KR101205731B1 - 5-히드록시-4-티오메틸피라졸 화합물의 제조 방법 - Google Patents

5-히드록시-4-티오메틸피라졸 화합물의 제조 방법 Download PDF

Info

Publication number
KR101205731B1
KR101205731B1 KR1020067019480A KR20067019480A KR101205731B1 KR 101205731 B1 KR101205731 B1 KR 101205731B1 KR 1020067019480 A KR1020067019480 A KR 1020067019480A KR 20067019480 A KR20067019480 A KR 20067019480A KR 101205731 B1 KR101205731 B1 KR 101205731B1
Authority
KR
South Korea
Prior art keywords
group
hydroxy
represented
general formula
groups
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
KR1020067019480A
Other languages
English (en)
Korean (ko)
Other versions
KR20070003964A (ko
Inventor
유키오 우치다
Original Assignee
이하라케미칼 고교가부시키가이샤
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=35063690&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=KR101205731(B1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by 이하라케미칼 고교가부시키가이샤 filed Critical 이하라케미칼 고교가부시키가이샤
Publication of KR20070003964A publication Critical patent/KR20070003964A/ko
Application granted granted Critical
Publication of KR101205731B1 publication Critical patent/KR101205731B1/ko
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/28—Two oxygen or sulfur atoms
    • C07D231/30—Two oxygen or sulfur atoms attached in positions 3 and 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020067019480A 2004-03-31 2005-03-31 5-히드록시-4-티오메틸피라졸 화합물의 제조 방법 Expired - Lifetime KR101205731B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2004102963A JP4621939B2 (ja) 2004-03-31 2004-03-31 ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法
JPJP-P-2004-00102963 2004-03-31
PCT/JP2005/006806 WO2005095352A1 (ja) 2004-03-31 2005-03-31 ５－ヒドロキシ－４－チオメチルピラゾール化合物の製造方法

Publications (2)

Publication Number Publication Date
KR20070003964A KR20070003964A (ko) 2007-01-05
KR101205731B1 true KR101205731B1 (ko) 2012-11-28

Family

ID=35063690

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020067019480A Expired - Lifetime KR101205731B1 (ko) 2004-03-31 2005-03-31 5-히드록시-4-티오메틸피라졸 화합물의 제조 방법

Country Status (19)

