CN101573308B - 氧化锆主体以及方法 - Google Patents

氧化锆主体以及方法 Download PDF

Info

Publication number
CN101573308B
CN101573308B CN200780048622.XA CN200780048622A CN101573308B CN 101573308 B CN101573308 B CN 101573308B CN 200780048622 A CN200780048622 A CN 200780048622A CN 101573308 B CN101573308 B CN 101573308B
Authority
CN
China
Prior art keywords
zirconia
sintered body
methods according
translucent
primary particle
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN200780048622.XA
Other languages
English (en)
Chinese (zh)
Other versions
CN101573308A (zh
Inventor
杰奎琳·C·罗尔夫
马丁·果兹格尔
霍尔格·豪普特曼
彼得·比辛格尔
鲁迪格尔·弗兰克
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Innovative Properties Co
Original Assignee
3M Innovative Properties Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 3M Innovative Properties Co filed Critical 3M Innovative Properties Co
Publication of CN101573308A publication Critical patent/CN101573308A/zh
Application granted granted Critical
Publication of CN101573308B publication Critical patent/CN101573308B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/48—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zirconium or hafnium oxides, zirconates, zircon or hafnates
    • C04B35/486—Fine ceramics
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61C—DENTISTRY; APPARATUS OR METHODS FOR ORAL OR DENTAL HYGIENE
    • A61C8/00—Means to be fixed to the jaw-bone for consolidating natural teeth or for fixing dental prostheses thereon; Dental implants; Implanting tools
    • A61C8/0012—Means to be fixed to the jaw-bone for consolidating natural teeth or for fixing dental prostheses thereon; Dental implants; Implanting tools characterised by the material or composition, e.g. ceramics, surface layer, metal alloy
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K6/00—Preparations for dentistry
    • A61K6/15—Compositions characterised by their physical properties
    • A61K6/17—Particle size
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K6/00—Preparations for dentistry
    • A61K6/80—Preparations for artificial teeth, for filling teeth or for capping teeth
    • A61K6/802—Preparations for artificial teeth, for filling teeth or for capping teeth comprising ceramics
    • A61K6/818—Preparations for artificial teeth, for filling teeth or for capping teeth comprising ceramics comprising zirconium oxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605—Treating the starting powders individually or as mixtures
    • C04B35/62625—Wet mixtures
    • C04B35/6263—Wet mixtures characterised by their solids loadings, i.e. the percentage of solids
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605—Treating the starting powders individually or as mixtures
    • C04B35/62625—Wet mixtures
    • C04B35/6264—Mixing media, e.g. organic solvents
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/64—Burning or sintering processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3208—Calcium oxide or oxide-forming salts thereof, e.g. lime
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C04B2235/3225—Yttrium oxide or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3251—Niobium oxides, niobates, tantalum oxides, tantalates, or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
    • C04B2235/449—Organic acids, e.g. EDTA, citrate, acetate, oxalate
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/52—Constituents or additives characterised by their shapes
    • C04B2235/5296—Constituents or additives characterised by their shapes with a defined aspect ratio, e.g. indicating sphericity
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54—Particle size related information
    • C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
    • C04B2235/5454—Particle size related information expressed by the size of the particles or aggregates thereof nanometer sized, i.e. below 100 nm
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/602—Making the green bodies or pre-forms by moulding
    • C04B2235/6027—Slip casting
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/608—Green bodies or pre-forms with well-defined density
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/612—Machining
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6562—Heating rate
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74—Physical characteristics
    • C04B2235/76—Crystal structural characteristics, e.g. symmetry
    • C04B2235/765—Tetragonal symmetry
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74—Physical characteristics
    • C04B2235/77—Density
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74—Physical characteristics
    • C04B2235/78—Grain sizes and shapes, product microstructures, e.g. acicular grains, equiaxed grains, platelet-structures
    • C04B2235/781—Nanograined materials, i.e. having grain sizes below 100 nm
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
    • C04B2235/9646—Optical properties
    • C04B2235/9653—Translucent or transparent ceramics other than alumina

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Structural Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Public Health (AREA)
  • Epidemiology (AREA)
  • Veterinary Medicine (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Nanotechnology (AREA)
  • Composite Materials (AREA)
  • Physics & Mathematics (AREA)
  • Plastic & Reconstructive Surgery (AREA)
  • Dentistry (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Orthopedic Medicine & Surgery (AREA)
  • Compositions Of Oxide Ceramics (AREA)
  • Dental Tools And Instruments Or Auxiliary Dental Instruments (AREA)
CN200780048622.XA 2006-12-29 2007-12-28 氧化锆主体以及方法 Expired - Fee Related CN101573308B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US88271406P 2006-12-29 2006-12-29
US60/882,714 2006-12-29
PCT/US2007/089057 WO2008083282A2 (en) 2006-12-29 2007-12-28 Zirconia body and methods

