BRPI0509353A8 - Processo para a produção de um composto de 5-hidróxi-4-tiometilpirazol - Google Patents
Processo para a produção de um composto de 5-hidróxi-4-tiometilpirazolInfo
- Publication number
- BRPI0509353A8 BRPI0509353A8 BRPI0509353A BRPI0509353A BRPI0509353A8 BR PI0509353 A8 BRPI0509353 A8 BR PI0509353A8 BR PI0509353 A BRPI0509353 A BR PI0509353A BR PI0509353 A BRPI0509353 A BR PI0509353A BR PI0509353 A8 BRPI0509353 A8 BR PI0509353A8
- Authority
- BR
- Brazil
- Prior art keywords
- hydroxy
- thiomethylpyrazole
- compound
- general formula
- production
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/18—One oxygen or sulfur atom
- C07D231/20—One oxygen atom attached in position 3 or 5
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/28—Two oxygen or sulfur atoms
- C07D231/30—Two oxygen or sulfur atoms attached in positions 3 and 5
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
- C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
- C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plural Heterocyclic Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
PROCESSO PARA A PRODUÇÃO DE UM COM POSTO DE 5-HIDRÓXI-4-TIOMETILPIRAZOL. A presente invenção refere-se a um composto de pirazol representado pela fórmula geral (1) que é reagido com um composto de enxofre representado pela fórmula geral (2) na presença de uma base e formaldeído, para produzir assim um composto de 5-hidróxi-4-tiometilpirazol representado pela fórmula geral (3). O composto de 5-hidróxi-4-tiometilpirazol pode ser facilmente produzido em um bom rendimento, através da utilização de tal processo. Ainda, este processo pode fornecer facilmente o composto de 5-hidróxi-4-tiometilpirazol sob uma condição suave em uma única etapa, sem utilizar um aparato especial, um catalisador ou um metal de transição dispendioso etc.Em adição, este processo pode ser realizado substancialmente sem produzir um rejeito prejudicial que pode ser derivado de um catalisador etc, e, portanto, este processo é inofensivo ao ambiente e tem valor industrial.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2004102963A JP4621939B2 (ja) | 2004-03-31 | 2004-03-31 | 5−ヒドロキシ−4−チオメチルピラゾール化合物の製造方法 |
PCT/JP2005/006806 WO2005095352A1 (ja) | 2004-03-31 | 2005-03-31 | 5-ヒドロキシ-4-チオメチルピラゾール化合物の製造方法 |
Publications (3)
Publication Number | Publication Date |
---|---|
BRPI0509353A BRPI0509353A (pt) | 2007-09-11 |
BRPI0509353A8 true BRPI0509353A8 (pt) | 2017-09-19 |
BRPI0509353B1 BRPI0509353B1 (pt) | 2019-01-02 |
Family
ID=35063690
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0509353A BRPI0509353B1 (pt) | 2004-03-31 | 2005-03-31 | processo para a produção de um composto de 5-hidróxi-4-tiometilpirazol |
Country Status (19)
Country | Link |
---|---|
US (1) | US7488831B2 (pt) |
EP (1) | EP1767528B1 (pt) |
JP (1) | JP4621939B2 (pt) |
KR (1) | KR101205731B1 (pt) |
CN (1) | CN1938278B (pt) |
AU (1) | AU2005228017B2 (pt) |
BR (1) | BRPI0509353B1 (pt) |
CA (1) | CA2560936C (pt) |
CR (1) | CR8640A (pt) |
ES (1) | ES2508765T3 (pt) |
IL (1) | IL178233A (pt) |
IN (1) | IN2006DE05581A (pt) |
MX (1) | MX280092B (pt) |
NZ (1) | NZ550143A (pt) |
PL (1) | PL1767528T3 (pt) |
RU (1) | RU2386619C2 (pt) |
TW (1) | TWI357899B (pt) |
UA (1) | UA83910C2 (pt) |
WO (1) | WO2005095352A1 (pt) |
