CN103189943B - 稀土磁体的制备方法 - Google Patents
稀土磁体的制备方法 Download PDFInfo
- Publication number
- CN103189943B CN103189943B CN201180049051.8A CN201180049051A CN103189943B CN 103189943 B CN103189943 B CN 103189943B CN 201180049051 A CN201180049051 A CN 201180049051A CN 103189943 B CN103189943 B CN 103189943B
- Authority
- CN
- China
- Prior art keywords
- rare earth
- earth magnet
- heat treatment
- temperature
- grain boundary
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F41/00—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties
- H01F41/02—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets
- H01F41/0253—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets for manufacturing permanent magnets
- H01F41/0273—Imparting anisotropy
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/002—Ferrous alloys, e.g. steel alloys containing In, Mg, or other elements not provided for in one single group C22C38/001 - C22C38/60
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/005—Ferrous alloys, e.g. steel alloys containing rare earths, i.e. Sc, Y, Lanthanides
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/06—Ferrous alloys, e.g. steel alloys containing aluminium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/16—Ferrous alloys, e.g. steel alloys containing copper
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
- H01F1/01—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F41/00—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F41/00—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties
- H01F41/005—Impregnating or encapsulating
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F41/00—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties
- H01F41/32—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for applying conductive, insulating or magnetic material on a magnetic film, specially adapted for a thin magnetic film
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/24—After-treatment of workpieces or articles
- B22F2003/248—Thermal after-treatment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
- B22F2998/10—Processes characterised by the sequence of their steps
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2999/00—Aspects linked to processes or compositions used in powder metallurgy
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C2202/00—Physical properties
- C22C2202/02—Magnetic
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
- H01F1/01—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
- H01F1/03—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
- H01F1/032—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials
- H01F1/04—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials metals or alloys
- H01F1/047—Alloys characterised by their composition
- H01F1/053—Alloys characterised by their composition containing rare earth metals
- H01F1/055—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5
- H01F1/057—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B
- H01F1/0571—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes
- H01F1/0575—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes pressed, sintered or bonded together
- H01F1/0576—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes pressed, sintered or bonded together pressed, e.g. hot working
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
- H01F1/01—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
- H01F1/03—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
- H01F1/032—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials
- H01F1/04—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials metals or alloys
- H01F1/047—Alloys characterised by their composition
- H01F1/053—Alloys characterised by their composition containing rare earth metals
