CN1131218C - 一种制备1－取代的5－或3－羟基吡唑的方法 - Google Patents

一种制备1－取代的5－或3－羟基吡唑的方法 Download PDF

Info

Publication number
CN1131218C
CN1131218C CN99814530A CN99814530A CN1131218C CN 1131218 C CN1131218 C CN 1131218C CN 99814530 A CN99814530 A CN 99814530A CN 99814530 A CN99814530 A CN 99814530A CN 1131218 C CN1131218 C CN 1131218C
Authority
CN
China
Prior art keywords
formula
alkyl
hydroxypyrazoles
methyl
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN99814530A
Other languages
English (en)
Chinese (zh)
Other versions
CN1330639A (zh
Inventor
V·梅沃尔德
A·斯泰恩梅兹
M·莱克
N·高兹
R·高兹
J·汉克尔曼
H·贝克
J·J·艾斯卡贝耶图
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of CN1330639A publication Critical patent/CN1330639A/zh
Application granted granted Critical
Publication of CN1131218C publication Critical patent/CN1131218C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
CN99814530A 1998-11-19 1999-11-06 一种制备1－取代的5－或3－羟基吡唑的方法 Expired - Fee Related CN1131218C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19853502 1998-11-19
DE19853502.3 1998-11-19

Publications (2)

Publication Number Publication Date
CN1330639A CN1330639A (zh) 2002-01-09
CN1131218C true CN1131218C (zh) 2003-12-17

Family

ID=7888404

Family Applications (1)

Application Number Title Priority Date Filing Date
CN99814530A Expired - Fee Related CN1131218C (zh) 1998-11-19 1999-11-06 一种制备1－取代的5－或3－羟基吡唑的方法

Country Status (27)

Country Link
US (1) US6392058B1 (https=)
EP (1) EP1131299B1 (https=)
JP (1) JP2002530381A (https=)
KR (1) KR100606323B1 (https=)
CN (1) CN1131218C (https=)
AR (1) AR021315A1 (https=)
AT (1) ATE250037T1 (https=)
AU (1) AU766546B2 (https=)
BG (1) BG65026B1 (https=)
BR (1) BR9915492A (https=)
CA (1) CA2351370C (https=)
CZ (1) CZ301828B6 (https=)
DE (1) DE59907053D1 (https=)
DK (1) DK1131299T3 (https=)
EA (1) EA003753B1 (https=)
ES (1) ES2207988T3 (https=)
HU (1) HU224721B1 (https=)
IL (1) IL143035A (https=)
NO (1) NO318052B1 (https=)
NZ (1) NZ511645A (https=)
PL (1) PL205283B1 (https=)
PT (1) PT1131299E (https=)
SK (1) SK286367B6 (https=)
TR (1) TR200101404T2 (https=)
UA (1) UA67815C2 (https=)
WO (1) WO2000031042A2 (https=)
ZA (1) ZA200104961B (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108129305A (zh) * 2017-12-25 2018-06-08 凯莱英生命科学技术(天津)有限公司 E-烷氧基丙烯酸酯连续合成的方法

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
UA67815C2 (uk) 1998-11-19 2004-07-15 Басф Акцієнгезелльшафт Спосіб одержання 1-заміщених 5- або 3-гідроксипіразолів
CN101781201B (zh) * 2009-06-26 2013-07-31 上海海事大学 一种合成3-烷氧基丙烯酸酯的改进工艺
CN103698459A (zh) * 2013-12-30 2014-04-02 中美华世通生物医药科技（武汉）有限公司 一种药物中游离肼的检测方法
CN104059020B (zh) * 2014-06-27 2016-08-31 湖南海利常德农药化工有限公司 1-芳基-5-羟基吡唑的制备方法
WO2016184378A1 (zh) 2015-05-18 2016-11-24 沈阳中化农药化工研发有限公司 含嘧啶的取代吡唑类化合物及其制备方法和用途
CN109320457A (zh) * 2018-10-12 2019-02-12 凯莱英医药化学（阜新）技术有限公司 羟基吡唑类化合物的制备方法及装置
CN112480008B (zh) * 2020-12-21 2022-10-11 浙江工业大学 一种1-甲基-5-羟基吡唑的合成方法
WO2024100791A1 (ja) 2022-11-09 2024-05-16 株式会社日本ファインケム １－アルキル－５－ヒドロキシピラゾールの製造方法

