CS244120B2 - Method of alpha aluminium oxide production with low content of alkali for ceramic purposes - Google Patents
Method of alpha aluminium oxide production with low content of alkali for ceramic purposes Download PDFInfo
- Publication number
- CS244120B2 CS244120B2 CS827974A CS797482A CS244120B2 CS 244120 B2 CS244120 B2 CS 244120B2 CS 827974 A CS827974 A CS 827974A CS 797482 A CS797482 A CS 797482A CS 244120 B2 CS244120 B2 CS 244120B2
- Authority
- CS
- Czechoslovakia
- Prior art keywords
- weight
- alkali
- alumina
- amount
- aluminum hydroxide
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 38
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 title claims abstract description 28
- 239000000919 ceramic Substances 0.000 title claims abstract description 12
- 239000003513 alkali Substances 0.000 title claims abstract description 10
- 238000004519 manufacturing process Methods 0.000 title description 11
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims abstract description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000000203 mixture Substances 0.000 claims abstract description 12
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910001424 calcium ion Inorganic materials 0.000 claims abstract description 9
- 230000001089 mineralizing effect Effects 0.000 claims abstract description 7
- 238000001354 calcination Methods 0.000 claims abstract description 5
- 230000003213 activating effect Effects 0.000 claims abstract description 3
- 150000001639 boron compounds Chemical class 0.000 claims abstract description 3
- 150000004820 halides Chemical class 0.000 claims abstract description 3
- 239000000654 additive Substances 0.000 claims description 12
- IRPGOXJVTQTAAN-UHFFFAOYSA-N 2,2,3,3,3-pentafluoropropanal Chemical compound FC(F)(F)C(F)(F)C=O IRPGOXJVTQTAAN-UHFFFAOYSA-N 0.000 claims description 10
- KLZUFWVZNOTSEM-UHFFFAOYSA-K Aluminum fluoride Inorganic materials F[Al](F)F KLZUFWVZNOTSEM-UHFFFAOYSA-K 0.000 claims description 10
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 7
- 239000004327 boric acid Substances 0.000 claims description 7
- 238000000137 annealing Methods 0.000 claims description 6
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 claims description 6
- 229910001634 calcium fluoride Inorganic materials 0.000 claims description 6
- 159000000007 calcium salts Chemical class 0.000 claims description 4
- 239000004615 ingredient Substances 0.000 claims description 2
- 238000005406 washing Methods 0.000 abstract description 6
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 abstract description 4
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 description 9
- 239000011734 sodium Substances 0.000 description 7
- 239000000725 suspension Substances 0.000 description 7
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 5
- 239000011575 calcium Substances 0.000 description 5
- 229910052791 calcium Inorganic materials 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 239000002253 acid Substances 0.000 description 4
- 238000001914 filtration Methods 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 230000000996 additive effect Effects 0.000 description 3
- 229910052782 aluminium Inorganic materials 0.000 description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 3
- 229910001948 sodium oxide Inorganic materials 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 2
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- 230000004913 activation Effects 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229910052573 porcelain Inorganic materials 0.000 description 2
- 230000001698 pyrogenic effect Effects 0.000 description 2
- 238000005245 sintering Methods 0.000 description 2
- 239000010802 sludge Substances 0.000 description 2
- DDFHBQSCUXNBSA-UHFFFAOYSA-N 5-(5-carboxythiophen-2-yl)thiophene-2-carboxylic acid Chemical compound S1C(C(=O)O)=CC=C1C1=CC=C(C(O)=O)S1 DDFHBQSCUXNBSA-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- 244000101724 Apium graveolens Dulce Group Species 0.000 description 1
- 235000015849 Apium graveolens Dulce Group Nutrition 0.000 description 1
- 235000010591 Appio Nutrition 0.000 description 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 239000000908 ammonium hydroxide Substances 0.000 description 1
- 239000002519 antifouling agent Substances 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 238000003490 calendering Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- -1 halide salts Chemical class 0.000 description 1
- 150000002366 halogen compounds Chemical class 0.000 description 1