Country Link
US (1) US7488831B2 (https=)
EP (1) EP1767528B1 (https=)
JP (1) JP4621939B2 (https=)
KR (1) KR101205731B1 (https=)
CN (1) CN1938278B (https=)
AU (1) AU2005228017B2 (https=)
BR (1) BRPI0509353B1 (https=)
CA (1) CA2560936C (https=)
CR (1) CR8640A (https=)
ES (1) ES2508765T3 (https=)
IL (1) IL178233A (https=)
IN (1) IN2006DE05581A (https=)
MX (1) MX280092B (https=)
NZ (1) NZ550143A (https=)
PL (1) PL1767528T3 (https=)
RU (1) RU2386619C2 (https=)
TW (1) TWI357899B (https=)
UA (1) UA83910C2 (https=)
WO (1) WO2005095352A1 (https=)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2333977T3 (es) 2004-10-05 2010-03-03 Syngenta Limited Derivados de isoxazolina y su uso como herbicidas.
MX274842B (es) * 2004-12-20 2010-03-30 Ihara Chemical Ind Co Procedimiento para la produccion de sales de (4,5-dihidroisoxazol- 3-il)tiocarboxamidina.
JP2007031342A (ja) * 2005-07-27 2007-02-08 Ihara Chem Ind Co Ltd ５−ヒドロキシ−１−アルキルピラゾール誘導体の製造方法
CA2642308C (en) * 2006-02-14 2013-12-17 Ihara Chemical Industry Co., Ltd. Process for production of 5-alkoxy-4-hydroxymethylpyrazole compound
TWI443090B (zh) * 2007-05-25 2014-07-01 Abbvie Deutschland 作為代謝性麩胺酸受體２（ｍｇｌｕ２ 受體）之正向調節劑之雜環化合物
GB0916267D0 (en) 2009-09-16 2009-10-28 Syngenta Ltd Herbicidal compounds
US20120238760A1 (en) 2009-11-26 2012-09-20 Basf Se Method for Producing 5,5-Disubstituted 2-Isoxazolines
ES2466322T3 (es) * 2009-11-26 2014-06-10 Basf Se Procedimiento para la preparación de sales de 4,5-dihidroisoxazol-3-tiocarboxamidina 5,5-disustituida
DK2571854T3 (en) * 2010-05-20 2015-02-09 Bayer Ip Gmbh PROCESS FOR THE PREPARATION OF 1-alkyl-3-difluoromethyl-5-hydroxypyrazoles
CA2843415C (en) 2011-07-29 2019-12-31 University Of Saskatchewan Polymer-based resonator antennas
CN103387541B (zh) * 2012-05-10 2016-02-10 中国中化股份有限公司 一种取代吡唑醚类化合物的制备方法
JP6400247B1 (ja) 2015-11-16 2018-10-03 ロンザ・リミテッド １−メチル−３−（トリフルオロメチル）−１ｈ−ピラゾール−５−オールの調製方法
TW201835036A (zh) 2017-02-27 2018-10-01 瑞士商隆薩有限公司 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法
JP6664036B2 (ja) 2017-12-27 2020-03-13 クミアイ化学工業株式会社 チオカルボキサミジン塩化合物の製造方法
CN112135814B (zh) * 2018-05-31 2021-09-28 组合化学工业株式会社 含氟吡唑衍生物的制造方法及其中间体
EP4003964B1 (en) 2019-07-30 2024-09-18 Adama Agan Ltd. Process and intermediates for the preparation of pyroxasulfone
KR102523028B1 (ko) 2019-10-31 2023-04-17 구미아이 가가쿠 고교 가부시키가이샤 제초제 및 그 중간체의 제조방법
IL296145A (en) 2020-03-05 2022-11-01 Adama Agan Ltd A process for the preparation of pyroxasulfone and intermediates obtained in this process
CN111574511A (zh) * 2020-06-28 2020-08-25 安徽久易农业股份有限公司 一种砜吡草唑的合成方法及其应用
EP4177252A3 (en) 2020-07-10 2023-08-09 Adama Agan Ltd. Process and intermediates for the preparation of pyroxasulfone, fenoxasulfone and various sulfone analogs of 5,5-dimethyl-4h-1,2-oxazole
CN112110912B (zh) * 2020-07-31 2022-07-05 绍兴贝斯美化工股份有限公司 一种合成硫醚类中间体的方法
WO2023074828A1 (ja) 2021-10-29 2023-05-04 クミアイ化学工業株式会社 ジスルフィド化合物、ポリスルフィド化合物及びその用途
AR127776A1 (es) 2021-11-28 2024-02-28 Adama Agan Ltd Composiciones de concentrado en suspensión de alta carga
CN114716428B (zh) * 2022-05-06 2024-02-06 山东潍坊润丰化工股份有限公司 制备砜吡草唑中间体的方法
CN115850178B (zh) * 2022-12-28 2025-04-04 宁夏格瑞精细化工有限公司 一种1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的制备方法
CN117417333B (zh) * 2023-10-07 2026-02-17 安徽久易农业股份有限公司 一种砜吡草唑的合成工艺
CN120590326B (zh) * 2025-06-05 2025-12-23 济南万兴达化工有限公司 一种1-甲基-3-（三氟甲基）-1h-吡唑-5-醇的制备方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004013106A1 (ja) 2002-08-01 2004-02-12 Ihara Chemical Industry Co., Ltd. ピラゾール誘導体及びその製造方法
WO2004014138A1 (ja) 2002-08-07 2004-02-19 Kumiai Chemical Industry Co., Ltd. 除草剤組成物

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4918085A (en) * 1989-03-02 1990-04-17 Rhone-Poulenc Ag Company Pesticidal 3-cyano-5-alkoxy-1-arylpyrazoles, compositions and use
AR035912A1 (es) * 2000-03-02 2004-07-28 Aventis Cropscience Sa Compuestos de 4-tiometilpirazol, composicion plaguicida, metodo para el control de plagas en un lugar, semillas tratadas o recubiertas,uso de estos compuestos o composiciones para el control de plagas, uso de estos compuestos para preparar un medicamento veterinario, y,proceso para la preparacion de
JP4465133B2 (ja) * 2001-02-08 2010-05-19 クミアイ化学工業株式会社 イソオキサゾリン誘導体及びこれを有効成分とする除草剤
WO2003000686A1 (en) * 2001-06-21 2003-01-03 Kumiai Chemical Industry Co., Ltd. Isoxazoline derivatives and herbicides

