RU2386619C2 - Способ получения 5-гидрокси-4-тиометилпиразольного соединения - Google Patents
Способ получения 5-гидрокси-4-тиометилпиразольного соединения Download PDFInfo
- Publication number
- RU2386619C2 RU2386619C2 RU2006138241/04A RU2006138241A RU2386619C2 RU 2386619 C2 RU2386619 C2 RU 2386619C2 RU 2006138241/04 A RU2006138241/04 A RU 2006138241/04A RU 2006138241 A RU2006138241 A RU 2006138241A RU 2386619 C2 RU2386619 C2 RU 2386619C2
- Authority
- RU
- Russia
- Prior art keywords
- group
- hydroxy
- compound
- mmol
- reaction
- Prior art date
Links
- 0 Cc1n[n](*)c(O)c1CS Chemical compound Cc1n[n](*)c(O)c1CS 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/18—One oxygen or sulfur atom
- C07D231/20—One oxygen atom attached in position 3 or 5
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/28—Two oxygen or sulfur atoms
- C07D231/30—Two oxygen or sulfur atoms attached in positions 3 and 5
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
- C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
- C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plural Heterocyclic Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2004-102963 | 2004-03-31 | ||
| JP2004102963A JP4621939B2 (ja) | 2004-03-31 | 2004-03-31 | ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2006138241A RU2006138241A (ru) | 2008-05-10 |
| RU2386619C2 true RU2386619C2 (ru) | 2010-04-20 |
Family
ID=35063690
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2006138241/04A RU2386619C2 (ru) | 2004-03-31 | 2005-03-31 | Способ получения 5-гидрокси-4-тиометилпиразольного соединения |
Country Status (19)
| Country | Link |
|---|---|
| US (1) | US7488831B2 (enExample) |
| EP (1) | EP1767528B1 (enExample) |
| JP (1) | JP4621939B2 (enExample) |
| KR (1) | KR101205731B1 (enExample) |
| CN (1) | CN1938278B (enExample) |
| AU (1) | AU2005228017B2 (enExample) |
| BR (1) | BRPI0509353B1 (enExample) |
| CA (1) | CA2560936C (enExample) |
| CR (1) | CR8640A (enExample) |
| ES (1) | ES2508765T3 (enExample) |
| IL (1) | IL178233A (enExample) |
| IN (1) | IN2006DE05581A (enExample) |
| MX (1) | MX280092B (enExample) |
| NZ (1) | NZ550143A (enExample) |
| PL (1) | PL1767528T3 (enExample) |
| RU (1) | RU2386619C2 (enExample) |
| TW (1) | TWI357899B (enExample) |
| UA (1) | UA83910C2 (enExample) |
| WO (1) | WO2005095352A1 (enExample) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2333977T3 (es) | 2004-10-05 | 2010-03-03 | Syngenta Limited | Derivados de isoxazolina y su uso como herbicidas. |
| US7714142B2 (en) * | 2004-12-20 | 2010-05-11 | Ihara Chemical Industry Co., Ltd. | Process for production of (4,5-dihydroisoxazol-3-Y) thio-carboxamidine salts |
| JP2007031342A (ja) * | 2005-07-27 | 2007-02-08 | Ihara Chem Ind Co Ltd | ５−ヒドロキシ−１−アルキルピラゾール誘導体の製造方法 |
| KR101401139B1 (ko) * | 2006-02-14 | 2014-05-29 | 이하라케미칼 고교가부시키가이샤 | 5-알콕시-4-히드록시메틸피라졸 화합물의 제조방법 |
| RU2479577C2 (ru) * | 2007-05-25 | 2013-04-20 | Эбботт Гмбх Унд Ко.Кг | Гетероциклические соединения в качестве положительных модуляторов метаботропного глутаматного рецептора 2 (рецептора mglu2) |
| GB0916267D0 (en) | 2009-09-16 | 2009-10-28 | Syngenta Ltd | Herbicidal compounds |
