CN101040035B - 在曲轴箱油中作为燃料经济性改进剂和抗磨剂的酒石酸衍生物及其制备 - Google Patents
在曲轴箱油中作为燃料经济性改进剂和抗磨剂的酒石酸衍生物及其制备 Download PDFInfo
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- CN101040035B CN101040035B CN2005800348432A CN200580034843A CN101040035B CN 101040035 B CN101040035 B CN 101040035B CN 2005800348432 A CN2005800348432 A CN 2005800348432A CN 200580034843 A CN200580034843 A CN 200580034843A CN 101040035 B CN101040035 B CN 101040035B
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- CUXYLFPMQMFGPL-SUTYWZMXSA-N all-trans-octadeca-9,11,13-trienoic acid Chemical compound CCCC\C=C\C=C\C=C\CCCCCCCC(O)=O CUXYLFPMQMFGPL-SUTYWZMXSA-N 0.000 description 1
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- 125000001204 arachidyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
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- 239000003153 chemical reaction reagent Substances 0.000 description 1
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- MIMDHDXOBDPUQW-UHFFFAOYSA-N dioctyl decanedioate Chemical compound CCCCCCCCOC(=O)CCCCCCCCC(=O)OCCCCCCCC MIMDHDXOBDPUQW-UHFFFAOYSA-N 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
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- 238000001914 filtration Methods 0.000 description 1
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- 125000000018 nitroso group Chemical group N(=O)* 0.000 description 1
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- SECPZKHBENQXJG-FPLPWBNLSA-N palmitoleic acid Chemical compound CCCCCC\C=C/CCCCCCCC(O)=O SECPZKHBENQXJG-FPLPWBNLSA-N 0.000 description 1
- 239000000312 peanut oil Substances 0.000 description 1
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- 239000005077 polysulfide Substances 0.000 description 1
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- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- CIBMHJPPKCXONB-UHFFFAOYSA-N propane-2,2-diol Chemical compound CC(C)(O)O CIBMHJPPKCXONB-UHFFFAOYSA-N 0.000 description 1
- 125000004076 pyridyl group Chemical group 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000012958 reprocessing Methods 0.000 description 1
- 150000003333 secondary alcohols Chemical class 0.000 description 1
- 150000003336 secondary aromatic amines Chemical class 0.000 description 1
- 239000003079 shale oil Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 229910052712 strontium Inorganic materials 0.000 description 1
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 1
- RINCXYDBBGOEEQ-UHFFFAOYSA-N succinic anhydride Chemical class O=C1CCC(=O)O1 RINCXYDBBGOEEQ-UHFFFAOYSA-N 0.000 description 1
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- 150000003899 tartaric acid esters Chemical class 0.000 description 1
- JZALLXAUNPOCEU-UHFFFAOYSA-N tetradecylbenzene Chemical compound CCCCCCCCCCCCCCC1=CC=CC=C1 JZALLXAUNPOCEU-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M163/00—Lubricating compositions characterised by the additive being a mixture of a compound of unknown or incompletely defined constitution and a non-macromolecular compound, each of these compounds being essential
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M129/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen
- C10M129/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen having a carbon chain of less than 30 atoms
- C10M129/68—Esters
- C10M129/72—Esters of polycarboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M133/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing nitrogen
- C10M133/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing nitrogen having a carbon chain of less than 30 atoms
