TWI565666B - 石英玻璃大型管之製造方法 - Google Patents
石英玻璃大型管之製造方法 Download PDFInfo
- Publication number
- TWI565666B TWI565666B TW103121820A TW103121820A TWI565666B TW I565666 B TWI565666 B TW I565666B TW 103121820 A TW103121820 A TW 103121820A TW 103121820 A TW103121820 A TW 103121820A TW I565666 B TWI565666 B TW I565666B
- Authority
- TW
- Taiwan
- Prior art keywords
- quartz glass
- semi
- cylinder
- tube
- less
- Prior art date
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims description 94
- 238000004519 manufacturing process Methods 0.000 title claims description 15
- 238000000034 method Methods 0.000 claims description 40
- 238000000465 moulding Methods 0.000 claims description 40
- 238000007493 shaping process Methods 0.000 claims description 36
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 33
- 239000012535 impurity Substances 0.000 claims description 10
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 9
- 229910052801 chlorine Inorganic materials 0.000 claims description 9
- 239000000460 chlorine Substances 0.000 claims description 9
- 238000001125 extrusion Methods 0.000 claims description 7
- 238000007664 blowing Methods 0.000 claims description 6
- 229910052782 aluminium Inorganic materials 0.000 claims description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 3
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- 238000003786 synthesis reaction Methods 0.000 claims description 3
- 229910052783 alkali metal Inorganic materials 0.000 claims description 2
- 150000001340 alkali metals Chemical class 0.000 claims description 2
- 238000005485 electric heating Methods 0.000 claims description 2
- 150000002736 metal compounds Chemical class 0.000 claims description 2
- 238000003825 pressing Methods 0.000 claims 1
- 238000002485 combustion reaction Methods 0.000 description 10
- 239000010883 coal ash Substances 0.000 description 9
- 238000009826 distribution Methods 0.000 description 7
- 229910052736 halogen Inorganic materials 0.000 description 6
- 150000002367 halogens Chemical class 0.000 description 6
- 230000008569 process Effects 0.000 description 6
- 239000000047 product Substances 0.000 description 5
- 229910004298 SiO 2 Inorganic materials 0.000 description 4
- 230000008859 change Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000011521 glass Substances 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 238000012423 maintenance Methods 0.000 description 4
- 238000005259 measurement Methods 0.000 description 4
- 239000011265 semifinished product Substances 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 3
- 230000007547 defect Effects 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 239000010439 graphite Substances 0.000 description 3
- 229910002804 graphite Inorganic materials 0.000 description 3
- 230000003287 optical effect Effects 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 230000001105 regulatory effect Effects 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 208000005156 Dehydration Diseases 0.000 description 2
- 229910003902 SiCl 4 Inorganic materials 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 210000000078 claw Anatomy 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 239000002274 desiccant Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 2
- 239000010931 gold Substances 0.000 description 2
- 229910052737 gold Inorganic materials 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 229910044991 metal oxide Inorganic materials 0.000 description 2
- 150000004706 metal oxides Chemical class 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000011017 operating method Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000010453 quartz Substances 0.000 description 2
- 239000004071 soot Substances 0.000 description 2
- 101710134784 Agnoprotein Proteins 0.000 description 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000012937 correction Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000006298 dechlorination reaction Methods 0.000 description 1
- 238000005137 deposition process Methods 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 210000001061 forehead Anatomy 0.000 description 1
- 239000005350 fused silica glass Substances 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 239000010455 vermiculite Substances 0.000 description 1
- 229910052902 vermiculite Inorganic materials 0.000 description 1
- 235000019354 vermiculite Nutrition 0.000 description 1
- 238000004017 vitrification Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B23/00—Re-forming shaped glass