Families Citing this family (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1799657B1 (en) | 2004-10-05 | 2009-12-02 | Syngenta Limited | Isoxazoline derivatives and their use as herbicides |
JP4927565B2 (ja) * | 2004-12-20 | 2012-05-09 | イハラケミカル工業株式会社 | (4,5−ジヒドロイソオキサゾロ−3−イル)チオカルボキサミジン塩化合物の製造方法 |
JP2007031342A (ja) * | 2005-07-27 | 2007-02-08 | Ihara Chem Ind Co Ltd | 5−ヒドロキシ−1−アルキルピラゾール誘導体の製造方法 |
TWI385155B (zh) * | 2006-02-14 | 2013-02-11 | Ihara Chemical Ind Co | 5-alkoxy-4-hydroxymethylpyrazole compound |
RU2479577C2 (ru) * | 2007-05-25 | 2013-04-20 | Эбботт Гмбх Унд Ко.Кг | Гетероциклические соединения в качестве положительных модуляторов метаботропного глутаматного рецептора 2 (рецептора mglu2) |
GB0916267D0 (en) | 2009-09-16 | 2009-10-28 | Syngenta Ltd | Herbicidal compounds |
WO2011063843A1 (de) | 2009-11-26 | 2011-06-03 | Basf Se | Verfahren zur herstellung 5,5-disubstituierter 2-isoxazoline |
MX2012005884A (es) * | 2009-11-26 | 2012-06-19 | Basf Se | Metodo para producir sales de 4,5-dihidroisoxazol-3-tiocarboxamidi na 5,5-disustituida. |
WO2011144549A1 (en) * | 2010-05-20 | 2011-11-24 | Bayer Cropscience Ag | Method for manufacturing 1 - alkyl - 3 - difluormethyl - 5 - hydroxypyrazoles |
US10361487B2 (en) | 2011-07-29 | 2019-07-23 | University Of Saskatchewan | Polymer-based resonator antennas |
CN103387541B (zh) * | 2012-05-10 | 2016-02-10 | 中国中化股份有限公司 | 一种取代吡唑醚类化合物的制备方法 |
JP6400247B1 (ja) * | 2015-11-16 | 2018-10-03 | ロンザ・リミテッド | 1−メチル−3−(トリフルオロメチル)−1h−ピラゾール−5−オールの調製方法 |
TW201835036A (zh) | 2017-02-27 | 2018-10-01 | 瑞士商隆薩有限公司 | 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法 |
MX2020006837A (es) * | 2017-12-27 | 2020-09-03 | Kumiai Chemical Industry Co | Metodo para producir un compuesto de sal de tiocarboxamidina. |
JP6714785B2 (ja) * | 2018-05-31 | 2020-06-24 | クミアイ化学工業株式会社 | 含フッ素ピラゾール誘導体の製造方法及びその中間体 |
CA3149137A1 (en) | 2019-07-30 | 2021-02-04 | Adama Agan Ltd. | Process and intermediates for the preparation of pyroxasulfone |
BR122023000998A8 (pt) | 2019-10-31 | 2023-05-02 | Kumiai Chemical Industry Co | Cristal de piroxassulfona, composição agroquímica, e, processos para a produção de um cristal de piroxassulfona e de uma composição agroquímica |
EP4114833A1 (en) | 2020-03-05 | 2023-01-11 | Adama Agan Ltd. | Process and intermediates for the preparation of pyroxasulfone |
CN111574511A (zh) * | 2020-06-28 | 2020-08-25 | 安徽久易农业股份有限公司 | 一种砜吡草唑的合成方法及其应用 |
EP3936503A1 (en) | 2020-07-10 | 2022-01-12 | Adama Agan Ltd. | Process and intermediates for the preparation of pyroxasulfone, fenoxasulfone and various sulfone analogs of 5,5-dimethyl-4h-1,2-oxazole |
CN112110912B (zh) * | 2020-07-31 | 2022-07-05 | 绍兴贝斯美化工股份有限公司 | 一种合成硫醚类中间体的方法 |
WO2023074828A1 (ja) | 2021-10-29 | 2023-05-04 | クミアイ化学工業株式会社 | ジスルフィド化合物、ポリスルフィド化合物及びその用途 |
AR127776A1 (es) | 2021-11-28 | 2024-02-28 | Adama Agan Ltd | Composiciones de concentrado en suspensión de alta carga |
CN114716428B (zh) * | 2022-05-06 | 2024-02-06 | 山东潍坊润丰化工股份有限公司 | 制备砜吡草唑中间体的方法 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AR035912A1 (es) * | 2000-03-02 | 2004-07-28 | Aventis Cropscience Sa | Compuestos de 4-tiometilpirazol, composicion plaguicida, metodo para el control de plagas en un lugar, semillas tratadas o recubiertas,uso de estos compuestos o composiciones para el control de plagas, uso de estos compuestos para preparar un medicamento veterinario, y,proceso para la preparacion de |
