CN1938278B - 5-羟基-4-硫甲基吡唑化合物的制备方法 - Google Patents

5-羟基-4-硫甲基吡唑化合物的制备方法 Download PDF

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Publication number
CN1938278B
CN1938278B CN2005800106359A CN200580010635A CN1938278B CN 1938278 B CN1938278 B CN 1938278B CN 2005800106359 A CN2005800106359 A CN 2005800106359A CN 200580010635 A CN200580010635 A CN 200580010635A CN 1938278 B CN1938278 B CN 1938278B
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China
Prior art keywords
hydroxyl
branched
carbonyl
straight
methyl
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Expired - Lifetime
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CN2005800106359A
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Chinese (zh)
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CN1938278A (zh
Inventor
内田幸生
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Kumiai Chemical Industry Co Ltd
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Ihara Chemical Industry Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/28—Two oxygen or sulfur atoms
    • C07D231/30—Two oxygen or sulfur atoms attached in positions 3 and 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN2005800106359A 2004-03-31 2005-03-31 5-羟基-4-硫甲基吡唑化合物的制备方法 Expired - Lifetime CN1938278B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2004102963A JP4621939B2 (ja) 2004-03-31 2004-03-31 ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法
JP102963/2004 2004-03-31
PCT/JP2005/006806 WO2005095352A1 (ja) 2004-03-31 2005-03-31 ５－ヒドロキシ－４－チオメチルピラゾール化合物の製造方法

Publications (2)

Publication Number Publication Date
CN1938278A CN1938278A (zh) 2007-03-28
CN1938278B true CN1938278B (zh) 2012-12-12

Family

ID=35063690

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2005800106359A Expired - Lifetime CN1938278B (zh) 2004-03-31 2005-03-31 5-羟基-4-硫甲基吡唑化合物的制备方法

Country Status (19)

Country Link
US (1) US7488831B2 (https=)
EP (1) EP1767528B1 (https=)
JP (1) JP4621939B2 (https=)
KR (1) KR101205731B1 (https=)
CN (1) CN1938278B (https=)
AU (1) AU2005228017B2 (https=)
BR (1) BRPI0509353B1 (https=)
CA (1) CA2560936C (https=)
CR (1) CR8640A (https=)
ES (1) ES2508765T3 (https=)
IL (1) IL178233A (https=)
IN (1) IN2006DE05581A (https=)
MX (1) MX280092B (https=)
NZ (1) NZ550143A (https=)
PL (1) PL1767528T3 (https=)
RU (1) RU2386619C2 (https=)
TW (1) TWI357899B (https=)
UA (1) UA83910C2 (https=)
WO (1) WO2005095352A1 (https=)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2333977T3 (es) 2004-10-05 2010-03-03 Syngenta Limited Derivados de isoxazolina y su uso como herbicidas.
MX274842B (es) * 2004-12-20 2010-03-30 Ihara Chemical Ind Co Procedimiento para la produccion de sales de (4,5-dihidroisoxazol- 3-il)tiocarboxamidina.
JP2007031342A (ja) * 2005-07-27 2007-02-08 Ihara Chem Ind Co Ltd ５−ヒドロキシ−１−アルキルピラゾール誘導体の製造方法
CA2642308C (en) * 2006-02-14 2013-12-17 Ihara Chemical Industry Co., Ltd. Process for production of 5-alkoxy-4-hydroxymethylpyrazole compound
TWI443090B (zh) * 2007-05-25 2014-07-01 Abbvie Deutschland 作為代謝性麩胺酸受體２（ｍｇｌｕ２ 受體）之正向調節劑之雜環化合物
GB0916267D0 (en) 2009-09-16 2009-10-28 Syngenta Ltd Herbicidal compounds
US20120238760A1 (en) 2009-11-26 2012-09-20 Basf Se Method for Producing 5,5-Disubstituted 2-Isoxazolines
ES2466322T3 (es) * 2009-11-26 2014-06-10 Basf Se Procedimiento para la preparación de sales de 4,5-dihidroisoxazol-3-tiocarboxamidina 5,5-disustituida
DK2571854T3 (en) * 2010-05-20 2015-02-09 Bayer Ip Gmbh PROCESS FOR THE PREPARATION OF 1-alkyl-3-difluoromethyl-5-hydroxypyrazoles
CA2843415C (en) 2011-07-29 2019-12-31 University Of Saskatchewan Polymer-based resonator antennas
CN103387541B (zh) * 2012-05-10 2016-02-10 中国中化股份有限公司 一种取代吡唑醚类化合物的制备方法
JP6400247B1 (ja) 2015-11-16 2018-10-03 ロンザ・リミテッド １−メチル−３−（トリフルオロメチル）−１ｈ−ピラゾール−５−オールの調製方法
TW201835036A (zh) 2017-02-27 2018-10-01 瑞士商隆薩有限公司 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法
JP6664036B2 (ja) 2017-12-27 2020-03-13 クミアイ化学工業株式会社 チオカルボキサミジン塩化合物の製造方法
CN112135814B (zh) * 2018-05-31 2021-09-28 组合化学工业株式会社 含氟吡唑衍生物的制造方法及其中间体
EP4003964B1 (en) 2019-07-30 2024-09-18 Adama Agan Ltd. Process and intermediates for the preparation of pyroxasulfone
KR102523028B1 (ko) 2019-10-31 2023-04-17 구미아이 가가쿠 고교 가부시키가이샤 제초제 및 그 중간체의 제조방법
IL296145A (en) 2020-03-05 2022-11-01 Adama Agan Ltd A process for the preparation of pyroxasulfone and intermediates obtained in this process
CN111574511A (zh) * 2020-06-28 2020-08-25 安徽久易农业股份有限公司 一种砜吡草唑的合成方法及其应用
EP4177252A3 (en) 2020-07-10 2023-08-09 Adama Agan Ltd. Process and intermediates for the preparation of pyroxasulfone, fenoxasulfone and various sulfone analogs of 5,5-dimethyl-4h-1,2-oxazole
CN112110912B (zh) * 2020-07-31 2022-07-05 绍兴贝斯美化工股份有限公司 一种合成硫醚类中间体的方法
WO2023074828A1 (ja) 2021-10-29 2023-05-04 クミアイ化学工業株式会社 ジスルフィド化合物、ポリスルフィド化合物及びその用途
AR127776A1 (es) 2021-11-28 2024-02-28 Adama Agan Ltd Composiciones de concentrado en suspensión de alta carga
CN114716428B (zh) * 2022-05-06 2024-02-06 山东潍坊润丰化工股份有限公司 制备砜吡草唑中间体的方法
CN115850178B (zh) * 2022-12-28 2025-04-04 宁夏格瑞精细化工有限公司 一种1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的制备方法
CN117417333B (zh) * 2023-10-07 2026-02-17 安徽久易农业股份有限公司 一种砜吡草唑的合成工艺
CN120590326B (zh) * 2025-06-05 2025-12-23 济南万兴达化工有限公司 一种1-甲基-3-（三氟甲基）-1h-吡唑-5-醇的制备方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001064651A1 (en) * 2000-03-02 2001-09-07 Bayer Cropscience S.A. 3-thiomethylpyrazoles as pesticides
WO2003000686A1 (en) * 2001-06-21 2003-01-03 Kumiai Chemical Industry Co., Ltd. Isoxazoline derivatives and herbicides
WO2004014138A1 (ja) * 2002-08-07 2004-02-19 Kumiai Chemical Industry Co., Ltd. 除草剤組成物
CN1491217A (zh) * 2001-02-08 2004-04-21 ��Ԩ��ѧ��ҵ��ʽ���� 异噁唑啉衍生物和含有它们作为活性组分的除草剂
CN1678588A (zh) * 2002-08-01 2005-10-05 庵原化学工业株式会社 吡唑衍生物及其生产方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4918085A (en) * 1989-03-02 1990-04-17 Rhone-Poulenc Ag Company Pesticidal 3-cyano-5-alkoxy-1-arylpyrazoles, compositions and use