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004013106A1 (ja) 2002-08-01 2004-02-12 Ihara Chemical Industry Co., Ltd. ピラゾール誘導体及びその製造方法
WO2004014138A1 (ja) 2002-08-07 2004-02-19 Kumiai Chemical Industry Co., Ltd. 除草剤組成物

Also Published As

Publication number Publication date
EP1767528A1 (en) 2007-03-28
EP1767528B1 (en) 2014-09-17
ES2508765T3 (es) 2014-10-16
JP4621939B2 (ja) 2011-02-02
CA2560936C (en) 2013-01-08
MXPA06011130A (es) 2007-01-25
TW200536832A (en) 2005-11-16
US20070185334A1 (en) 2007-08-09
CR8640A (es) 2007-08-28
BRPI0509353A (pt) 2007-09-11
IL178233A (en) 2014-02-27
AU2005228017A1 (en) 2005-10-13
RU2386619C2 (ru) 2010-04-20
BRPI0509353B1 (pt) 2019-01-02
CN1938278B (zh) 2012-12-12
NZ550143A (en) 2010-04-30
UA83910C2 (ru) 2008-08-26
PL1767528T3 (pl) 2015-03-31
CN1938278A (zh) 2007-03-28
KR20070003964A (ko) 2007-01-05
IN2006DE05581A (https=) 2007-08-31
AU2005228017B2 (en) 2010-09-30
RU2006138241A (ru) 2008-05-10
CA2560936A1 (en) 2005-10-13
IL178233A0 (en) 2006-12-31
BRPI0509353A8 (pt) 2017-09-19
EP1767528A4 (en) 2010-04-21
WO2005095352A1 (ja) 2005-10-13
US7488831B2 (en) 2009-02-10
TWI357899B (en) 2012-02-11
MX280092B (es) 2010-10-18
JP2005289824A (ja) 2005-10-20

Similar Documents

Publication Publication Date Title
KR101205731B1 (ko) 5-히드록시-4-티오메틸피라졸 화합물의 제조 방법
EP1541561B1 (en) Pyrazole derivatives and process for the production thereof
JP4703077B2 (ja) ピリミジン誘導体及びそれを含有する除草剤
JP2002308857A (ja) イソオキサゾリン誘導体及びこれを有効成分とする除草剤
BG64648B1 (bg) Метод за получаване на пиразолови производни
DK1858858T3 (en) PROCEDURE FOR THE PREPARATION OF ALKYLANILIDES
IL308857A (en) Drug therapy delivery systems and methods
JP2007246396A (ja) ５−ジフルオロメトキシ−４−チオメチルピラゾール化合物の製造方法
JP2003527381A (ja) スピロ環式テトロン酸誘導体の製造方法
JP2003531146A (ja) チアゾリジンジオン誘導体及び中間体の製造方法
JP4075357B2 (ja) ４，５−ジ置換−１，２，３−トリアゾール及びその製造法
KR101308227B1 (ko) 니코틴산 유도체 또는 그의 염의 제조 방법
WO2010116121A1 (en) Processes for making isoxazoline derivatives
JP2000229955A (ja) ５−アミノイソオキサゾリルイソオキサゾールおよびその製造法
EP2264021A1 (en) Process for producing an anthranilamide compound

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

T11-X000 Administrative time limit extension requested

St.27 status event code: U-3-3-T10-T11-oth-X000

T11-X000 Administrative time limit extension requested

St.27 status event code: U-3-3-T10-T11-oth-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

FPAY Annual fee payment

Payment date: 20161012

Year of fee payment: 5

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

FPAY Annual fee payment

Payment date: 20171017

Year of fee payment: 6

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 6

FPAY Annual fee payment

Payment date: 20181004

Year of fee payment: 7

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 7

FPAY Annual fee payment

Payment date: 20191008

Year of fee payment: 8

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 8

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 9

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 10

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 11

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 12

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 13

PC1801 Expiration of term

St.27 status event code: N-4-6-H10-H14-oth-PC1801

Not in force date: 20250401

Ip right cessation event data comment text: Termination Category : EXPIRATION_OF_DURATION