TWI357899B - Process for producing 5-hydroxy-4-thiomethylpyrazo - Google Patents

Process for producing 5-hydroxy-4-thiomethylpyrazo Download PDF

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Publication number
TWI357899B
TWI357899B TW094110223A TW94110223A TWI357899B TW I357899 B TWI357899 B TW I357899B TW 094110223 A TW094110223 A TW 094110223A TW 94110223 A TW94110223 A TW 94110223A TW I357899 B TWI357899 B TW I357899B
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TW
Taiwan
Prior art keywords
group
hydroxy
reaction
mmol
compound
Prior art date
Application number
TW094110223A
Other languages
English (en)
Chinese (zh)
Other versions
TW200536832A (en
Inventor
Yukio Uchida
Original Assignee
Ihara Chemical Ind Co
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Publication date
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Application filed by Ihara Chemical Ind Co filed Critical Ihara Chemical Ind Co
Publication of TW200536832A publication Critical patent/TW200536832A/zh
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Publication of TWI357899B publication Critical patent/TWI357899B/zh

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/28—Two oxygen or sulfur atoms
    • C07D231/30—Two oxygen or sulfur atoms attached in positions 3 and 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
TW094110223A 2004-03-31 2005-03-31 Process for producing 5-hydroxy-4-thiomethylpyrazo TWI357899B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2004102963A JP4621939B2 (ja) 2004-03-31 2004-03-31 ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法

Publications (2)

Publication Number Publication Date
TW200536832A TW200536832A (en) 2005-11-16
TWI357899B true TWI357899B (en) 2012-02-11

Family

ID=35063690

Family Applications (1)

Application Number Title Priority Date Filing Date
TW094110223A TWI357899B (en) 2004-03-31 2005-03-31 Process for producing 5-hydroxy-4-thiomethylpyrazo

Country Status (19)

Country Link
US (1) US7488831B2 (https=)
EP (1) EP1767528B1 (https=)
JP (1) JP4621939B2 (https=)
KR (1) KR101205731B1 (https=)
CN (1) CN1938278B (https=)
AU (1) AU2005228017B2 (https=)
BR (1) BRPI0509353B1 (https=)
CA (1) CA2560936C (https=)
CR (1) CR8640A (https=)
ES (1) ES2508765T3 (https=)
IL (1) IL178233A (https=)
IN (1) IN2006DE05581A (https=)
MX (1) MX280092B (https=)
NZ (1) NZ550143A (https=)
PL (1) PL1767528T3 (https=)
RU (1) RU2386619C2 (https=)
TW (1) TWI357899B (https=)
UA (1) UA83910C2 (https=)
WO (1) WO2005095352A1 (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI848950B (zh) * 2018-05-31 2024-07-21 日商組合化學工業股份有限公司 含氟之吡唑衍生物之製造方法及其中間物