Family Cites Families (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5714997A (en) 1980-06-30 1982-01-26 Matsushita Electric Works Ltd Signal processing circuit for ionization smoke sensor
JPS58140073A (ja) 1982-02-09 1983-08-19 Nissan Chem Ind Ltd １−メチル−５−ハイドロキシピラゾ−ルの製造法
JPS58174369A (ja) 1983-03-26 1983-10-13 Nissan Chem Ind Ltd １−メチル−５−ハイドロキシピラゾ−ル−４−カルボン酸低級アルキルエステルおよびその製造法
JPS6051175A (ja) 1983-08-30 1985-03-22 Nissan Chem Ind Ltd ピラゾ−ル誘導体および選択性除草剤
JPS61189271A (ja) * 1985-02-19 1986-08-22 Ube Ind Ltd １−メチル−５−ヒドロキシピラゾ−ルの製法
JPH0662577B2 (ja) 1985-04-03 1994-08-17 日産化学工業株式会社 １−メチル−５−ヒドロキシピラゾ−ルの製造法
JPS61257974A (ja) 1985-05-11 1986-11-15 Nissan Chem Ind Ltd ピラゾ−ル誘導体，その製造方法および選択性除草剤
US4744815A (en) 1985-05-11 1988-05-17 Nissan Chemical Industries, Ltd. 4-benzoyl-1-alkyl (alkenyl) - pyrazoles, composition containing them, herbicidal method of using them, and intermediate in their preparation
US4643757A (en) 1985-05-20 1987-02-17 Nissan Chemical Industries, Ltd. Herbicidal 4-benzoyl-1-methyl-5-hydroxypyrazoles
JPH0688977B2 (ja) 1985-05-23 1994-11-09 日産化学工業株式会社 １−メチル−５−ヒドロキシピラゾ−ルの製造法
JPH0730031B2 (ja) * 1986-04-02 1995-04-05 日産化学工業株式会社 ２―ピラゾリン―５―オン類の製造法
DE4230283A1 (de) * 1992-09-10 1994-03-17 Basf Ag Verfahren zur Herstellung von alpha, beta-ungesättigten beta-Oxycarbonsäurechloriden
US5607898A (en) 1993-08-02 1997-03-04 Idemitsu Kosan Company, Ltd. Pyrazole derivatives
JPH0735361B2 (ja) 1993-09-09 1995-04-19 日産化学工業株式会社 ヒドラゾン誘導体およびその製造方法
BR9508191A (pt) 1994-06-27 1997-08-12 Idemitsu Kosan Co Composição herbicida
EP0810226B1 (en) 1995-02-13 2003-05-02 Idemitsu Kosan Company Limited Pyrazole derivatives
JP4117386B2 (ja) 1995-02-24 2008-07-16 ビーエーエスエフ ソシエタス・ヨーロピア ピラゾリルベンゾイル誘導体
AR001805A1 (es) 1995-03-28 1997-12-10 Idemitsu Kosan Co Derivado de pirazol, acido carboxilico util como material de partida en la sintesis de dicho derivado y composicion herbicida que lo contiene
EP0819691A4 (en) 1995-04-05 1998-07-29 Idemitsu Kosan Co PYRAZOLE DERIVATIVES
BR9609502A (pt) 1995-06-29 1999-05-25 Du Pont Composto composição herbicida e método para controle do crescimento de vegetação indesejável
WO1997008164A1 (en) 1995-08-25 1997-03-06 E.I. Du Pont De Nemours And Company Bicyclic herbicides
EP0970956A4 (en) 1995-10-04 2000-01-12 Idemitsu Kosan Co PYRAZOLE DERIVATIVES
US5985799A (en) 1995-11-17 1999-11-16 E.I. Du Pont De Nemours And Company Tricyclic herbicidal heterocycles
WO1997023135A1 (fr) 1995-12-25 1997-07-03 Idemitsu Kosan Co., Ltd. Composition herbicide
US5631210A (en) 1996-06-14 1997-05-20 E. I. Du Pont De Nemours And Company Herbicidal thiophene ketones
JP3719318B2 (ja) * 1996-10-18 2005-11-24 宇部興産株式会社 １−エチル−５−ヒドロキシピラゾールの製法
US5808092A (en) 1996-10-18 1998-09-15 Ube Industries, Ltd. Process for preparing-1-ethyl-5-hydroxypyrazole
US5663365A (en) * 1996-10-29 1997-09-02 Japan Hydrazine Co., Ltd. Process for the preparation of pyrazolones
UA67815C2 (uk) 1998-11-19 2004-07-15 Басф Акцієнгезелльшафт Спосіб одержання 1-заміщених 5- або 3-гідроксипіразолів