Publications (2)

Publication Number Publication Date
CN101573308A CN101573308A (zh) 2009-11-04
CN101573308B true CN101573308B (zh) 2016-11-09

Family

ID=39589214

Family Applications (1)

Application Number Title Priority Date Filing Date
CN200780048622.XA Expired - Fee Related CN101573308B (zh) 2006-12-29 2007-12-28 氧化锆主体以及方法

Country Status (5)

Country Link
US (2) US20100041542A1 (enExample)
EP (1) EP2104654A2 (enExample)
JP (1) JP5331705B2 (enExample)
CN (1) CN101573308B (enExample)
WO (1) WO2008083282A2 (enExample)

Families Citing this family (45)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5018142B2 (ja) * 2007-03-07 2012-09-05 東ソー株式会社 透光性ジルコニア焼結体及びその製造方法
WO2009048573A2 (en) * 2007-10-10 2009-04-16 Massachusetts Institute Of Technology Densification of metal oxides
GB2464473B (en) 2008-10-15 2012-09-12 Univ Loughborough Deformable granule production
JP5397829B2 (ja) * 2008-12-04 2014-01-22 堺化学工業株式会社 酸化ジルコニウム分散液の製造方法
JP5549122B2 (ja) * 2009-06-15 2014-07-16 住友大阪セメント株式会社 透光性セラミックス及びその製造方法
CN102471168B (zh) * 2009-08-07 2017-05-03 东曹株式会社 透明氧化锆烧结体、其生产方法及其用途
DE102009039102B4 (de) * 2009-08-27 2022-01-27 Wdt-Wolz-Dental-Technik Gmbh Verfahren zur Herstellung von Zahnteilen aus Dentalmetallpulver
US8598058B2 (en) 2009-12-29 2013-12-03 3M Innovative Properties Company Zirconia-based material doped with yttrium and lanthanum
JP5814937B2 (ja) 2009-12-29 2015-11-17 スリーエム イノベイティブ プロパティズ カンパニー ランタニド元素をドープしたジルコニア系粒子
US8298329B2 (en) * 2010-04-29 2012-10-30 James R. Glidewell Dental Ceramics, Inc. Nano-crystalline dental ceramics
DE102011075808B4 (de) * 2010-09-10 2017-06-29 Biolitec Ag Implantat zur Anwendung bei einer photo-dynamischen Behandlung sowie Verfahren zur Herstellung des Implantats
CN102344285B (zh) * 2011-07-04 2013-04-17 辽宁爱尔创生物材料有限公司 改变牙科氧化锆材料透光性的方法
JP4926287B1 (ja) * 2011-07-15 2012-05-09 菊水化学工業株式会社 インプラントフィクスチャー及びその製造方法
WO2013055432A1 (en) 2011-10-10 2013-04-18 3M Innovative Properties Company Aerogels, calcined and crystalline articles and methods of making the same
US8936848B2 (en) * 2012-02-23 2015-01-20 B&D Dental Corp Non-pre-colored multi-layer zirconia dental blank that has a gradual change in translucency through a thickness after sintering
US9434651B2 (en) 2012-05-26 2016-09-06 James R. Glidewell Dental Ceramics, Inc. Method of fabricating high light transmission zirconia blanks for milling into natural appearance dental appliances
DE102012213279A1 (de) * 2012-07-27 2014-01-30 Sirona Dental Systems Gmbh Sinterofen für Bauteile aus einem Sinterwerkstoff, insbesondere für Dentalbauteile und Verfahren zur Sinterung derartiger Bauteile
CN104918577B (zh) * 2012-08-03 2018-10-23 3M创新有限公司 用于氧化锆陶瓷的半透明度增强溶液
EP2692311B1 (en) * 2012-08-03 2016-06-22 3M Innovative Properties Company Dental blank comprising a pre-sintered porous zirconia material , process of its production and dental article formed from said dental blank
RU2607847C2 (ru) 2012-09-20 2017-01-20 3М Инновейтив Пропертиз Компани Окрашивание керамики на основе диоксида циркония