- C03B23/04—Re-forming tubes or rods
- C03B23/053—Re-forming tubes or rods by centrifuging
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/06—Glass compositions containing silica with more than 90% silica by weight, e.g. quartz
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/14—Other methods of shaping glass by gas- or vapour- phase reaction processes
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B23/00—Re-forming shaped glass
- C03B23/04—Re-forming tubes or rods
- C03B23/043—Heating devices specially adapted for re-forming tubes or rods in general, e.g. burners
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B23/00—Re-forming shaped glass
- C03B23/04—Re-forming tubes or rods
- C03B23/045—Tools or apparatus specially adapted for re-forming tubes or rods in general, e.g. glass lathes, chucks
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B23/00—Re-forming shaped glass
- C03B23/04—Re-forming tubes or rods
- C03B23/07—Re-forming tubes or rods by blowing, e.g. for making electric bulbs
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B23/00—Re-forming shaped glass
- C03B23/04—Re-forming tubes or rods
- C03B23/08—Re-forming tubes or rods to exact dimensions, e.g. calibrating
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B2201/00—Type of glass produced
- C03B2201/02—Pure silica glass, e.g. pure fused quartz
- C03B2201/03—Impurity concentration specified
- C03B2201/04—Hydroxyl ion (OH)
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2203/00—Production processes
- C03C2203/40—Gas-phase processes
- C03C2203/42—Gas-phase processes using silicon halides as starting materials
- C03C2203/44—Gas-phase processes using silicon halides as starting materials chlorine containing
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Re-Forming, After-Treatment, Cutting And Transporting Of Glass Products (AREA)
- Glass Melting And Manufacturing (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102013107435.9A DE102013107435B4 (de) | 2013-07-12 | 2013-07-12 | Verfahren zur Herstellung eines Quarzglas-Großrohres |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| TW201504166A TW201504166A (zh) | 2015-02-01 |
| TWI565666B true TWI565666B (zh) | 2017-01-11 |
Family
ID=51162803
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW103121820A TWI565666B (zh) | 2013-07-12 | 2014-06-25 | 石英玻璃大型管之製造方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US20160168005A1 (ja) |
| EP (1) | EP3019453A1 (ja) |
| JP (1) | JP6478990B2 (ja) |
| KR (1) | KR102117985B1 (ja) |
| CN (1) | CN105358494B (ja) |
| DE (1) | DE102013107435B4 (ja) |
| SG (1) | SG11201600207TA (ja) |
| TW (1) | TWI565666B (ja) |
| WO (1) | WO2015004103A1 (ja) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3034477B1 (de) * | 2014-12-19 | 2019-02-06 | Heraeus Quarzglas GmbH & Co. KG | Verfahren zur herstellung eines rohres aus glas |
| DE102015002456A1 (de) | 2015-02-23 | 2016-08-25 | Schott Schweiz Ag | Vorrichtung und Verfahren zur Formung von Glaskörpern |
| US10550027B2 (en) * | 2015-04-24 | 2020-02-04 | Nipro Corporation | Method for producing medical glass container in which occurrence of cracking is reduced |
| WO2016171197A1 (ja) * | 2015-04-24 | 2016-10-27 | ニプロ株式会社 | 医療用ガラス容器の製造方法及び回転装置を備えたファイアブラスト装置 |
| EP3088370B1 (de) * | 2015-04-28 | 2018-09-26 | Heraeus Quarzglas GmbH & Co. KG | Verfahren und vorrichtung zur herstellung eines rohres aus glas |
| DE102015117215B4 (de) | 2015-10-08 | 2019-03-14 | Gerresheimer Bünde Gmbh | Vorrichtung und Verfahren zur Herstellung eines medizinischen Glasbehälters |
| US11299417B2 (en) | 2015-12-18 | 2022-04-12 | Heraeus Quarzglas Gmbh & Co. Kg | Preparation of a quartz glass body in a melting crucible of refractory metal |
| CN108698888A (zh) | 2015-12-18 | 2018-10-23 | 贺利氏石英玻璃有限两合公司 | 在石英玻璃制备中作为中间物的经碳掺杂的二氧化硅颗粒的制备 |
| WO2017103160A1 (de) | 2015-12-18 | 2017-06-22 | Heraeus Quarzglas Gmbh & Co. Kg | Herstellung von quarzglaskörpern aus siliziumdioxidgranulat |
| TWI808933B (zh) | 2015-12-18 | 2023-07-21 | 德商何瑞斯廓格拉斯公司 | 石英玻璃體、二氧化矽顆粒、光導、施照體、及成型體及其製備方法 |
| WO2017103124A2 (de) | 2015-12-18 | 2017-06-22 | Heraeus Quarzglas Gmbh & Co. Kg | Erhöhen des siliziumgehalts bei der herstellung von quarzglas |
| WO2017103123A2 (de) | 2015-12-18 | 2017-06-22 | Heraeus Quarzglas Gmbh & Co. Kg | Herstellung von quarzglaskörpern mit taupunktkontrolle im schmelzofen |
| TWI788278B (zh) | 2015-12-18 | 2023-01-01 | 德商何瑞斯廓格拉斯公司 | 由均質石英玻璃製得之玻璃纖維及預成型品 |
| JP6881777B2 (ja) | 2015-12-18 | 2021-06-02 | ヘレウス クワルツグラス ゲーエムベーハー ウント コンパニー カーゲー | 合成石英ガラス粒の調製 |