| BR112012012584B1 (pt) * | 2009-11-26 | 2017-10-31 | Basf Se | A process for preparing 5,5-disubstituted 4,5-dihydroisoxazol-3-thiocarboxamidine salts |
| EP2504321B1 (de) | 2009-11-26 | 2014-04-16 | Basf Se | Verfahren zur herstellung 5,5-disubstituierter 2-isoxazoline |
| WO2011144549A1 (en) * | 2010-05-20 | 2011-11-24 | Bayer Cropscience Ag | Method for manufacturing 1 - alkyl - 3 - difluormethyl - 5 - hydroxypyrazoles |
| EP2737575B1 (en) | 2011-07-29 | 2024-05-01 | University of Saskatchewan | Polymer-based resonator antennas |
| CN103387541B (zh) * | 2012-05-10 | 2016-02-10 | 中国中化股份有限公司 | 一种取代吡唑醚类化合物的制备方法 |
| WO2017084995A1 (en) | 2015-11-16 | 2017-05-26 | Lonza Ltd | Method for preparation of 1-methyl-3-(trifluoromethyl)-1hpyrazol-5-ol |
| TW201835036A (zh) | 2017-02-27 | 2018-10-01 | 瑞士商隆薩有限公司 | 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法 |
| BR112020012995B1 (pt) * | 2017-12-27 | 2021-08-24 | Kumiai Chemical Industry Co., Ltd | Processo para produzir um composto de sal de (4,5-dihidroisoxasol-3-il)tiocarboxamidina |
| WO2019230831A1 (ja) * | 2018-05-31 | 2019-12-05 | クミアイ化学工業株式会社 | 含フッ素ピラゾール誘導体の製造方法及びその中間体 |
| CN114450270B (zh) | 2019-07-30 | 2025-05-06 | 安道麦阿甘有限公司 | 砜吡草唑的制备方法和中间体 |
| IL292532B1 (en) | 2019-10-31 | 2024-04-01 | Kumiai Chemical Industry Co | Process for producing herbicide and intermediate thereof |
| BR112022017794A2 (pt) | 2020-03-05 | 2022-10-25 | Adama Agan Ltd | Processo e intermediários para a preparação de piroxassulfona |
| CN111574511A (zh) * | 2020-06-28 | 2020-08-25 | 安徽久易农业股份有限公司 | 一种砜吡草唑的合成方法及其应用 |
| EP4177252A3 (en) | 2020-07-10 | 2023-08-09 | Adama Agan Ltd. | Process and intermediates for the preparation of pyroxasulfone, fenoxasulfone and various sulfone analogs of 5,5-dimethyl-4h-1,2-oxazole |
| CN112110912B (zh) * | 2020-07-31 | 2022-07-05 | 绍兴贝斯美化工股份有限公司 | 一种合成硫醚类中间体的方法 |
| TW202334128A (zh) | 2021-10-29 | 2023-09-01 | 日商組合化學工業股份有限公司 | 二硫化物化合物、多硫化物化合物及其用途 |
| AR127776A1 (es) | 2021-11-28 | 2024-02-28 | Adama Agan Ltd | Composiciones de concentrado en suspensión de alta carga |
| CN114716428B (zh) * | 2022-05-06 | 2024-02-06 | 山东潍坊润丰化工股份有限公司 | 制备砜吡草唑中间体的方法 |
| CN115850178B (zh) * | 2022-12-28 | 2025-04-04 | 宁夏格瑞精细化工有限公司 | 一种1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的制备方法 |
| CN117417333A (zh) * | 2023-10-07 | 2024-01-19 | 安徽久易农业股份有限公司 | 一种砜吡草唑的合成工艺 |
| CN120590326B (zh) * | 2025-06-05 | 2025-12-23 | 济南万兴达化工有限公司 | 一种1-甲基-3-（三氟甲基）-1h-吡唑-5-醇的制备方法 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2037488C1 (ru) * | 1989-03-02 | 1995-06-19 | Рон-Пуленк Агрошими | Производные 3-циано-5-алкокси-1-арилпиразолов и композиция на их основе |
| WO2001064651A1 (en) * | 2000-03-02 | 2001-09-07 | Bayer Cropscience S.A. | 3-thiomethylpyrazoles as pesticides |
| EP1364946A1 (en) * | 2001-02-08 | 2003-11-26 | Kumiai Chemical Industry Co., Ltd. | Isoxazoline derivative and herbicide comprising the same as active ingredient |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4317445B2 (ja) * | 2001-06-21 | 2009-08-19 | クミアイ化学工業株式会社 | イソオキサゾリン誘導体及び除草剤 |
| RS53725B1 (sr) * | 2002-08-01 | 2015-06-30 | Ihara Chemical Industry Co. Ltd. | Derivati pirazola i postupak njihovog dobijanja |