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000012212 insulator Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000011225 non-oxide ceramic Substances 0.000 description 1
- 229910052575 non-oxide ceramic Inorganic materials 0.000 description 1
- 230000003534 oscillatory effect Effects 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
- C04B35/111—Fine ceramics
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/44—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water
- C01F7/441—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water by calcination
- C01F7/442—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water by calcination in presence of a calcination additive
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| HU813358A HU185474B (en) | 1981-11-10 | 1981-11-10 | Process for preparing alpha-aluminium oxyde poor in alkali for ceramic purposes |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CS797482A2 CS797482A2 (en) | 1985-08-15 |
| CS244120B2 true CS244120B2 (en) | 1986-07-17 |
Family
ID=10963719
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CS827974A CS244120B2 (en) | 1981-11-10 | 1982-11-09 | Method of alpha aluminium oxide production with low content of alkali for ceramic purposes |
Country Status (8)
Families Citing this family (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| HU185474B (en) * | 1981-11-10 | 1985-02-28 | Almasfuezitoei Timfoeldgyar | Process for preparing alpha-aluminium oxyde poor in alkali for ceramic purposes |
| US5383945A (en) * | 1984-01-19 | 1995-01-24 | Norton Company | Abrasive material and method |
| US4623364A (en) * | 1984-03-23 | 1986-11-18 | Norton Company | Abrasive material and method for preparing the same |
| FI79830C (fi) * | 1985-07-15 | 1990-03-12 | Norddeutsche Schleifmittel Ind | Foerfarande foer framstaellning av keramiskt polykristallint slipmaterial. |
| US5340781A (en) * | 1986-07-14 | 1994-08-23 | Showa Denko Kabushiki Kaisha | Spherical corundum particles, process for preparation thereof and rubber or plastic composition having high thermal conductivity and having spherical corundum paticles incorporated therein |
| DE3629100A1 (de) * | 1986-08-27 | 1988-03-03 | Bosch Gmbh Robert | Elektrochemisch stabile keramik aus aluminiumoxid |
| US5302368A (en) * | 1987-01-29 | 1994-04-12 | Sumitomo Chemical Company, Limited | Process for preparation of alumina |
| US4822592A (en) * | 1987-02-05 | 1989-04-18 | Aluminum Company Of America | Producing alpha alumina particles with pressurized acidic steam |
| ES2004759A6 (es) * | 1987-07-17 | 1989-02-01 | Espanola Alumina Sa | Metodo de obtencion de alumina especial a partir del polvo producido en la calcinacion de alumina metalurgica |
| HU210595B (en) * | 1988-02-03 | 1995-05-29 | Almasfuezitoei Timfoeldgyar | Process for producing aluminiume-oxides using to the ceramic which contains smaller than 1 micrometer one-crystalsize grains, too |
| US5296085A (en) * | 1989-09-21 | 1994-03-22 | Atochem | Macrocrystalline α-alumina hexagonal platelets |
| AU639326B2 (en) * | 1990-05-23 | 1993-07-22 | Atochem | Ceramic preforms comprising monocrystalline hexagonal platelets of alpha-alumina, their production and applications thereof |
| CN1068092A (zh) * | 1991-06-21 | 1993-01-20 | 瑞士隆萨股份公司 | 生产以α-氧化铝为基质的烧结材料特别是磨料的方法 |
| IL109236A (en) * | 1993-04-13 | 1998-01-04 | Sumitomo Chemical Co | A-alumina powder and its production |
| JP3744010B2 (ja) * | 1993-06-30 | 2006-02-08 | 住友化学株式会社 | α−アルミナ粉末の製造方法 |
| US5438129A (en) * | 1993-09-27 | 1995-08-01 | Becton Dickinson And Company | DNA purification by solid phase extraction using partially fluorinated aluminum hydroxide adsorbant |
| EP0656319B1 (en) * | 1993-11-25 | 2003-04-09 | Sumitomo Chemical Company, Limited | Method for producing alpha-alumina powder |
| AU699077B2 (en) * | 1995-02-21 | 1998-11-19 | Sumitomo Chemical Company, Limited | Alpha-alumina and method for producing the same |
| JPH09263440A (ja) * | 1996-03-29 | 1997-10-07 | Ngk Insulators Ltd | アルミナ焼結体およびその製造方法 |
| JP3457495B2 (ja) * | 1996-03-29 | 2003-10-20 | 日本碍子株式会社 | 窒化アルミニウム焼結体、金属埋設品、電子機能材料および静電チャック |
| RU2117631C1 (ru) * | 1997-07-11 | 1998-08-20 | Российский химико-технологический университет им.Д.И.Менделеева | Способ получения порошка оксида алюминия для изготовления прозрачной керамики |
| WO2002034692A2 (en) * | 2000-10-20 | 2002-05-02 | Showa Denko K.K. | Method of producing low soda alumina, low soda alumina and method of producing porcelain |
| DE10297611T5 (de) * | 2001-12-27 | 2005-01-13 | Showa Denko K.K. | Teilchemförmiges Aluminiumoxid, Verfahren zur Herstellung von teilchenförmigem Aluminiumoxid und Zusammensetzung, die teilchenförmiges Aluminiumoxid enthält |
