RU2386619C2 - Способ получения 5-гидрокси-4-тиометилпиразольного соединения - Google Patents
Способ получения 5-гидрокси-4-тиометилпиразольного соединения Download PDFInfo
- Publication number
- RU2386619C2 RU2386619C2 RU2006138241/04A RU2006138241A RU2386619C2 RU 2386619 C2 RU2386619 C2 RU 2386619C2 RU 2006138241/04 A RU2006138241/04 A RU 2006138241/04A RU 2006138241 A RU2006138241 A RU 2006138241A RU 2386619 C2 RU2386619 C2 RU 2386619C2
- Authority
- RU
- Russia
- Prior art keywords
- group
- hydroxy
- compound
- mmol
- reaction
- Prior art date
Links
- 0 Cc1n[n](*)c(O)c1CS Chemical compound Cc1n[n](*)c(O)c1CS 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/18—One oxygen or sulfur atom
- C07D231/20—One oxygen atom attached in position 3 or 5
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/28—Two oxygen or sulfur atoms
- C07D231/30—Two oxygen or sulfur atoms attached in positions 3 and 5
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
- C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
- C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plural Heterocyclic Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2004102963A JP4621939B2 (ja) | 2004-03-31 | 2004-03-31 | ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法 |
| JP2004-102963 | 2004-03-31 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2006138241A RU2006138241A (ru) | 2008-05-10 |
| RU2386619C2 true RU2386619C2 (ru) | 2010-04-20 |
Family
ID=35063690
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2006138241/04A RU2386619C2 (ru) | 2004-03-31 | 2005-03-31 | Способ получения 5-гидрокси-4-тиометилпиразольного соединения |
Country Status (19)
| Country | Link |
|---|---|
| US (1) | US7488831B2 (https=) |
| EP (1) | EP1767528B1 (https=) |
| JP (1) | JP4621939B2 (https=) |
| KR (1) | KR101205731B1 (https=) |
| CN (1) | CN1938278B (https=) |
| AU (1) | AU2005228017B2 (https=) |
| BR (1) | BRPI0509353B1 (https=) |
| CA (1) | CA2560936C (https=) |
| CR (1) | CR8640A (https=) |
| ES (1) | ES2508765T3 (https=) |
| IL (1) | IL178233A (https=) |
| IN (1) | IN2006DE05581A (https=) |
| MX (1) | MX280092B (https=) |
| NZ (1) | NZ550143A (https=) |
| PL (1) | PL1767528T3 (https=) |
| RU (1) | RU2386619C2 (https=) |
| TW (1) | TWI357899B (https=) |
| UA (1) | UA83910C2 (https=) |
| WO (1) | WO2005095352A1 (https=) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2333977T3 (es) | 2004-10-05 | 2010-03-03 | Syngenta Limited | Derivados de isoxazolina y su uso como herbicidas. |
| MX274842B (es) * | 2004-12-20 | 2010-03-30 | Ihara Chemical Ind Co | Procedimiento para la produccion de sales de (4,5-dihidroisoxazol- 3-il)tiocarboxamidina. |
| JP2007031342A (ja) * | 2005-07-27 | 2007-02-08 | Ihara Chem Ind Co Ltd | ５−ヒドロキシ−１−アルキルピラゾール誘導体の製造方法 |
| CA2642308C (en) * | 2006-02-14 | 2013-12-17 | Ihara Chemical Industry Co., Ltd. | Process for production of 5-alkoxy-4-hydroxymethylpyrazole compound |
| TWI443090B (zh) * | 2007-05-25 | 2014-07-01 | Abbvie Deutschland | 作為代謝性麩胺酸受體２（ｍｇｌｕ２ 受體）之正向調節劑之雜環化合物 |
| GB0916267D0 (en) | 2009-09-16 | 2009-10-28 | Syngenta Ltd | Herbicidal compounds |