US10028809B2 (en) * 2012-10-17 2018-07-24 3M Innovative Properties Company Multi sectional dental zirconia milling block, process of production and use thereof
CN105338948B (zh) * 2013-06-27 2019-02-01 义获嘉伟瓦登特股份有限公司 纳米晶体氧化锆及其加工方法
US9878954B2 (en) 2013-09-13 2018-01-30 3M Innovative Properties Company Vacuum glazing pillars for insulated glass units
WO2015038890A1 (en) * 2013-09-13 2015-03-19 3M Innovative Properties Company Metal oxide particles
CN105705112B (zh) 2013-10-04 2018-02-27 3M创新有限公司 牙科研磨坯料、牙科修复体以及形成牙科研磨坯料的方法
CN103641472B (zh) * 2013-11-14 2015-04-15 厦门惠方生物科技有限公司 一种制备着色半透性氧化锆预烧结体的方法
EP3076894B1 (en) * 2013-12-04 2017-11-22 3M Innovative Properties Company Dental mill blank, process for production and use thereof
EP3137013A4 (en) * 2014-04-30 2018-09-19 Osseodyne Surgical Solutions, LLC Osseointegrative surgical implant
WO2015168332A2 (en) * 2014-04-30 2015-11-05 Osseodyne Surgical Solutions, Llc Osseointegrative surgical implant
JP6359400B2 (ja) * 2014-09-22 2018-07-18 クラレノリタケデンタル株式会社 透光性ジルコニア焼結体の製造方法及びその製造方法によって得られる透光性ジルコニア焼結体、並びに、透光性ジルコニア焼結体作製用の焼結前仮焼体
JP6326363B2 (ja) * 2014-12-22 2018-05-16 クラレノリタケデンタル株式会社 ジルコニア組成物、ジルコニア仮焼体、ジルコニア焼結体及びジルコニア焼結体の製造方法、並びに歯科用製品
WO2016191162A1 (en) 2015-05-28 2016-12-01 3M Innovative Properties Company Additive manufacturing process for producing ceramic articles using a sol containing nano-sized particles
EP3303254B1 (en) 2015-05-28 2022-06-29 3M Innovative Properties Company Use of a sol containing nano zirconia particles in an additive manufacturing process and a process
US9822039B1 (en) 2016-08-18 2017-11-21 Ivoclar Vivadent Ag Metal oxide ceramic nanomaterials and methods of making and using same
KR102658088B1 (ko) 2017-07-31 2024-04-17 쿠라레 노리타케 덴탈 가부시키가이샤 지르코니아 입자를 포함하는 분말의 제조 방법
JP6949606B2 (ja) * 2017-07-31 2021-10-13 クラレノリタケデンタル株式会社 ジルコニア成形体の製造方法
JP6978925B2 (ja) * 2017-12-18 2021-12-08 クラレノリタケデンタル株式会社 歯科用ジルコニア仮焼体
US11731312B2 (en) 2020-01-29 2023-08-22 James R. Glidewell Dental Ceramics, Inc. Casting apparatus, cast zirconia ceramic bodies and methods for making the same
JP7367207B2 (ja) * 2020-05-12 2023-10-23 共立マテリアル株式会社 透光性高靭化ジルコニア焼結体
FR3112770A1 (fr) * 2020-07-23 2022-01-28 Mathym Céramique d’oxyde métallique, ses précurseurs, sa préparation et son utilisation
EP4063337A1 (en) * 2021-03-26 2022-09-28 Glassomer GmbH Material and process for fabricating and shaping of transparent ceramics
CN113683412B (zh) * 2021-10-11 2022-10-28 福建省长汀金龙稀土有限公司 一种柱状晶氧化锆粉体及其制备方法与应用
KR102711498B1 (ko) * 2021-11-30 2024-09-26 아주대학교산학협력단 세가지 치과용 지르코니아의 표면 형상 변화와 잔류 응력 개선을 위한 샌드블라스팅 표면처리방법
CN114315348B (zh) * 2021-12-22 2023-06-30 西南科技大学 一种全稳定四方ysz靶材及超长寿命eb-pvd涂层的制备方法
WO2023127793A1 (ja) * 2021-12-27 2023-07-06 クラレノリタケデンタル株式会社 ジルコニア焼結体及びその製造方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4742030A (en) * 1985-09-06 1988-05-03 Toray Industries, Inc. Sintered zirconia material and method for manufacturing the material

