CN101189366B - 用于制备用以冷成型的金属工件的方法 - Google Patents

用于制备用以冷成型的金属工件的方法 Download PDF

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Publication number
CN101189366B
CN101189366B CN200680017145.6A CN200680017145A CN101189366B CN 101189366 B CN101189366 B CN 101189366B CN 200680017145 A CN200680017145 A CN 200680017145A CN 101189366 B CN101189366 B CN 101189366B
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Prior art keywords
phosphate
phosphating solution
coating
lubricant
phosphating
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CN200680017145.6A
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Chinese (zh)
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CN101189366A (zh
Inventor
K·-D·尼特尔
R·施奈德
A·兰
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Chemetall GmbH
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Chemetall GmbH
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    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
    • C25D11/36—Phosphatising
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
    • C23C22/08—Orthophosphates
    • C23C22/12—Orthophosphates containing zinc cations
    • C23C22/17—Orthophosphates containing zinc cations containing also organic acids
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
    • C23C22/08—Orthophosphates
    • C23C22/18—Orthophosphates containing manganese cations
    • C23C22/188—Orthophosphates containing manganese cations containing also magnesium cations
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
    • C23C22/08—Orthophosphates
    • C23C22/22—Orthophosphates containing alkaline earth metal cations
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31678—Of metal

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Electrochemistry (AREA)
  • Chemical Treatment Of Metals (AREA)
  • Lubricants (AREA)
CN200680017145.6A 2005-05-19 2006-05-03 用于制备用以冷成型的金属工件的方法 Active CN101189366B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102005023023.7A DE102005023023B4 (de) 2005-05-19 2005-05-19 Verfahren zur Vorbereitung von metallischen Werkstücken zum Kaltumformen, mit dem Verfahren beschichtete Werkstücke und ihre Verwendung
DE102005023023.7 2005-05-19
PCT/EP2006/004121 WO2006122651A1 (de) 2005-05-19 2006-05-03 Verfahren zur vorbereitung von metallischen werkstücken zum kaltumformen

Publications (2)

Publication Number Publication Date
CN101189366A CN101189366A (zh) 2008-05-28
CN101189366B true CN101189366B (zh) 2015-05-06

Family

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CN200680017145.6A Active CN101189366B (zh) 2005-05-19 2006-05-03 用于制备用以冷成型的金属工件的方法

Country Status (14)