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001064651A1 (en) * 2000-03-02 2001-09-07 Bayer Cropscience S.A. 3-thiomethylpyrazoles as pesticides
CN1491217A (zh) * 2001-02-08 2004-04-21 ��Ԩ��ѧ��ҵ��ʽ���� 异噁唑啉衍生物和含有它们作为活性组分的除草剂
WO2003000686A1 (en) * 2001-06-21 2003-01-03 Kumiai Chemical Industry Co., Ltd. Isoxazoline derivatives and herbicides
CN1678588A (zh) * 2002-08-01 2005-10-05 庵原化学工业株式会社 吡唑衍生物及其生产方法
WO2004014138A1 (ja) * 2002-08-07 2004-02-19 Kumiai Chemical Industry Co., Ltd. 除草剤組成物

Also Published As

Publication number Publication date
EP1767528A1 (en) 2007-03-28
EP1767528B1 (en) 2014-09-17
ES2508765T3 (es) 2014-10-16
JP4621939B2 (ja) 2011-02-02
CA2560936C (en) 2013-01-08
MXPA06011130A (es) 2007-01-25
TW200536832A (en) 2005-11-16
US20070185334A1 (en) 2007-08-09
CR8640A (es) 2007-08-28
BRPI0509353A (pt) 2007-09-11
IL178233A (en) 2014-02-27
AU2005228017A1 (en) 2005-10-13
RU2386619C2 (ru) 2010-04-20
BRPI0509353B1 (pt) 2019-01-02
NZ550143A (en) 2010-04-30
UA83910C2 (ru) 2008-08-26
PL1767528T3 (pl) 2015-03-31
CN1938278A (zh) 2007-03-28
KR20070003964A (ko) 2007-01-05
IN2006DE05581A (https=) 2007-08-31
AU2005228017B2 (en) 2010-09-30
RU2006138241A (ru) 2008-05-10
CA2560936A1 (en) 2005-10-13
IL178233A0 (en) 2006-12-31
KR101205731B1 (ko) 2012-11-28
BRPI0509353A8 (pt) 2017-09-19
EP1767528A4 (en) 2010-04-21
WO2005095352A1 (ja) 2005-10-13
US7488831B2 (en) 2009-02-10
TWI357899B (en) 2012-02-11
MX280092B (es) 2010-10-18
JP2005289824A (ja) 2005-10-20

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SE01 Entry into force of request for substantive examination
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GR01 Patent grant
TR01 Transfer of patent right

Effective date of registration: 20210203

Address after: Tokyo, Japan

Patentee after: Kumiai Chemical Industry Co.,Ltd.

Address before: Tokyo, Japan

Patentee before: Ihara Chemical Industry Co.,Ltd.

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CX01 Expiry of patent term

Granted publication date: 20121212

CX01 Expiry of patent term