- H01F1/055—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5
- H01F1/057—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B
- H01F1/0571—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes
- H01F1/0575—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes pressed, sintered or bonded together
- H01F1/0577—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes pressed, sintered or bonded together sintered
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F10/00—Thin magnetic films, e.g. of one-domain structure
- H01F10/08—Thin magnetic films, e.g. of one-domain structure characterised by magnetic layers
- H01F10/10—Thin magnetic films, e.g. of one-domain structure characterised by magnetic layers characterised by the composition
- H01F10/12—Thin magnetic films, e.g. of one-domain structure characterised by magnetic layers characterised by the composition being metals or alloys
- H01F10/126—Thin magnetic films, e.g. of one-domain structure characterised by magnetic layers characterised by the composition being metals or alloys containing rare earth metals
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Power Engineering (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Hard Magnetic Materials (AREA)
- Manufacturing Cores, Coils, And Magnets (AREA)
- Powder Metallurgy (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP10306166.9A EP2444985B1 (en) | 2010-10-25 | 2010-10-25 | Production method of rare earth magnet |
| EP10306166.9 | 2010-10-25 | ||
| PCT/JP2011/061608 WO2012056755A1 (en) | 2010-10-25 | 2011-05-13 | Production method of rare earth magnet |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103189943A CN103189943A (zh) | 2013-07-03 |
| CN103189943B true CN103189943B (zh) | 2016-05-04 |
Family
ID=43272396
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201180049051.8A Expired - Fee Related CN103189943B (zh) | 2010-10-25 | 2011-05-13 | 稀土磁体的制备方法 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US9520230B2 (enExample) |
| EP (1) | EP2444985B1 (enExample) |
| JP (1) | JP5933535B2 (enExample) |
| CN (1) | CN103189943B (enExample) |
| WO (1) | WO2012056755A1 (enExample) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104011811B (zh) * | 2012-01-04 | 2016-11-02 | 丰田自动车株式会社 | 稀土类纳米复合磁铁 |
| US10234410B2 (en) | 2012-03-12 | 2019-03-19 | Massachusetts Institute Of Technology | Stable binary nanocrystalline alloys and methods of identifying same |
| JP6649876B2 (ja) | 2013-03-14 | 2020-02-19 | マサチューセッツ インスティテュート オブ テクノロジー | 焼結されたナノ結晶合金 |
| KR20150033423A (ko) * | 2013-09-24 | 2015-04-01 | 엘지전자 주식회사 | 열간가압성형 공정을 이용한 이방성 열간가압성형 자석의 제조방법 및 이 방법으로 제조된 열간가압성형 자석 |
| JP5915637B2 (ja) | 2013-12-19 | 2016-05-11 | トヨタ自動車株式会社 | 希土類磁石の製造方法 |
| JP5924335B2 (ja) | 2013-12-26 | 2016-05-25 | トヨタ自動車株式会社 | 希土類磁石とその製造方法 |
| KR101868763B1 (ko) * | 2014-10-27 | 2018-06-18 | 제이엑스금속주식회사 | 희토류 박막 자석 및 그 제조 방법 |
| US11644288B2 (en) | 2015-09-17 | 2023-05-09 | Massachusetts Institute Of Technology | Nanocrystalline alloy penetrators |
| JP6848735B2 (ja) * | 2016-07-15 | 2021-03-24 | Tdk株式会社 | R−t−b系希土類永久磁石 |
| JP6604321B2 (ja) * | 2016-12-27 | 2019-11-13 | トヨタ自動車株式会社 | 希土類磁石の製造方法 |
| US11167422B2 (en) | 2017-03-30 | 2021-11-09 | Soft Robotics, Inc. | User-assisted robotic control systems |
| CN109979743B (zh) * | 2017-12-27 | 2022-03-04 | 宁波科宁达工业有限公司 | 一种钕铁硼磁体晶界扩散的方法及稀土磁体 |
| JP7110662B2 (ja) * | 2018-03-28 | 2022-08-02 | Tdk株式会社 | R‐t‐b系焼結磁石 |
| US11004600B2 (en) | 2018-06-19 | 2021-05-11 | Ford Global Technologies, Llc | Permanent magnet and method of making permanent magnet |
| CN112053824B (zh) * | 2019-06-05 | 2023-08-22 | 中国科学院宁波材料技术与工程研究所 | 一种烧结钕铁硼永磁体及其制备方法 |
| WO2021039763A1 (ja) * | 2019-08-26 | 2021-03-04 | 日本電産株式会社 | モータ、駆動システム、掃除機、無人飛行体、電動航空機 |