Country Link
US (1) US20080166575A1 (cg-RX-API-DMAC7.html)
EP (1) EP1888819B1 (cg-RX-API-DMAC7.html)
JP (1) JP2008540845A (cg-RX-API-DMAC7.html)
CN (1) CN101189366B (cg-RX-API-DMAC7.html)
AU (1) AU2006246764B2 (cg-RX-API-DMAC7.html)
BR (1) BRPI0610136B1 (cg-RX-API-DMAC7.html)
CA (1) CA2608390C (cg-RX-API-DMAC7.html)
DE (1) DE102005023023B4 (cg-RX-API-DMAC7.html)
EA (1) EA012533B1 (cg-RX-API-DMAC7.html)
ES (1) ES2749926T3 (cg-RX-API-DMAC7.html)
MX (1) MX2007014320A (cg-RX-API-DMAC7.html)
UA (1) UA93509C2 (cg-RX-API-DMAC7.html)
WO (1) WO2006122651A1 (cg-RX-API-DMAC7.html)
ZA (1) ZA200710308B (cg-RX-API-DMAC7.html)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100792278B1 (ko) * 2007-02-27 2008-01-07 고려상사주식회사 인산염 피막 냉간 압조용 스테인리스 강선 및 이를 이용한직결 나사
DE102007061109B4 (de) * 2007-12-19 2013-01-17 Henkel Ag & Co. Kgaa Behandlungslösung zum Beschichten eines Stahlbandes, ein Verfahren zum Aufbringen derselben sowie ein Stahlband mit einer Beschichtung erhalten aus der Behandlungslösung zur Verbesserung des Umformverhaltens
TWI457431B (zh) 2008-01-30 2014-10-21 Chemetall Gmbh 將金屬表面施以一種潤滑劑組成物的方法
TWI457433B (zh) 2008-01-30 2014-10-21 Chemetall Gmbh 將金屬表面施以一磷酸鹽層然後施以一潤滑劑層的方法
TWI457432B (zh) 2008-01-30 2014-10-21 Chemetall Gmbh 將金屬表面施以一含蠟的潤滑劑組成物的方法
DE102008000600B4 (de) * 2008-03-11 2010-05-12 Chemetall Gmbh Verfahren zur Beschichtung von metallischen Oberflächen mit einem Passivierungsmittel, das Passivierungsmittel, die hiermit erzeugte Beschichtung und ihre Verwendung
DE102009041248A1 (de) * 2009-09-04 2011-05-05 Innotere Gmbh Bioaktiv beschichtete Metallimplantate und Verfahren zu deren Herstellung
DE102011009012A1 (de) * 2011-01-20 2012-07-26 Profil Verbindungstechnik Gmbh & Co. Kg Funktionselement in Form eines Einpresselements
CN102719872B (zh) * 2012-06-08 2018-04-27 南京派诺金属表面处理技术有限公司 一种无渣低温快速电解磷化液及其磷化工艺
CN102899702B (zh) * 2012-08-31 2015-10-28 华南理工大学 镁合金表面复合处理方法
MX368832B (es) * 2013-03-06 2019-10-18 Quaker Chem Corp Recubrimiento de conversión a alta temperatura sobre sustratos de acero y hierro.
CN103643230B (zh) * 2013-12-07 2015-07-15 山东建筑大学 一种适应温挤压的复合硫酸-磷酸钙盐表面处理方法
EP2883917A1 (de) * 2013-12-13 2015-06-17 Kronos International, Inc. Calciumphosphat-haltige Kompositpigmente und Verfahren zu ihrer Herstellung
CN104087919A (zh) * 2014-06-30 2014-10-08 张家港市华尊宝特种材料科技有限公司 一种异型钢管的表面磷化工艺
CN104451097A (zh) * 2014-09-26 2015-03-25 无锡市天力五金弹簧厂 一种弹簧渗碳淬火工艺
CN104962896B (zh) * 2015-06-30 2017-12-05 大连碧城环保科技股份有限公司 一种锌系磷化液添加剂及其使用方法
DE102016100245A1 (de) 2016-01-08 2017-07-13 Staku Anlagenbau Gmbh Selbstschmierende elektrolytisch abgeschiedene Phosphatierungsbeschichtung
DE102017124724B4 (de) 2016-10-25 2022-01-05 Koki Technik Transmission Systems Gmbh Verfahren zur Herstellung einer Schaltgabel
CN108949315B (zh) * 2018-06-25 2021-11-12 杰锡工业技术（上海）有限公司 一种环保节能的新型金属冷成型加工方法
CN109097809A (zh) * 2018-08-06 2018-12-28 佛山科学技术学院 一种高耐蚀厚磷化膜层的制备工艺
CN111575696A (zh) * 2020-06-20 2020-08-25 烟台博昌汽车标准件有限公司 一种螺栓磷化后表面处理设备与工艺
DE102021004167A1 (de) 2021-03-25 2022-09-29 Wilhelm Brummer Verfahren für Vorbehandlung von Stahl und Eisen in einem Behandlungsbad
EP4063535A3 (de) * 2021-03-25 2022-11-30 Brummer, Wilhelm Verfahren für vorbehandlung von stahl und eisen in einem behandlungsbad
CN113652727A (zh) * 2021-07-29 2021-11-16 天津正达科技有限责任公司 一种循环冷却水系统快速预膜方法
CN118291962B (zh) * 2024-03-25 2025-10-21 福建安泰新能源科技有限公司 一种高性能铝合金光伏支架挤压模具的保养工艺
WO2025237770A1 (en) 2024-05-14 2025-11-20 Chemetall Gmbh Process for preparing a workpiece prior metal forming

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4944813A (en) * 1988-01-14 1990-07-31 Gerhard Collardin Gmbh Process for phosphating metal surfaces
CN1242439A (zh) * 1998-07-01 2000-01-26 日本巴可莱新株式会社 在钢线材上迅速形成磷酸盐被膜的方法及装置
WO2000015879A1 (en) * 1998-09-11 2000-03-23 Henkel Corporation Method for forming a lubricative film for cold working
CN1248644A (zh) * 1998-09-11 2000-03-29 日本巴可莱新株式会社 形成冷挤压制造用润滑被膜的方法
CN1283710A (zh) * 2000-08-02 2001-02-14 暨南大学 钢铁冷变形加工的磷化液及其磷化工艺
US6346186B1 (en) * 1996-08-29 2002-02-12 Danfoss A/S Method for electrochemical phosphating of metal surfaces

