1995-03-29 1996-10-02 Henkel Kgaa Verfahren zur Phosphatierung mit metallhaltiger Nachspülung
DE19544614A1 (de) * 1995-11-30 1997-06-05 Metallgesellschaft Ag Verfahren zur Phospatierung von Metalloberflächen
WO1999007916A1 (de) * 1997-08-06 1999-02-18 Henkel Kommanditgesellschaft Auf Aktien Mit n-oxiden beschleunigtes phosphatierverfahren
DE10110833B4 (de) * 2001-03-06 2005-03-24 Chemetall Gmbh Verfahren zum Aufbringen eines Phosphatüberzuges und Verwendung der derart phosphatierten Metallteile
DE10310680A1 (de) * 2003-03-12 2004-09-23 Henkel Kgaa Verfahren zur Phosphatierung mit einer Kombination von Beschleunigern
DE10323305B4 (de) * 2003-05-23 2006-03-30 Chemetall Gmbh Verfahren zur Beschichtung von metallischen Oberflächen mit einer Wasserstoffperoxid enthaltenden Phosphatierungslösung, Phosphatierlösung und Verwendung der behandelten Gegenstände

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE805343C (de) * 1950-01-31 1951-05-17 American Chem Paint Co Verfahren zur Erzeugung von Phosphatueberzuegen auf Metallen, insbesondere Eisen und Stahl
DE1208599B (de) * 1959-11-27 1966-01-05 Metallgesellschaft Ag Verfahren zum Aufbringen von Phosphatueberzuegen auf Metallen
DE4013483A1 (de) * 1990-04-27 1991-10-31 Metallgesellschaft Ag Verfahren zur phosphatierung von metalloberflaechen
WO1997014821A1 (de) * 1995-10-18 1997-04-24 Henkel Kommanditgesellschaft Auf Aktien Schichtgewichtssteuerung bei hydroxylamin-beschleunigten phosphatiersystemen

Also Published As

Publication number Publication date
RU2008116542A (ru) 2009-11-10
CN101278075B (zh) 2012-05-16
ZA200802778B (en) 2008-12-31
RU2428518C2 (ru) 2011-09-10
WO2007039015A1 (de) 2007-04-12
US20090071573A1 (en) 2009-03-19
CN101278075A (zh) 2008-10-01
EP1929070A1 (de) 2008-06-11

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Legal Events

Date Code Title Description
OP8 Request for examination as to paragraph 44 patent law
8127 New person/name/address of the applicant

Owner name: HENKEL AG & CO. KGAA, 40589 DUESSELDORF, DE

R002 Refusal decision in examination/registration proceedings
R003 Refusal decision now final

Effective date: 20131211