JP4465133B2 (ja) * | 2001-02-08 | 2010-05-19 | クミアイ化学工業株式会社 | イソオキサゾリン誘導体及びこれを有効成分とする除草剤 |
DE60238194D1 (de) * | 2001-06-21 | 2010-12-16 | Kumiai Chemical Industry Co | Isoxazolinderivate und herbizide |
ES2519442T3 (es) * | 2002-08-01 | 2014-11-07 | Ihara Chemical Industry Co., Ltd. | Derivados del pirazol y procesos para la producción de los mismos |
UA78071C2 (en) * | 2002-08-07 | 2007-02-15 | Kumiai Chemical Industry Co | Herbicidal composition |
-
2004
- 2004-03-31 JP JP2004102963A patent/JP4621939B2/ja not_active Expired - Lifetime
-
2005
- 2005-03-31 AU AU2005228017A patent/AU2005228017B2/en active Active
- 2005-03-31 TW TW094110223A patent/TWI357899B/zh active
- 2005-03-31 US US10/594,710 patent/US7488831B2/en active Active
- 2005-03-31 CA CA2560936A patent/CA2560936C/en active Active
- 2005-03-31 WO PCT/JP2005/006806 patent/WO2005095352A1/ja active Application Filing
- 2005-03-31 BR BRPI0509353A patent/BRPI0509353B1/pt active IP Right Grant
- 2005-03-31 MX MXPA06011130 patent/MX280092B/es active IP Right Grant
- 2005-03-31 CN CN2005800106359A patent/CN1938278B/zh active Active
- 2005-03-31 PL PL05728918T patent/PL1767528T3/pl unknown
- 2005-03-31 UA UAA200611331A patent/UA83910C2/ru unknown
- 2005-03-31 EP EP05728918.3A patent/EP1767528B1/en active Active
- 2005-03-31 KR KR1020067019480A patent/KR101205731B1/ko active IP Right Grant
- 2005-03-31 ES ES05728918.3T patent/ES2508765T3/es active Active
- 2005-03-31 RU RU2006138241/04A patent/RU2386619C2/ru active
- 2005-03-31 NZ NZ550143A patent/NZ550143A/en unknown
-
2006
- 2006-09-20 CR CR8640A patent/CR8640A/es unknown
- 2006-09-21 IL IL178233A patent/IL178233A/en active IP Right Grant
- 2006-09-25 IN IN5581DE2006 patent/IN2006DE05581A/en unknown
Also Published As
Publication number | Publication date |
---|---|
AU2005228017B2 (en) | 2010-09-30 |
IN2006DE05581A (pt) | 2007-08-31 |
MX280092B (es) | 2010-10-18 |
CR8640A (es) | 2007-08-28 |
UA83910C2 (ru) | 2008-08-26 |
CN1938278B (zh) | 2012-12-12 |
TW200536832A (en) | 2005-11-16 |
TWI357899B (en) | 2012-02-11 |
US20070185334A1 (en) | 2007-08-09 |
JP4621939B2 (ja) | 2011-02-02 |
RU2386619C2 (ru) | 2010-04-20 |
EP1767528B1 (en) | 2014-09-17 |
IL178233A0 (en) | 2006-12-31 |
EP1767528A4 (en) | 2010-04-21 |
CA2560936C (en) | 2013-01-08 |
CA2560936A1 (en) | 2005-10-13 |
MXPA06011130A (es) | 2007-01-25 |
BRPI0509353B1 (pt) | 2019-01-02 |
EP1767528A1 (en) | 2007-03-28 |
IL178233A (en) | 2014-02-27 |
CN1938278A (zh) | 2007-03-28 |
WO2005095352A1 (ja) | 2005-10-13 |
PL1767528T3 (pl) | 2015-03-31 |
RU2006138241A (ru) | 2008-05-10 |
BRPI0509353A (pt) | 2007-09-11 |
US7488831B2 (en) | 2009-02-10 |
NZ550143A (en) | 2010-04-30 |
KR101205731B1 (ko) | 2012-11-28 |
AU2005228017A1 (en) | 2005-10-13 |
JP2005289824A (ja) | 2005-10-20 |
KR20070003964A (ko) | 2007-01-05 |
ES2508765T3 (es) | 2014-10-16 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B06F | Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette] | ||
B07D | Technical examination (opinion) related to article 229 of industrial property law [chapter 7.4 patent gazette] | ||
B25A | Requested transfer of rights approved |
Owner name: KUMIAI CHEMICAL INDUSTRY CO., LTD. (JP) |
|
B07G | Grant request does not fulfill article 229-c lpi (prior consent of anvisa) [chapter 7.7 patent gazette] | ||
B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 02/01/2019, OBSERVADAS AS CONDICOES LEGAIS. |