| UA78071C2 (en) * | 2002-08-07 | 2007-02-15 | Kumiai Chemical Industry Co | Herbicidal composition |
-
2004
- 2004-03-31 JP JP2004102963A patent/JP4621939B2/ja not_active Expired - Lifetime
-
2005
- 2005-03-31 CN CN2005800106359A patent/CN1938278B/zh not_active Expired - Lifetime
- 2005-03-31 CA CA2560936A patent/CA2560936C/en not_active Expired - Lifetime
- 2005-03-31 US US10/594,710 patent/US7488831B2/en active Active
- 2005-03-31 TW TW094110223A patent/TWI357899B/zh not_active IP Right Cessation
- 2005-03-31 MX MXPA06011130 patent/MX280092B/es active IP Right Grant
- 2005-03-31 NZ NZ550143A patent/NZ550143A/en not_active IP Right Cessation
- 2005-03-31 RU RU2006138241/04A patent/RU2386619C2/ru active
- 2005-03-31 UA UAA200611331A patent/UA83910C2/ru unknown
- 2005-03-31 EP EP05728918.3A patent/EP1767528B1/en not_active Expired - Lifetime
- 2005-03-31 BR BRPI0509353A patent/BRPI0509353B1/pt active IP Right Grant
- 2005-03-31 AU AU2005228017A patent/AU2005228017B2/en not_active Expired
- 2005-03-31 WO PCT/JP2005/006806 patent/WO2005095352A1/ja not_active Ceased
- 2005-03-31 ES ES05728918.3T patent/ES2508765T3/es not_active Expired - Lifetime
- 2005-03-31 PL PL05728918T patent/PL1767528T3/pl unknown
- 2005-03-31 KR KR1020067019480A patent/KR101205731B1/ko not_active Expired - Lifetime
-
2006
- 2006-09-20 CR CR8640A patent/CR8640A/es unknown
- 2006-09-21 IL IL178233A patent/IL178233A/en active IP Right Grant
- 2006-09-25 IN IN5581DE2006 patent/IN2006DE05581A/en unknown
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2037488C1 (ru) * | 1989-03-02 | 1995-06-19 | Рон-Пуленк Агрошими | Производные 3-циано-5-алкокси-1-арилпиразолов и композиция на их основе |
| WO2001064651A1 (en) * | 2000-03-02 | 2001-09-07 | Bayer Cropscience S.A. | 3-thiomethylpyrazoles as pesticides |
| EP1364946A1 (en) * | 2001-02-08 | 2003-11-26 | Kumiai Chemical Industry Co., Ltd. | Isoxazoline derivative and herbicide comprising the same as active ingredient |
Also Published As
| Publication number | Publication date |
|---|---|
| US20070185334A1 (en) | 2007-08-09 |
| BRPI0509353A (pt) | 2007-09-11 |
| JP4621939B2 (ja) | 2011-02-02 |
| MX280092B (es) | 2010-10-18 |
| ES2508765T3 (es) | 2014-10-16 |
| CA2560936A1 (en) | 2005-10-13 |
| IL178233A0 (en) | 2006-12-31 |
| CN1938278B (zh) | 2012-12-12 |
| KR20070003964A (ko) | 2007-01-05 |
| AU2005228017B2 (en) | 2010-09-30 |
| NZ550143A (en) | 2010-04-30 |
| BRPI0509353B1 (pt) | 2019-01-02 |
| EP1767528A1 (en) | 2007-03-28 |
| AU2005228017A1 (en) | 2005-10-13 |
| CN1938278A (zh) | 2007-03-28 |
| KR101205731B1 (ko) | 2012-11-28 |
| BRPI0509353A8 (pt) | 2017-09-19 |
| EP1767528B1 (en) | 2014-09-17 |
| MXPA06011130A (es) | 2007-01-25 |
| PL1767528T3 (pl) | 2015-03-31 |
| IL178233A (en) | 2014-02-27 |
| WO2005095352A1 (ja) | 2005-10-13 |
| IN2006DE05581A (enExample) | 2007-08-31 |
| RU2006138241A (ru) | 2008-05-10 |
| JP2005289824A (ja) | 2005-10-20 |
| TWI357899B (en) | 2012-02-11 |
| EP1767528A4 (en) | 2010-04-21 |
| UA83910C2 (ru) | 2008-08-26 |
| TW200536832A (en) | 2005-11-16 |
| CR8640A (es) | 2007-08-28 |
| CA2560936C (en) | 2013-01-08 |
| US7488831B2 (en) | 2009-02-10 |
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