| TWI733723B (zh) | 2015-12-18 | 2021-07-21 | 德商何瑞斯廓格拉斯公司 | 不透明石英玻璃體的製備 |
| US10730780B2 (en) | 2015-12-18 | 2020-08-04 | Heraeus Quarzglas Gmbh & Co. Kg | Preparation of a quartz glass body in a multi-chamber oven |
| DE102017207572A1 (de) * | 2017-05-05 | 2018-11-08 | Schott Ag | Verfahren zur Herstellung eines Glasrohres mit einem von einer Kreisform abweichenden Querschnitt durch Umformen |
| EP3421434B1 (de) * | 2017-06-30 | 2020-06-10 | Heraeus Quarzglas GmbH & Co. KG | Verfahren zur erzeugung einer stoffschlüssigen fügeverbindung zwischen bauteilen aus quarzglas und dafür geeigneter heizbrenner |
| CN108565064B (zh) * | 2017-12-30 | 2020-02-07 | 西北有色金属研究院 | 一种MgB2超导线材的快速热处理方法 |
| EP3656746B1 (en) * | 2018-11-23 | 2024-06-05 | Heraeus Conamic UK Limited | Method and apparatus for cutting a hollow quartz glass ingot |
| DE102018133140A1 (de) * | 2018-12-20 | 2020-06-25 | Endress+Hauser Conducta Gmbh+Co. Kg | Verfahren zur Ausbildung eines Bauteils eines potentiometrischen Sensors zur pH-Bestimmung und potentiometrischer Sensor |
| CN111039549A (zh) * | 2019-12-11 | 2020-04-21 | 中国建筑材料科学研究总院有限公司 | 石英玻璃碇熔制装置及系统 |
| CN111039548A (zh) * | 2019-12-11 | 2020-04-21 | 中国建筑材料科学研究总院有限公司 | 石英玻璃碇等径度控制方法 |
| EP4067315A1 (de) * | 2021-03-29 | 2022-10-05 | Heraeus Quarzglas GmbH & Co. KG | Rohr aus quarzglas und verfahren zur herstellung desselben |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5364433A (en) * | 1991-06-29 | 1994-11-15 | Shin-Etsu Quartz Products Company Limited | Optical member of synthetic quartz glass for excimer lasers and method for producing same |
| JP2009149506A (ja) * | 2007-12-18 | 2009-07-09 | Shinetsu Quartz Prod Co Ltd | 石英ガラス管の製造方法及びこの方法を実施するための装置 |
| US20100260949A1 (en) * | 2003-03-21 | 2010-10-14 | Heraeus Quarzglas Gmbh & Co. Kg | Synthetic silica glass tube for the production of a preform |
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| FR1267805A (fr) * | 1960-04-15 | 1961-07-28 | Commissariat Energie Atomique | Procédé de calibrage du diamètre intérieur de tubes de silice vitreuse par déformation locale en zone visqueuse |
| US3620707A (en) * | 1969-09-15 | 1971-11-16 | Research Corp | Glass-tube reforming apparatus |
| US3679385A (en) * | 1970-09-18 | 1972-07-25 | Gen Electric | Manufacture of interior coated bulbs for high temperature glass lamps |
| US3715197A (en) * | 1970-12-10 | 1973-02-06 | Bendix Corp | Method and preform for reshaping glass tubing |
| DE2121611B2 (de) * | 1971-05-03 | 1973-03-15 | Siemens AG, 1000 Berlin u. 8000 München | Kreuzschienenverteiler fuer videosignale |
| US4178165A (en) * | 1976-07-09 | 1979-12-11 | Lothar Jung | Apparatus for manufacturing hollow and solid ingots |
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| CN102887624B (zh) * | 2012-03-23 | 2015-08-26 | 连云港市东海县宏伟石英制品有限公司 | 一种超大口径石英玻璃管的制造方法 |
-
2013
- 2013-07-12 DE DE102013107435.9A patent/DE102013107435B4/de active Active
-
2014
- 2014-06-25 TW TW103121820A patent/TWI565666B/zh active
- 2014-07-08 US US14/904,308 patent/US20160168005A1/en not_active Abandoned
- 2014-07-08 JP JP2016524788A patent/JP6478990B2/ja active Active
- 2014-07-08 EP EP14736800.5A patent/EP3019453A1/de not_active Withdrawn
- 2014-07-08 WO PCT/EP2014/064541 patent/WO2015004103A1/de active Application Filing
- 2014-07-08 KR KR1020167002808A patent/KR102117985B1/ko active IP Right Grant
- 2014-07-08 SG SG11201600207TA patent/SG11201600207TA/en unknown
- 2014-07-08 CN CN201480039724.5A patent/CN105358494B/zh active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5364433A (en) * | 1991-06-29 | 1994-11-15 | Shin-Etsu Quartz Products Company Limited | Optical member of synthetic quartz glass for excimer lasers and method for producing same |
| US20100260949A1 (en) * | 2003-03-21 | 2010-10-14 | Heraeus Quarzglas Gmbh & Co. Kg | Synthetic silica glass tube for the production of a preform |
| JP2009149506A (ja) * | 2007-12-18 | 2009-07-09 | Shinetsu Quartz Prod Co Ltd | 石英ガラス管の製造方法及びこの方法を実施するための装置 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE102013107435B4 (de) | 2015-01-29 |
| CN105358494B (zh) | 2019-03-08 |
| TW201504166A (zh) | 2015-02-01 |
| WO2015004103A1 (de) | 2015-01-15 |
| KR20160030533A (ko) | 2016-03-18 |
| JP6478990B2 (ja) | 2019-03-06 |
| JP2016528142A (ja) | 2016-09-15 |
| DE102013107435A1 (de) | 2015-01-15 |
| US20160168005A1 (en) | 2016-06-16 |
| CN105358494A (zh) | 2016-02-24 |
| KR102117985B1 (ko) | 2020-06-03 |
| EP3019453A1 (de) | 2016-05-18 |
| SG11201600207TA (en) | 2016-02-26 |
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