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ES2333977T3 (es) 2004-10-05 2010-03-03 Syngenta Limited Derivados de isoxazolina y su uso como herbicidas.
MX274842B (es) * 2004-12-20 2010-03-30 Ihara Chemical Ind Co Procedimiento para la produccion de sales de (4,5-dihidroisoxazol- 3-il)tiocarboxamidina.
JP2007031342A (ja) * 2005-07-27 2007-02-08 Ihara Chem Ind Co Ltd ５−ヒドロキシ−１−アルキルピラゾール誘導体の製造方法
CA2642308C (en) * 2006-02-14 2013-12-17 Ihara Chemical Industry Co., Ltd. Process for production of 5-alkoxy-4-hydroxymethylpyrazole compound
TWI443090B (zh) * 2007-05-25 2014-07-01 Abbvie Deutschland 作為代謝性麩胺酸受體２（ｍｇｌｕ２ 受體）之正向調節劑之雜環化合物
GB0916267D0 (en) 2009-09-16 2009-10-28 Syngenta Ltd Herbicidal compounds
US20120238760A1 (en) 2009-11-26 2012-09-20 Basf Se Method for Producing 5,5-Disubstituted 2-Isoxazolines
ES2466322T3 (es) * 2009-11-26 2014-06-10 Basf Se Procedimiento para la preparación de sales de 4,5-dihidroisoxazol-3-tiocarboxamidina 5,5-disustituida
DK2571854T3 (en) * 2010-05-20 2015-02-09 Bayer Ip Gmbh PROCESS FOR THE PREPARATION OF 1-alkyl-3-difluoromethyl-5-hydroxypyrazoles
CA2843415C (en) 2011-07-29 2019-12-31 University Of Saskatchewan Polymer-based resonator antennas
CN103387541B (zh) * 2012-05-10 2016-02-10 中国中化股份有限公司 一种取代吡唑醚类化合物的制备方法
JP6400247B1 (ja) 2015-11-16 2018-10-03 ロンザ・リミテッド １−メチル−３−（トリフルオロメチル）−１ｈ−ピラゾール−５−オールの調製方法
TW201835036A (zh) 2017-02-27 2018-10-01 瑞士商隆薩有限公司 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法
JP6664036B2 (ja) 2017-12-27 2020-03-13 クミアイ化学工業株式会社 チオカルボキサミジン塩化合物の製造方法
EP4003964B1 (en) 2019-07-30 2024-09-18 Adama Agan Ltd. Process and intermediates for the preparation of pyroxasulfone
KR102523028B1 (ko) 2019-10-31 2023-04-17 구미아이 가가쿠 고교 가부시키가이샤 제초제 및 그 중간체의 제조방법
IL296145A (en) 2020-03-05 2022-11-01 Adama Agan Ltd A process for the preparation of pyroxasulfone and intermediates obtained in this process
CN111574511A (zh) * 2020-06-28 2020-08-25 安徽久易农业股份有限公司 一种砜吡草唑的合成方法及其应用
EP4177252A3 (en) 2020-07-10 2023-08-09 Adama Agan Ltd. Process and intermediates for the preparation of pyroxasulfone, fenoxasulfone and various sulfone analogs of 5,5-dimethyl-4h-1,2-oxazole
CN112110912B (zh) * 2020-07-31 2022-07-05 绍兴贝斯美化工股份有限公司 一种合成硫醚类中间体的方法
WO2023074828A1 (ja) 2021-10-29 2023-05-04 クミアイ化学工業株式会社 ジスルフィド化合物、ポリスルフィド化合物及びその用途
AR127776A1 (es) 2021-11-28 2024-02-28 Adama Agan Ltd Composiciones de concentrado en suspensión de alta carga
CN114716428B (zh) * 2022-05-06 2024-02-06 山东潍坊润丰化工股份有限公司 制备砜吡草唑中间体的方法
CN115850178B (zh) * 2022-12-28 2025-04-04 宁夏格瑞精细化工有限公司 一种1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的制备方法
CN117417333B (zh) * 2023-10-07 2026-02-17 安徽久易农业股份有限公司 一种砜吡草唑的合成工艺
CN120590326B (zh) * 2025-06-05 2025-12-23 济南万兴达化工有限公司 一种1-甲基-3-（三氟甲基）-1h-吡唑-5-醇的制备方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4918085A (en) * 1989-03-02 1990-04-17 Rhone-Poulenc Ag Company Pesticidal 3-cyano-5-alkoxy-1-arylpyrazoles, compositions and use
AR035912A1 (es) * 2000-03-02 2004-07-28 Aventis Cropscience Sa Compuestos de 4-tiometilpirazol, composicion plaguicida, metodo para el control de plagas en un lugar, semillas tratadas o recubiertas,uso de estos compuestos o composiciones para el control de plagas, uso de estos compuestos para preparar un medicamento veterinario, y,proceso para la preparacion de
JP4465133B2 (ja) * 2001-02-08 2010-05-19 クミアイ化学工業株式会社 イソオキサゾリン誘導体及びこれを有効成分とする除草剤
WO2003000686A1 (en) * 2001-06-21 2003-01-03 Kumiai Chemical Industry Co., Ltd. Isoxazoline derivatives and herbicides
AU2003252447B2 (en) * 2002-08-01 2008-06-05 Kumiai Chemical Industry Co., Ltd. Pyrazole derivatives and process for the production thereof
UA78071C2 (en) * 2002-08-07 2007-02-15 Kumiai Chemical Industry Co Herbicidal composition

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI848950B (zh) * 2018-05-31 2024-07-21 日商組合化學工業股份有限公司 含氟之吡唑衍生物之製造方法及其中間物

Also Published As

Publication number Publication date
EP1767528A1 (en) 2007-03-28
EP1767528B1 (en) 2014-09-17
ES2508765T3 (es) 2014-10-16
JP4621939B2 (ja) 2011-02-02
CA2560936C (en) 2013-01-08
MXPA06011130A (es) 2007-01-25
TW200536832A (en) 2005-11-16
US20070185334A1 (en) 2007-08-09
CR8640A (es) 2007-08-28
BRPI0509353A (pt) 2007-09-11
IL178233A (en) 2014-02-27
AU2005228017A1 (en) 2005-10-13
RU2386619C2 (ru) 2010-04-20
BRPI0509353B1 (pt) 2019-01-02
CN1938278B (zh) 2012-12-12
NZ550143A (en) 2010-04-30
UA83910C2 (ru) 2008-08-26
PL1767528T3 (pl) 2015-03-31
CN1938278A (zh) 2007-03-28
KR20070003964A (ko) 2007-01-05
IN2006DE05581A (https=) 2007-08-31
AU2005228017B2 (en) 2010-09-30
RU2006138241A (ru) 2008-05-10
CA2560936A1 (en) 2005-10-13
IL178233A0 (en) 2006-12-31
KR101205731B1 (ko) 2012-11-28
BRPI0509353A8 (pt) 2017-09-19
EP1767528A4 (en) 2010-04-21
WO2005095352A1 (ja) 2005-10-13
US7488831B2 (en) 2009-02-10
MX280092B (es) 2010-10-18
JP2005289824A (ja) 2005-10-20

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