| US20120238760A1 (en) | 2009-11-26 | 2012-09-20 | Basf Se | Method for Producing 5,5-Disubstituted 2-Isoxazolines |
| ES2466322T3 (es) * | 2009-11-26 | 2014-06-10 | Basf Se | Procedimiento para la preparación de sales de 4,5-dihidroisoxazol-3-tiocarboxamidina 5,5-disustituida |
| DK2571854T3 (en) * | 2010-05-20 | 2015-02-09 | Bayer Ip Gmbh | PROCESS FOR THE PREPARATION OF 1-alkyl-3-difluoromethyl-5-hydroxypyrazoles |
| CA2843415C (en) | 2011-07-29 | 2019-12-31 | University Of Saskatchewan | Polymer-based resonator antennas |
| CN103387541B (zh) * | 2012-05-10 | 2016-02-10 | 中国中化股份有限公司 | 一种取代吡唑醚类化合物的制备方法 |
| JP6400247B1 (ja) | 2015-11-16 | 2018-10-03 | ロンザ・リミテッド | １−メチル−３−（トリフルオロメチル）−１ｈ−ピラゾール−５−オールの調製方法 |
| TW201835036A (zh) | 2017-02-27 | 2018-10-01 | 瑞士商隆薩有限公司 | 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法 |
| JP6664036B2 (ja) | 2017-12-27 | 2020-03-13 | クミアイ化学工業株式会社 | チオカルボキサミジン塩化合物の製造方法 |
| CN112135814B (zh) * | 2018-05-31 | 2021-09-28 | 组合化学工业株式会社 | 含氟吡唑衍生物的制造方法及其中间体 |
| EP4003964B1 (en) | 2019-07-30 | 2024-09-18 | Adama Agan Ltd. | Process and intermediates for the preparation of pyroxasulfone |
| KR102523028B1 (ko) | 2019-10-31 | 2023-04-17 | 구미아이 가가쿠 고교 가부시키가이샤 | 제초제 및 그 중간체의 제조방법 |
| IL296145A (en) | 2020-03-05 | 2022-11-01 | Adama Agan Ltd | A process for the preparation of pyroxasulfone and intermediates obtained in this process |
| CN111574511A (zh) * | 2020-06-28 | 2020-08-25 | 安徽久易农业股份有限公司 | 一种砜吡草唑的合成方法及其应用 |
| EP4177252A3 (en) | 2020-07-10 | 2023-08-09 | Adama Agan Ltd. | Process and intermediates for the preparation of pyroxasulfone, fenoxasulfone and various sulfone analogs of 5,5-dimethyl-4h-1,2-oxazole |
| CN112110912B (zh) * | 2020-07-31 | 2022-07-05 | 绍兴贝斯美化工股份有限公司 | 一种合成硫醚类中间体的方法 |
| WO2023074828A1 (ja) | 2021-10-29 | 2023-05-04 | クミアイ化学工業株式会社 | ジスルフィド化合物、ポリスルフィド化合物及びその用途 |
| AR127776A1 (es) | 2021-11-28 | 2024-02-28 | Adama Agan Ltd | Composiciones de concentrado en suspensión de alta carga |
| CN114716428B (zh) * | 2022-05-06 | 2024-02-06 | 山东潍坊润丰化工股份有限公司 | 制备砜吡草唑中间体的方法 |
| CN115850178B (zh) * | 2022-12-28 | 2025-04-04 | 宁夏格瑞精细化工有限公司 | 一种1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的制备方法 |
| CN117417333B (zh) * | 2023-10-07 | 2026-02-17 | 安徽久易农业股份有限公司 | 一种砜吡草唑的合成工艺 |
| CN120590326B (zh) * | 2025-06-05 | 2025-12-23 | 济南万兴达化工有限公司 | 一种1-甲基-3-（三氟甲基）-1h-吡唑-5-醇的制备方法 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2037488C1 (ru) * | 1989-03-02 | 1995-06-19 | Рон-Пуленк Агрошими | Производные 3-циано-5-алкокси-1-арилпиразолов и композиция на их основе |
| WO2001064651A1 (en) * | 2000-03-02 | 2001-09-07 | Bayer Cropscience S.A. | 3-thiomethylpyrazoles as pesticides |
| EP1364946A1 (en) * | 2001-02-08 | 2003-11-26 | Kumiai Chemical Industry Co., Ltd. | Isoxazoline derivative and herbicide comprising the same as active ingredient |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003000686A1 (en) * | 2001-06-21 | 2003-01-03 | Kumiai Chemical Industry Co., Ltd. | Isoxazoline derivatives and herbicides |
| AU2003252447B2 (en) * | 2002-08-01 | 2008-06-05 | Kumiai Chemical Industry Co., Ltd. | Pyrazole derivatives and process for the production thereof |
| UA78071C2 (en) * | 2002-08-07 | 2007-02-15 | Kumiai Chemical Industry Co | Herbicidal composition |