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108129305A (zh) * 2017-12-25 2018-06-08 凯莱英生命科学技术(天津)有限公司 E-烷氧基丙烯酸酯连续合成的方法

Also Published As

Publication number Publication date
HUP0104504A3 (en) 2002-12-28
AR021315A1 (es) 2002-07-17
IL143035A0 (en) 2002-04-21
IL143035A (en) 2005-07-25
KR100606323B1 (ko) 2006-08-02
DE59907053D1 (de) 2003-10-23
WO2000031042A2 (de) 2000-06-02
CZ301828B6 (cs) 2010-07-07
EP1131299B1 (de) 2003-09-17
CZ20011713A3 (cs) 2002-01-16
ZA200104961B (en) 2002-06-18
JP2002530381A (ja) 2002-09-17
NO20012470D0 (no) 2001-05-18
WO2000031042A3 (de) 2000-10-26
EP1131299A2 (de) 2001-09-12
BG65026B1 (bg) 2006-12-29
AU1380900A (en) 2000-06-13
BG105538A (en) 2002-04-30
PL205283B1 (pl) 2010-03-31
EA003753B1 (ru) 2003-08-28
BR9915492A (pt) 2001-08-07
EA200100522A1 (ru) 2001-10-22
DK1131299T3 (da) 2004-02-02
CN1330639A (zh) 2002-01-09
NO20012470L (no) 2001-05-21
PT1131299E (pt) 2004-02-27
PL348751A1 (en) 2002-06-03
UA67815C2 (uk) 2004-07-15
HU224721B1 (en) 2006-01-30
KR20010080490A (ko) 2001-08-22
ES2207988T3 (es) 2004-06-01
NZ511645A (en) 2003-07-25
CA2351370A1 (en) 2000-06-02
SK286367B6 (sk) 2008-08-05
SK6792001A3 (en) 2001-11-06
AU766546B2 (en) 2003-10-16
ATE250037T1 (de) 2003-10-15
CA2351370C (en) 2008-03-11
TR200101404T2 (tr) 2002-01-21
NO318052B1 (no) 2005-01-24
US6392058B1 (en) 2002-05-21
HUP0104504A2 (hu) 2002-03-28

Similar Documents

Publication Publication Date Title
JP5284266B2 (ja) ジフルオロメチルピラゾリルカルボキシレートの調製方法
JP5889299B2 (ja) １−置換−３−フルオロアルキル−ピラゾール−４−カルボン酸のエステルの調製方法
CN1131218C (zh) 一种制备1－取代的5－或3－羟基吡唑的方法
US6133451A (en) Method for producing 2-(3-pyrazolyl-oxymethylene) nitrobenzenes
JP4114948B2 (ja) α−メトキシイミノカルボン酸メチルアミドの製造方法およびその中間生成物
TW201623245A (zh) 自α，α－二鹵胺類與酮亞胺類製備３，５－雙（鹵烷基）吡唑衍生物之方法
JP4672148B2 (ja) １−置換−５−ヒドロキシピラゾールの製造方法
CN1479723A (zh) 制备4-卤代烷基烟腈的方法
JP6514722B2 (ja) ケチミン類のアシル化を介した３，５−ビス（ハロアルキル）ピラゾール類の製造方法
JP4709456B2 (ja) ベンゾフラノンオキシムの製造方法
US20230095589A1 (en) One step process for the preparation of phenyl ethyl amine derivatives
KR101308227B1 (ko) 니코틴산 유도체 또는 그의 염의 제조 방법
CA2097184C (en) 2-aminocinnamic esters
JP2003246779A (ja) ４，５−ジアルコキシカルボニル又は４，５−ジシアノイミダゾールの製造方法
JP2002275155A (ja) 環状アミン誘導体の製造方法
JP2002128767A (ja) ２，４−オキサゾリジンジオン類の製造方法
JP2011051954A (ja) ピオグリタゾンの中間体、及びその製造方法、並びにピオグリタゾンまたはその塩酸塩の製造方法

Legal Events

Date Code Title Description
C06 Publication
C10 Entry into substantive examination
PB01 Publication
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20031217

Termination date: 20111106