CN1938278B - 5-羟基-4-硫甲基吡唑化合物的制备方法 - Google Patents

5-羟基-4-硫甲基吡唑化合物的制备方法 Download PDF

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Publication number
CN1938278B
CN1938278B CN2005800106359A CN200580010635A CN1938278B CN 1938278 B CN1938278 B CN 1938278B CN 2005800106359 A CN2005800106359 A CN 2005800106359A CN 200580010635 A CN200580010635 A CN 200580010635A CN 1938278 B CN1938278 B CN 1938278B
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China
Prior art keywords
hydroxyl
branched
carbonyl
straight
methyl
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Expired - Lifetime
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CN2005800106359A
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Chinese (zh)
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CN1938278A (zh
Inventor
内田幸生
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Kumiai Chemical Industry Co Ltd
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Ihara Chemical Industry Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/28—Two oxygen or sulfur atoms
    • C07D231/30—Two oxygen or sulfur atoms attached in positions 3 and 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN2005800106359A 2004-03-31 2005-03-31 5-羟基-4-硫甲基吡唑化合物的制备方法 Expired - Lifetime CN1938278B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP102963/2004 2004-03-31
JP2004102963A JP4621939B2 (ja) 2004-03-31 2004-03-31 ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法
PCT/JP2005/006806 WO2005095352A1 (ja) 2004-03-31 2005-03-31 ５－ヒドロキシ－４－チオメチルピラゾール化合物の製造方法

Publications (2)

Publication Number Publication Date
CN1938278A CN1938278A (zh) 2007-03-28
CN1938278B true CN1938278B (zh) 2012-12-12

Family

ID=35063690

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2005800106359A Expired - Lifetime CN1938278B (zh) 2004-03-31 2005-03-31 5-羟基-4-硫甲基吡唑化合物的制备方法

Country Status (19)

Country Link
US (1) US7488831B2 (https=)
EP (1) EP1767528B1 (https=)
JP (1) JP4621939B2 (https=)
KR (1) KR101205731B1 (https=)
CN (1) CN1938278B (https=)
AU (1) AU2005228017B2 (https=)
BR (1) BRPI0509353B1 (https=)
CA (1) CA2560936C (https=)
CR (1) CR8640A (https=)
ES (1) ES2508765T3 (https=)
IL (1) IL178233A (https=)
IN (1) IN2006DE05581A (https=)
MX (1) MX280092B (https=)
NZ (1) NZ550143A (https=)
PL (1) PL1767528T3 (https=)
RU (1) RU2386619C2 (https=)
TW (1) TWI357899B (https=)
UA (1) UA83910C2 (https=)
WO (1) WO2005095352A1 (https=)

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WO2006037945A1 (en) 2004-10-05 2006-04-13 Syngenta Limited Isoxazoline derivatives and their use as herbicides
US7714142B2 (en) * 2004-12-20 2010-05-11 Ihara Chemical Industry Co., Ltd. Process for production of (4,5-dihydroisoxazol-3-Y) thio-carboxamidine salts
JP2007031342A (ja) * 2005-07-27 2007-02-08 Ihara Chem Ind Co Ltd ５−ヒドロキシ−１−アルキルピラゾール誘導体の製造方法
NZ570495A (en) 2006-02-14 2011-10-28 Ihara Chemical Ind Co Process for production of 5-alkoxy-4-hydroxymethylpyrazole compound
EP2167464B1 (en) * 2007-05-25 2014-12-03 AbbVie Deutschland GmbH & Co KG Heterocyclic compounds as positive modulators of metabotropic glutamate receptor 2 (mglu2 receptor)
GB0916267D0 (en) 2009-09-16 2009-10-28 Syngenta Ltd Herbicidal compounds
CN102666502B (zh) 2009-11-26 2015-01-07 巴斯夫欧洲公司 生产5,5-二取代的4,5-二氢异噁唑-3-硫基甲脒盐的方法
CA2781409A1 (en) 2009-11-26 2011-06-03 Basf Se Method for producing 5,5-disubstituted 2-isoxazolines
EP2571854B1 (en) * 2010-05-20 2014-11-05 Bayer Intellectual Property GmbH Method for manufacturing 1-alkyl-3-difluormethyl-5-hydroxypyrazoles
CN103843198B (zh) 2011-07-29 2016-05-04 萨斯喀彻温大学 聚合物基谐振器天线
CN103387541B (zh) * 2012-05-10 2016-02-10 中国中化股份有限公司 一种取代吡唑醚类化合物的制备方法
JP6400247B1 (ja) * 2015-11-16 2018-10-03 ロンザ・リミテッド １−メチル−３−（トリフルオロメチル）−１ｈ−ピラゾール−５−オールの調製方法
TW201835036A (zh) 2017-02-27 2018-10-01 瑞士商隆薩有限公司 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法
JP6664036B2 (ja) * 2017-12-27 2020-03-13 クミアイ化学工業株式会社 チオカルボキサミジン塩化合物の製造方法
WO2019230831A1 (ja) * 2018-05-31 2019-12-05 クミアイ化学工業株式会社 含フッ素ピラゾール誘導体の製造方法及びその中間体
AR119524A1 (es) 2019-07-30 2021-12-22 Adama Agan Ltd Proceso e intermediarios para la preparación de piroxasulfona
EP4053125B1 (en) 2019-10-31 2024-12-04 Kumiai Chemical Industry Co., Ltd. Process for the production of a pyroxasulfone herbicide
WO2021176456A1 (en) 2020-03-05 2021-09-10 Adama Agan Ltd. Process and intermediates for the preparation of pyroxasulfone
CN111574511A (zh) * 2020-06-28 2020-08-25 安徽久易农业股份有限公司 一种砜吡草唑的合成方法及其应用
EP4177252A3 (en) 2020-07-10 2023-08-09 Adama Agan Ltd. Process and intermediates for the preparation of pyroxasulfone, fenoxasulfone and various sulfone analogs of 5,5-dimethyl-4h-1,2-oxazole
CN112110912B (zh) * 2020-07-31 2022-07-05 绍兴贝斯美化工股份有限公司 一种合成硫醚类中间体的方法
WO2023074828A1 (ja) 2021-10-29 2023-05-04 クミアイ化学工業株式会社 ジスルフィド化合物、ポリスルフィド化合物及びその用途
AR127776A1 (es) 2021-11-28 2024-02-28 Adama Agan Ltd Composiciones de concentrado en suspensión de alta carga
CN114716428B (zh) * 2022-05-06 2024-02-06 山东潍坊润丰化工股份有限公司 制备砜吡草唑中间体的方法
CN115850178B (zh) * 2022-12-28 2025-04-04 宁夏格瑞精细化工有限公司 一种1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的制备方法
CN117417333B (zh) * 2023-10-07 2026-02-17 安徽久易农业股份有限公司 一种砜吡草唑的合成工艺
CN120590326B (zh) * 2025-06-05 2025-12-23 济南万兴达化工有限公司 一种1-甲基-3-（三氟甲基）-1h-吡唑-5-醇的制备方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001064651A1 (en) * 2000-03-02 2001-09-07 Bayer Cropscience S.A. 3-thiomethylpyrazoles as pesticides
WO2003000686A1 (en) * 2001-06-21 2003-01-03 Kumiai Chemical Industry Co., Ltd. Isoxazoline derivatives and herbicides
WO2004014138A1 (ja) * 2002-08-07 2004-02-19 Kumiai Chemical Industry Co., Ltd. 除草剤組成物
CN1491217A (zh) * 2001-02-08 2004-04-21 ��Ԩ��ѧ��ҵ��ʽ���� 异噁唑啉衍生物和含有它们作为活性组分的除草剂
CN1678588A (zh) * 2002-08-01 2005-10-05 庵原化学工业株式会社 吡唑衍生物及其生产方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4918085A (en) * 1989-03-02 1990-04-17 Rhone-Poulenc Ag Company Pesticidal 3-cyano-5-alkoxy-1-arylpyrazoles, compositions and use