Family Cites Families (40)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2578241B1 (fr) * 1985-03-01 1990-03-30 Rhone Poulenc Spec Chim Zircone stabilisee, son procede de preparation et son application dans des compositions ceramiques
DE3683959D1 (de) 1985-06-20 1992-04-02 Tosoh Corp Zirkoniumdioxidsinterkoerper mit verbesserter lichtdurchlaessigkeit.
JPS62153163A (ja) * 1985-09-06 1987-07-08 東レ株式会社 ジルコニア焼結体
US4639356A (en) 1985-11-05 1987-01-27 American Cyanamid Company High technology ceramics with partially stabilized zirconia
IT1217414B (it) 1988-04-14 1990-03-22 Istituto Guido Donegami S P A Processo per la preparazione di polveri submicroniche di ossido di zirconio stabilizzato con ossido i ittrio
US5453262A (en) 1988-12-09 1995-09-26 Battelle Memorial Institute Continuous process for production of ceramic powders with controlled morphology
US5037579A (en) 1990-02-12 1991-08-06 Nalco Chemical Company Hydrothermal process for producing zirconia sol
JPH0679965B2 (ja) * 1991-04-12 1994-10-12 株式会社コロイドリサーチ ジルコニアゾルの製造方法およびジルコニア成形体の製造方法
CA2074235C (en) 1991-07-18 2000-02-08 Hiroshi Itoh Hardenable composition, aqueous gel and applications thereof
US5152149A (en) 1991-07-23 1992-10-06 The Boc Group, Inc. Air separation method for supplying gaseous oxygen in accordance with a variable demand pattern
US5652192A (en) 1992-07-10 1997-07-29 Battelle Memorial Institute Catalyst material and method of making
US6030914A (en) 1996-11-12 2000-02-29 Tosoh Corporation Zirconia fine powder and method for its production
US6087285A (en) 1997-10-13 2000-07-11 Tosoh Corporation Zirconia sintered body, process for production thereof, and application thereof
DE19746265A1 (de) 1997-10-20 1999-04-22 Bayer Ag Verbunde aus Polyurethan und einem thermoplastischen Material
JP3799459B2 (ja) * 1997-11-11 2006-07-19 博 木村 アモルファスセラミックス粉末製高密度焼結体の製造方法
JP3134092B2 (ja) * 1997-11-11 2001-02-13 ファインセラミックス技術研究組合 酸化ジルコニウム系焼結体およびその製造方法
US6030606A (en) 1998-06-22 2000-02-29 3M Innovative Properties Company Dental restoratives comprising Bis-EMA6
JP4524463B2 (ja) 1999-07-27 2010-08-18 三井化学株式会社 ガスバリア性ポリウレタン樹脂及びこれを含むガスバリア性フィルム
DE19938143A1 (de) 1999-08-16 2001-02-22 Espe Dental Ag Verwendung von Zirkonoxidkeramiken mit Sinterzusatz zur Herstellung von Zahnersatz
US6376590B2 (en) 1999-10-28 2002-04-23 3M Innovative Properties Company Zirconia sol, process of making and composite material
US6962946B2 (en) 2001-11-21 2005-11-08 3M Innovative Properties Company Nanoparticles having a rutile-like crystalline phase and method of preparing same
US6878456B2 (en) 2001-12-28 2005-04-12 3M Innovative Properties Co. Polycrystalline translucent alumina-based ceramic material, uses, and methods
JP2003206137A (ja) * 2002-01-11 2003-07-22 Dowa Mining Co Ltd 部分安定化または安定化ジルコニア微粉体とその前駆体およびそれらの製造方法
DE10261720A1 (de) 2002-12-30 2004-07-15 Meyer, Gerhard, Prof. Dr. Fräskeramiken aus Metalloxid-Pulvern mit bimodaler Korngrößenverteilung
JP4470378B2 (ja) * 2003-02-28 2010-06-02 住友化学株式会社 ジルコニア焼結体およびその製造方法
JP4210533B2 (ja) * 2003-03-11 2009-01-21 第一工業製薬株式会社 易焼結性正方晶ジルコニア粉末およびその製造方法
TWI252215B (en) 2003-03-27 2006-04-01 Univ Nat Central Zirconia sol and method of preparing the same
US7169375B2 (en) 2003-08-29 2007-01-30 General Electric Company Metal oxide nanoparticles, methods of making, and methods of use
US7074463B2 (en) 2003-09-12 2006-07-11 3M Innovative Properties Company Durable optical element
US20050148735A1 (en) 2003-12-30 2005-07-07 Olson David B. Polymerizable composition for optical articles
US20050147838A1 (en) 2003-12-30 2005-07-07 3M Innovative Properties Company Polymerizable compositions for optical articles
JP2005193494A (ja) 2004-01-06 2005-07-21 Toyo Tire & Rubber Co Ltd 押出機用ダイインサート
CN101039877A (zh) * 2004-09-01 2007-09-19 先进纳米技术有限公司 氧化锆陶瓷
US7241437B2 (en) 2004-12-30 2007-07-10 3M Innovative Properties Company Zirconia particles
JP5356639B2 (ja) * 2005-03-04 2013-12-04 東ソー株式会社 ジルコニア微粉末及びその製造方法
US20060204745A1 (en) 2005-03-14 2006-09-14 Jones Clint L Light management films with zirconia particles
US20060204676A1 (en) 2005-03-11 2006-09-14 Jones Clinton L Polymerizable composition comprising low molecular weight organic component
JP5277541B2 (ja) * 2006-07-25 2013-08-28 東ソー株式会社 高強度ジルコニア焼結体および製造方法
JP5061554B2 (ja) * 2006-09-25 2012-10-31 東ソー株式会社 ジルコニア微粉末及びその製造方法
EP2620413B1 (en) 2007-12-28 2020-07-01 3M Innovative Properties Company Continuous hydrothermal reactor system comprising a fluorinated polymer tubular reactor