- C10M133/16—Amides; Imides
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/02—Hydroxy compounds
- C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
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Abstract
Description
实施例 | 比较例1 | 比较例2 | 实施例3 |
琥珀酰亚胺分散剂 | 5.1 | 5 | 5 |
二烷基二硫代磷酸锌 | 0.84 | 0.86 | 0.86 |
抗氧化剂 | 2.44 | 2.2 | 2.2 |
倾点下降剂 | 0 | 0 | 0.3 |
高碱性的磺酸钙清净剂 | 1.53 | 1.53 | 1.53 |
粘度指数改进剂 | 8.15 | 8.15 | 8 |
硼酸烷基酯 | 0 | 0.05 | 0.05 |
摩擦改进剂 | 0 | 0.1 | 0.1 |
甘油单油酸酯 | n.p | 0.4 | n.p |
油烯基胺酒石酰亚胺 | n.p | n.p | 0.5 |
Sequence VIB发动机 |
初始燃料经济性(合格≥1.5) | 1.5 | 1.8 | 1.9 |
耐久性(合格≥1.5) | 1.2 | 1.4 | 1.9 |
比较例30.1%P | 比较例40.05%P | 实施例50.05%P | 实施例60.05%P | 实施例70.05%P | 实施例80.05%P | 实施例90.05%P | 实施例100.05%P | |
其它组分 | ||||||||
[1,3]二氧戊环C12-C14烷基酒石酸酯 | 0.5 | |||||||
油烯基酒石酰亚胺 | 0.5 | |||||||
油烯基酒石酰亚胺 | 1 | |||||||
带支链的C13烷基酒石酸酯 | 1 | |||||||
十三烷基丙氧基胺酒石酰亚胺 | 1 | |||||||
硼酸化的十三烷基丙氧基胺酒石酰 | 1 |
亚胺 | ||||||||
测试 | ||||||||
1.4Ball LowPS测试 | ||||||||
平均磨痕直径(mm) | 0.59 | 0.61,0.77 | 0.51 | 0.7 | n.r. | n.r. | 0.45 | 0.41 |
2.HFRR1%CHP测试 | ||||||||
磨损痕迹直径(μm) | 161,185 | 285,295,435 | 236 | 251 | 260 | 286 | 297 | 183 |
膜厚(%) | 94,83 | 1,1,23 | 86 | 66 | 58 | 56 | 97 | 50 |
3.Cameron-Plint高温往复磨损测试 | ||||||||
磨损痕迹直径(μm) | 339 | 661 | n.r. | n.r. | 375 | 352 | n.r. | n.r. |
膜厚(%) | 100 | 62 | n.r. | n.r. | 100 | 99 | n.r. | n.r. |
Claims (22)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
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US10/963,082 | 2004-10-12 | ||
US10/963,082 US7651987B2 (en) | 2004-10-12 | 2004-10-12 | Tartaric acid derivatives as fuel economy improvers and antiwear agents in crankcase oils and preparation thereof |
PCT/US2005/036569 WO2006044411A1 (en) | 2004-10-12 | 2005-10-11 | Tartaric acid derivatives as fuel economy improvers and antiwear agents in crankcase oils and preparation thereof |
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CN2012100218464A Division CN102604697A (zh) | 2004-10-12 | 2005-10-11 | 在曲轴箱油中作为燃料经济性改进剂和抗磨剂的酒石酸衍生物及其制备 |
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CN101040035A CN101040035A (zh) | 2007-09-19 |
CN101040035B true CN101040035B (zh) | 2012-03-28 |
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CN2012100218464A Pending CN102604697A (zh) | 2004-10-12 | 2005-10-11 | 在曲轴箱油中作为燃料经济性改进剂和抗磨剂的酒石酸衍生物及其制备 |
CN2005800348432A Expired - Fee Related CN101040035B (zh) | 2004-10-12 | 2005-10-11 | 在曲轴箱油中作为燃料经济性改进剂和抗磨剂的酒石酸衍生物及其制备 |
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CN2012100218464A Pending CN102604697A (zh) | 2004-10-12 | 2005-10-11 | 在曲轴箱油中作为燃料经济性改进剂和抗磨剂的酒石酸衍生物及其制备 |
Country Status (6)
Country | Link |
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US (3) | US7651987B2 (zh) |
EP (1) | EP1802730B1 (zh) |
JP (3) | JP5178197B2 (zh) |
CN (2) | CN102604697A (zh) |
CA (1) | CA2582618A1 (zh) |
WO (1) | WO2006044411A1 (zh) |
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CN1671827A (zh) * | 2002-06-28 | 2005-09-21 | 新日本石油株式会社 | 润滑油组合物 |
Non-Patent Citations (1)
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US20060079413A1 (en) | 2006-04-13 |
CN101040035A (zh) | 2007-09-19 |
JP2012087317A (ja) | 2012-05-10 |
CN102604697A (zh) | 2012-07-25 |
CA2582618A1 (en) | 2006-04-27 |
WO2006044411A1 (en) | 2006-04-27 |
US7651987B2 (en) | 2010-01-26 |
JP2012087318A (ja) | 2012-05-10 |
JP2008516055A (ja) | 2008-05-15 |
JP5178197B2 (ja) | 2013-04-10 |
EP1802730B1 (en) | 2019-08-07 |
US20100081592A1 (en) | 2010-04-01 |
US20110131868A1 (en) | 2011-06-09 |
US8133290B2 (en) | 2012-03-13 |
EP1802730A1 (en) | 2007-07-04 |
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