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2132438A (en) * 1933-12-11 1938-10-11 American Chem Paint Co Method of coating metal
US3586612A (en) * 1969-03-27 1971-06-22 Council Scient Ind Res Anodic phosphating of metallic articles
JPS5429979B2 (cg-RX-API-DMAC7.html) * 1974-02-22 1979-09-27
SE406940B (sv) * 1974-04-13 1979-03-05 Collardin Gmbh Gerhard Forfarande for framstellning av fosfatbeleggningar med sprutningsmetoden pa jern och stal
JPS5456038A (en) * 1977-10-12 1979-05-04 Nippon Paint Co Ltd Controlling method for acidic phosphate film forming liquid
JPS6043491A (ja) * 1983-08-19 1985-03-08 Nippon Denso Co Ltd 鉄鋼表面に燐酸塩化成被膜を形成する方法
JPS6148597A (ja) * 1984-08-14 1986-03-10 Nippon Paint Co Ltd リン酸亜鉛化成処理法
JPS6250496A (ja) * 1985-08-29 1987-03-05 Nippon Kokan Kk <Nkk> 金属材料の電解処理方法
JPH01100281A (ja) * 1987-10-13 1989-04-18 Nippon Parkerizing Co Ltd 金属表面の皮膜化成処理液
DE3808609A1 (de) * 1988-03-15 1989-09-28 Electro Chem Eng Gmbh Verfahren zur erzeugung von korrosions- und verschleissbestaendigen schutzschichten auf magnesium und magnesiumlegierungen
JPH0436498A (ja) * 1990-06-01 1992-02-06 Nippon Parkerizing Co Ltd 鉄鋼線材の表面処理方法
DE4111186A1 (de) * 1991-04-06 1992-10-08 Henkel Kgaa Verfahren zum phosphatieren von metalloberflaechen
JPH0578881A (ja) * 1991-07-22 1993-03-30 Kawasaki Steel Corp 表面処理厚鋼板
DE4232292A1 (de) * 1992-09-28 1994-03-31 Henkel Kgaa Verfahren zum Phosphatieren von verzinkten Stahloberflächen
DE4433946A1 (de) * 1994-09-23 1996-03-28 Henkel Kgaa Phosphatierverfahren ohne Nachspülung
JPH1046351A (ja) * 1996-07-25 1998-02-17 Nippon Parkerizing Co Ltd 軸受用鋼線材の表面処理方法
JPH116076A (ja) * 1997-06-13 1999-01-12 Nippon Parkerizing Co Ltd 鉄鋼材料のりん酸塩処理方法
CN1221687C (zh) * 1998-12-17 2005-10-05 株式会社电装 电解磷酸盐的化学处理方法及在钢材表面形成的一种复合薄膜
DE10010355A1 (de) * 2000-03-07 2001-09-13 Chemetall Gmbh Verfahren zum Aufbringen eines Phosphatüberzuges und Verwendung der derart phosphatierten Metallteile
MXPA02011893A (es) * 2000-06-06 2004-09-06 Henkel Kgaa Revestimiento para metales de trabajo en frio.
US20050205166A1 (en) * 2002-07-10 2005-09-22 Jurgen Specht Method for coating metallic surfaces

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4944813A (en) * 1988-01-14 1990-07-31 Gerhard Collardin Gmbh Process for phosphating metal surfaces
US6346186B1 (en) * 1996-08-29 2002-02-12 Danfoss A/S Method for electrochemical phosphating of metal surfaces
CN1242439A (zh) * 1998-07-01 2000-01-26 日本巴可莱新株式会社 在钢线材上迅速形成磷酸盐被膜的方法及装置
WO2000015879A1 (en) * 1998-09-11 2000-03-23 Henkel Corporation Method for forming a lubricative film for cold working
CN1248644A (zh) * 1998-09-11 2000-03-29 日本巴可莱新株式会社 形成冷挤压制造用润滑被膜的方法
CN1283710A (zh) * 2000-08-02 2001-02-14 暨南大学 钢铁冷变形加工的磷化液及其磷化工艺

Also Published As

Publication number Publication date
ZA200710308B (en) 2009-05-27
EA012533B1 (ru) 2009-10-30
AU2006246764A1 (en) 2006-11-23
CN101189366A (zh) 2008-05-28
UA93509C2 (uk) 2011-02-25
ES2749926T3 (es) 2020-03-24
EA200702422A1 (ru) 2008-06-30
WO2006122651A1 (de) 2006-11-23
MX2007014320A (es) 2008-02-11
US20080166575A1 (en) 2008-07-10
BRPI0610136A2 (pt) 2010-06-01
EP1888819B1 (de) 2019-07-10
JP2008540845A (ja) 2008-11-20
DE102005023023A1 (de) 2006-11-23
CA2608390A1 (en) 2006-11-23
DE102005023023B4 (de) 2017-02-09
AU2006246764B2 (en) 2011-09-08
BRPI0610136B1 (pt) 2018-02-06
EP1888819A1 (de) 2008-02-20
CA2608390C (en) 2013-01-08

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