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001064651A1 (en) * 2000-03-02 2001-09-07 Bayer Cropscience S.A. 3-thiomethylpyrazoles as pesticides
CN1491217A (zh) * 2001-02-08 2004-04-21 ��Ԩ��ѧ��ҵ��ʽ���� 异噁唑啉衍生物和含有它们作为活性组分的除草剂
WO2003000686A1 (en) * 2001-06-21 2003-01-03 Kumiai Chemical Industry Co., Ltd. Isoxazoline derivatives and herbicides
CN1678588A (zh) * 2002-08-01 2005-10-05 庵原化学工业株式会社 吡唑衍生物及其生产方法
WO2004014138A1 (ja) * 2002-08-07 2004-02-19 Kumiai Chemical Industry Co., Ltd. 除草剤組成物

Also Published As

Publication number Publication date
RU2006138241A (ru) 2008-05-10
CA2560936A1 (en) 2005-10-13
IN2006DE05581A (https=) 2007-08-31
EP1767528B1 (en) 2014-09-17
KR101205731B1 (ko) 2012-11-28
JP4621939B2 (ja) 2011-02-02
TW200536832A (en) 2005-11-16
KR20070003964A (ko) 2007-01-05
MX280092B (es) 2010-10-18
MXPA06011130A (es) 2007-01-25
NZ550143A (en) 2010-04-30
AU2005228017B2 (en) 2010-09-30
WO2005095352A1 (ja) 2005-10-13
BRPI0509353A8 (pt) 2017-09-19
CR8640A (es) 2007-08-28
BRPI0509353B1 (pt) 2019-01-02
US20070185334A1 (en) 2007-08-09
BRPI0509353A (pt) 2007-09-11
RU2386619C2 (ru) 2010-04-20
IL178233A (en) 2014-02-27
IL178233A0 (en) 2006-12-31
PL1767528T3 (pl) 2015-03-31
ES2508765T3 (es) 2014-10-16
CA2560936C (en) 2013-01-08
TWI357899B (en) 2012-02-11
CN1938278A (zh) 2007-03-28
JP2005289824A (ja) 2005-10-20
EP1767528A4 (en) 2010-04-21
AU2005228017A1 (en) 2005-10-13
EP1767528A1 (en) 2007-03-28
UA83910C2 (ru) 2008-08-26
US7488831B2 (en) 2009-02-10

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Effective date of registration: 20210203

Address after: Tokyo, Japan

Patentee after: Kumiai Chemical Industry Co.,Ltd.

Address before: Tokyo, Japan

Patentee before: Ihara Chemical Industry Co.,Ltd.

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CX01 Expiry of patent term

Granted publication date: 20121212

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