| US20060189740A1 (en) * | 2003-06-12 | 2006-08-24 | Showa Denko K.K. | Method for producing particulate alumina and composition containing particulate alumina |
| SG177010A1 (en) * | 2003-08-22 | 2012-01-30 | Dow Technology Investments Llc | Improved alumina carriers and silver-based catalysts for the production of alkylene oxides |
| US20060293180A1 (en) * | 2003-08-22 | 2006-12-28 | Thorsteinson Erlind M | Modified alumina carriers and silver-based catalysts for the production of alkylene oxides |
| US20070111886A1 (en) | 2003-10-16 | 2007-05-17 | Serafin Juliana G | Catalysts having enhanced stability, efficiency and/or activity for alkylene oxide production |
| TW200616988A (en) | 2004-06-18 | 2006-06-01 | Shell Int Research | A process for the production of an olefin oxide, a 1,2-diol, a 1,2-diol ether, or an alkanolamine |
| MXPA06014560A (es) * | 2004-06-18 | 2007-03-23 | Shell Int Research | Proceso para la produccion de un oxido de olefina, un 1,2-diol, un 1,2-diol eter o una alcanolamina. |
| US8536083B2 (en) | 2004-09-01 | 2013-09-17 | Shell Oil Company | Olefin epoxidation process, a catalyst for use in the process, a carrier for use in preparing the catalyst, and a process for preparing the carrier |
| CN101027124B (zh) * | 2004-09-01 | 2010-06-09 | 国际壳牌研究有限公司 | 烯烃环氧化方法、用于该方法的催化剂、用于制备该催化剂的载体以及制备该载体的方法 |
| KR20070106772A (ko) * | 2005-02-21 | 2007-11-05 | 셀 인터나쵸나아레 레사아치 마아츠샤피 비이부이 | 올레핀의 에폭시화 방법, 그 방법에 사용하기 위한 촉매,그 촉매를 제조하는데 이용하기 위한 담체, 및 그 담체의제조방법 |
| CN100348494C (zh) * | 2005-08-26 | 2007-11-14 | 郑州大学 | 一种高分散性α－Al2O3纳米粉体的制备方法 |
| DE102006005400A1 (de) | 2006-02-18 | 2007-08-23 | Nabaltec Ag | Verfahren zur Herstellung von gereinigtem Aluminiumoxid aus alkalihaltiger Tonerde |
| CN114772618B (zh) * | 2022-03-28 | 2023-07-04 | 中铝山东有限公司 | 一种研抛用类球形α氧化铝的制备方法 |
| GB2621393B (en) | 2022-08-12 | 2024-12-25 | Thermo Fisher Scient Bremen Gmbh | Methods and mass spectrometry systems for acquiring mass spectral data |
| GB2621394B (en) | 2022-08-12 | 2024-12-04 | Thermo Fisher Scient Bremen Gmbh | Methods and Mass Spectrometry Systems for Acquiring Mass Spectral Data |
| GB2621395B (en) | 2022-08-12 | 2025-02-05 | Thermo Fisher Scient Bremen Gmbh | Methods and mass spectrometry systems for acquiring mass spectral data |
| CN117125731B (zh) * | 2023-08-28 | 2024-04-26 | 福建明瑞科维新材料科技有限公司 | 一种降低氧化铝锻烧相变温度的矿化剂及其制备方法和应用 |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1950883A (en) * | 1932-05-31 | 1934-03-13 | Aluminum Co Of America | Treatment of aluminum hydrate |
| US3092453A (en) * | 1959-08-18 | 1963-06-04 | Aluminum Co Of America | Production of low-soda alumina |
| US3092452A (en) * | 1959-08-18 | 1963-06-04 | Aluminum Co Of America | Production of low-soda alumina |
| GB1046582A (en) * | 1964-03-04 | 1966-10-26 | Gen Motors Ltd | Improved method of producing alumina |
| US3262754A (en) * | 1964-12-07 | 1966-07-26 | Aluminium Lab Ltd | Method of making low soda alumina of small crystal size |
| US4045234A (en) * | 1976-08-23 | 1977-08-30 | Kaiser Aluminum & Chemical Corporation | Process for producing high density sintered alumina |
| DE2816194A1 (de) * | 1978-04-14 | 1979-10-25 | Giulini Chemie | Sinteraktive und alkaliarme tonerde |
| CH654819A5 (de) * | 1980-09-23 | 1986-03-14 | Alusuisse | Verfahren zur herstellung von grobkristallinem alpha-aluminiumoxid und dessen verwendung. |
| HU185474B (en) * | 1981-11-10 | 1985-02-28 | Almasfuezitoei Timfoeldgyar | Process for preparing alpha-aluminium oxyde poor in alkali for ceramic purposes |
-
1981
- 1981-11-10 HU HU813358A patent/HU185474B/hu not_active IP Right Cessation
-
1982
- 1982-11-09 US US06/440,260 patent/US4477427A/en not_active Expired - Fee Related
- 1982-11-09 CS CS827974A patent/CS244120B2/cs unknown
- 1982-11-09 GB GB08231972A patent/GB2108949B/en not_active Expired
- 1982-11-10 DE DE19823241582 patent/DE3241582A1/de active Granted
- 1982-11-10 IT IT24155/82A patent/IT1191068B/it active
- 1982-11-10 FR FR8218881A patent/FR2535703B1/fr not_active Expired
- 1982-11-10 DD DD82244749A patent/DD205675A5/de not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| IT1191068B (it) | 1988-02-24 |
| DE3241582A1 (de) | 1983-06-01 |
| HU185474B (en) | 1985-02-28 |
| IT8224155A0 (it) | 1982-11-10 |
| DE3241582C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1991-07-25 |
| US4477427A (en) | 1984-10-16 |
| CS797482A2 (en) | 1985-08-15 |
| FR2535703A1 (fr) | 1984-05-11 |
| GB2108949A (en) | 1983-05-25 |
| GB2108949B (en) | 1985-03-06 |
| DD205675A5 (de) | 1984-01-04 |
| FR2535703B1 (fr) | 1985-11-22 |
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