| CN112908667B (zh) * | 2020-06-29 | 2022-07-15 | 京磁材料科技股份有限公司 | 稀土永磁体的晶界扩散方法 |
| CN115728684B (zh) * | 2022-11-17 | 2025-11-25 | 杭州美磁科技有限公司 | 通过磁场分布识别晶界扩散钕铁硼磁体不可逆退磁的方法 |
| CN116230346B (zh) | 2023-02-16 | 2023-08-22 | 四川大学 | 一种各向异性纳米晶稀土永磁体及制备方法 |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5055142A (en) * | 1986-05-23 | 1991-10-08 | Centre National De La Recherche Scientifique | Process for preparing permanent magnets by division of crystals |
| CN1363101A (zh) * | 2000-02-22 | 2002-08-07 | 住友特殊金属株式会社 | 永久磁铁薄膜及其制造方法 |
| CN1447354A (zh) * | 1998-03-23 | 2003-10-08 | 住友特殊金属株式会社 | 永久磁体和r-tm-b系永久磁体 |
| CN1461486A (zh) * | 2001-05-15 | 2003-12-10 | 住友特殊金属株式会社 | 铁基稀土合金纳米复合磁体及其制造方法 |
| CN1735947A (zh) * | 2002-05-24 | 2006-02-15 | 代顿大学 | 纳米晶态和纳米复合稀土永磁体材料及其制造方法 |
| CN101640087A (zh) * | 2008-07-04 | 2010-02-03 | 大同特殊钢株式会社 | 稀土磁体及其制造方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5405455A (en) | 1991-06-04 | 1995-04-11 | Shin-Etsu Chemical Co. Ltd. | Rare earth-based permanent magnet |
| JP2853839B2 (ja) | 1991-06-04 | 1999-02-03 | 信越化学工業株式会社 | 希土類永久磁石の製造方法 |
| JP2853838B2 (ja) | 1991-06-04 | 1999-02-03 | 信越化学工業株式会社 | 希土類永久磁石の製造方法 |
| US6287391B1 (en) * | 1997-06-26 | 2001-09-11 | Sumitomo Special Metals Co., Ltd. | Method of producing laminated permanent magnet |
| US20040025974A1 (en) | 2002-05-24 | 2004-02-12 | Don Lee | Nanocrystalline and nanocomposite rare earth permanent magnet materials and method of making the same |
| EP1744328B1 (en) * | 2005-06-10 | 2012-07-25 | Nissan Motor Co., Ltd. | Rare earth magnet having high strength and high electrical resistance |
| KR101378090B1 (ko) | 2007-05-02 | 2014-03-27 | 히다찌긴조꾸가부시끼가이사 | R-t-b계 소결 자석 |
| US20100261038A1 (en) * | 2007-11-02 | 2010-10-14 | Nobuyoshi Imaoka | Composite magnetic material for magnet and method for manufacturing such material |
| EP2099039A1 (en) | 2008-02-29 | 2009-09-09 | Daido Steel Co.,Ltd. | Material for magnetic anisotropic magnet |
| JP5532745B2 (ja) | 2009-08-21 | 2014-06-25 | 大同特殊鋼株式会社 | 磁気異方性磁石及びその製造方法 |
| CN104143402B (zh) * | 2009-01-07 | 2017-05-24 | 大同特殊钢株式会社 | 磁各向异性磁体原材料 |
| JP5692231B2 (ja) | 2010-07-16 | 2015-04-01 | トヨタ自動車株式会社 | 希土類磁石の製造方法、及び希土類磁石 |
-
2010
- 2010-10-25 EP EP10306166.9A patent/EP2444985B1/en not_active Not-in-force
-
2011
- 2011-05-13 US US13/824,572 patent/US9520230B2/en not_active Expired - Fee Related
- 2011-05-13 WO PCT/JP2011/061608 patent/WO2012056755A1/en not_active Ceased
- 2011-05-13 CN CN201180049051.8A patent/CN103189943B/zh not_active Expired - Fee Related
- 2011-05-13 JP JP2013516808A patent/JP5933535B2/ja active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5055142A (en) * | 1986-05-23 | 1991-10-08 | Centre National De La Recherche Scientifique | Process for preparing permanent magnets by division of crystals |
| CN1447354A (zh) * | 1998-03-23 | 2003-10-08 | 住友特殊金属株式会社 | 永久磁体和r-tm-b系永久磁体 |
| CN1363101A (zh) * | 2000-02-22 | 2002-08-07 | 住友特殊金属株式会社 | 永久磁铁薄膜及其制造方法 |
| CN1461486A (zh) * | 2001-05-15 | 2003-12-10 | 住友特殊金属株式会社 | 铁基稀土合金纳米复合磁体及其制造方法 |
| CN1735947A (zh) * | 2002-05-24 | 2006-02-15 | 代顿大学 | 纳米晶态和纳米复合稀土永磁体材料及其制造方法 |
| CN101640087A (zh) * | 2008-07-04 | 2010-02-03 | 大同特殊钢株式会社 | 稀土磁体及其制造方法 |
Non-Patent Citations (1)
| Title |
|---|
| Growth and characterization of NdFeB thin films;L.Castaldi et al;《Journal of Magnetism and Magnetic Materials》;20020430;第242-245卷;1284-1286 * |
Also Published As
| Publication number | Publication date |
|---|---|
| EP2444985B1 (en) | 2018-07-11 |
| JP5933535B2 (ja) | 2016-06-08 |
| WO2012056755A1 (en) | 2012-05-03 |
| US20130248754A1 (en) | 2013-09-26 |
| JP2014502034A (ja) | 2014-01-23 |
| EP2444985A1 (en) | 2012-04-25 |
| US9520230B2 (en) | 2016-12-13 |
| CN103189943A (zh) | 2013-07-03 |
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