-
2004
- 2004-03-31 JP JP2004102963A patent/JP4621939B2/ja not_active Expired - Lifetime
-
2005
- 2005-03-31 CA CA2560936A patent/CA2560936C/en not_active Expired - Lifetime
- 2005-03-31 UA UAA200611331A patent/UA83910C2/ru unknown
- 2005-03-31 AU AU2005228017A patent/AU2005228017B2/en not_active Expired
- 2005-03-31 MX MXPA06011130 patent/MX280092B/es active IP Right Grant
- 2005-03-31 TW TW094110223A patent/TWI357899B/zh not_active IP Right Cessation
- 2005-03-31 ES ES05728918.3T patent/ES2508765T3/es not_active Expired - Lifetime
- 2005-03-31 KR KR1020067019480A patent/KR101205731B1/ko not_active Expired - Lifetime
- 2005-03-31 US US10/594,710 patent/US7488831B2/en not_active Expired - Lifetime
- 2005-03-31 EP EP05728918.3A patent/EP1767528B1/en not_active Expired - Lifetime
- 2005-03-31 WO PCT/JP2005/006806 patent/WO2005095352A1/ja not_active Ceased
- 2005-03-31 RU RU2006138241/04A patent/RU2386619C2/ru active
- 2005-03-31 CN CN2005800106359A patent/CN1938278B/zh not_active Expired - Lifetime
- 2005-03-31 PL PL05728918T patent/PL1767528T3/pl unknown
- 2005-03-31 NZ NZ550143A patent/NZ550143A/en not_active IP Right Cessation
- 2005-03-31 BR BRPI0509353A patent/BRPI0509353B1/pt active IP Right Grant
-
2006
- 2006-09-20 CR CR8640A patent/CR8640A/es unknown
- 2006-09-21 IL IL178233A patent/IL178233A/en active IP Right Grant
- 2006-09-25 IN IN5581DE2006 patent/IN2006DE05581A/en unknown
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2037488C1 (ru) * | 1989-03-02 | 1995-06-19 | Рон-Пуленк Агрошими | Производные 3-циано-5-алкокси-1-арилпиразолов и композиция на их основе |
| WO2001064651A1 (en) * | 2000-03-02 | 2001-09-07 | Bayer Cropscience S.A. | 3-thiomethylpyrazoles as pesticides |
| EP1364946A1 (en) * | 2001-02-08 | 2003-11-26 | Kumiai Chemical Industry Co., Ltd. | Isoxazoline derivative and herbicide comprising the same as active ingredient |
Also Published As
| Publication number | Publication date |
|---|---|
| EP1767528A1 (en) | 2007-03-28 |
| EP1767528B1 (en) | 2014-09-17 |
| ES2508765T3 (es) | 2014-10-16 |
| JP4621939B2 (ja) | 2011-02-02 |
| CA2560936C (en) | 2013-01-08 |
| MXPA06011130A (es) | 2007-01-25 |
| TW200536832A (en) | 2005-11-16 |
| US20070185334A1 (en) | 2007-08-09 |
| CR8640A (es) | 2007-08-28 |
| BRPI0509353A (pt) | 2007-09-11 |
| IL178233A (en) | 2014-02-27 |
| AU2005228017A1 (en) | 2005-10-13 |
| BRPI0509353B1 (pt) | 2019-01-02 |
| CN1938278B (zh) | 2012-12-12 |
| NZ550143A (en) | 2010-04-30 |
| UA83910C2 (ru) | 2008-08-26 |
| PL1767528T3 (pl) | 2015-03-31 |
| CN1938278A (zh) | 2007-03-28 |
| KR20070003964A (ko) | 2007-01-05 |
| IN2006DE05581A (https=) | 2007-08-31 |
| AU2005228017B2 (en) | 2010-09-30 |
| RU2006138241A (ru) | 2008-05-10 |
| CA2560936A1 (en) | 2005-10-13 |
| IL178233A0 (en) | 2006-12-31 |
| KR101205731B1 (ko) | 2012-11-28 |
| BRPI0509353A8 (pt) | 2017-09-19 |
| EP1767528A4 (en) | 2010-04-21 |
| WO2005095352A1 (ja) | 2005-10-13 |
| US7488831B2 (en) | 2009-02-10 |
| TWI357899B (en) | 2012-02-11 |
| MX280092B (es) | 2010-10-18 |
| JP2005289824A (ja) | 2005-10-20 |
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