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4742030A (en) * 1985-09-06 1988-05-03 Toray Industries, Inc. Sintered zirconia material and method for manufacturing the material

Also Published As

Publication number Publication date
US8309015B2 (en) 2012-11-13
US20110260349A1 (en) 2011-10-27
WO2008083282A2 (en) 2008-07-10
JP5331705B2 (ja) 2013-10-30
US20100041542A1 (en) 2010-02-18
CN101573308A (zh) 2009-11-04
EP2104654A2 (en) 2009-09-30
JP2010514665A (ja) 2010-05-06
WO2008083282A3 (en) 2009-03-19

Similar Documents

Publication Publication Date Title
CN101573308B (zh) 氧化锆主体以及方法
EP3303255B1 (en) Additive manufacturing process for producing ceramic articles using a sol containing nano-sized particles
EP3284724B1 (en) Aerogels, calcined and crystalline articles and methods of making the same
US7655586B1 (en) Dental restorations using nanocrystalline materials and methods of manufacture
EP3303254B1 (en) Use of a sol containing nano zirconia particles in an additive manufacturing process and a process
EP1836128B1 (en) Zirconia particles
JP4251758B2 (ja) ジルコニア焼結体からなる光ファイバーコネクター部品
EP2519478B1 (en) Zirconia-based material doped with yttrium and lanthanum
EP3583083B1 (en) Zirconia article with high alumina content, process of production and use thereof
KR102583377B1 (ko) 겔 조성물, 형상화된 겔 물품 및 소결 물품의 제조 방법
CN105338948A (zh) 纳米晶体氧化锆及其加工方法
JP7585695B2 (ja) ジルコニア焼結体及びその製造方法
JP7763859B2 (ja) ジルコニア組成物、ジルコニア仮焼体及びジルコニア焼結体並びにこれらの製造方法
Paygin et al. Effect of technological parameters on optical and mechanical properties of spark plasma sintered transparent YSZ ceramics
Zhou et al. Low-temperature fabrication of zirconia transparent ceramics via hydrothermal nanopowder
Díaz-Parralejo et al. A novel strategy for the preparation of yttria-stabilized zirconia powders: Deposition and scratching of thin films obtained by the sol–gel method
EP2945597B1 (en) Glass ceramic material and method
Shahmiri Characterisation and Modification of the Optical Properties of Zirconia-Based Ceramics for Aesthetic Dental Restorations
Il’icheva et al. Morphological properties of nanopowders of the system Al2O3–ZrO2–CeO2 as a function of the conditions for obtaining precursors
CN118302386A (zh) 粉末及其制造方法
BR102015010531A2 (pt) Process of synthetization of zan derived nanoceramics with praseodymia for application in the areas of health, biology, chemistry, laser, optical and luminescent devices, electronics and ceramic industry
JP2005320216A (ja) 合成ケイ素酸化物粒子とその製造方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20161109

Termination date: 20191228

CF01 Termination of patent right due to non-payment of annual fee