RU2386619C2 - Способ получения 5-гидрокси-4-тиометилпиразольного соединения - Google Patents
Способ получения 5-гидрокси-4-тиометилпиразольного соединения Download PDFInfo
- Publication number
- RU2386619C2 RU2386619C2 RU2006138241/04A RU2006138241A RU2386619C2 RU 2386619 C2 RU2386619 C2 RU 2386619C2 RU 2006138241/04 A RU2006138241/04 A RU 2006138241/04A RU 2006138241 A RU2006138241 A RU 2006138241A RU 2386619 C2 RU2386619 C2 RU 2386619C2
- Authority
- RU
- Russia
- Prior art keywords
- group
- hydroxy
- compound
- mmol
- reaction
- Prior art date
Links
- 0 Cc1n[n](*)c(O)c1CS Chemical compound Cc1n[n](*)c(O)c1CS 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/18—One oxygen or sulfur atom
- C07D231/20—One oxygen atom attached in position 3 or 5
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/28—Two oxygen or sulfur atoms
- C07D231/30—Two oxygen or sulfur atoms attached in positions 3 and 5
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
- C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
- C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plural Heterocyclic Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2004-102963 | 2004-03-31 | ||
| JP2004102963A JP4621939B2 (ja) | 2004-03-31 | 2004-03-31 | ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2006138241A RU2006138241A (ru) | 2008-05-10 |
| RU2386619C2 true RU2386619C2 (ru) | 2010-04-20 |
Family
ID=35063690
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2006138241/04A RU2386619C2 (ru) | 2004-03-31 | 2005-03-31 | Способ получения 5-гидрокси-4-тиометилпиразольного соединения |
Country Status (19)
| Country | Link |
|---|---|
| US (1) | US7488831B2 (enExample) |
| EP (1) | EP1767528B1 (enExample) |
| JP (1) | JP4621939B2 (enExample) |
| KR (1) | KR101205731B1 (enExample) |
| CN (1) | CN1938278B (enExample) |
| AU (1) | AU2005228017B2 (enExample) |
| BR (1) | BRPI0509353B1 (enExample) |
| CA (1) | CA2560936C (enExample) |
| CR (1) | CR8640A (enExample) |
| ES (1) | ES2508765T3 (enExample) |
| IL (1) | IL178233A (enExample) |
| IN (1) | IN2006DE05581A (enExample) |
| MX (1) | MX280092B (enExample) |
| NZ (1) | NZ550143A (enExample) |
| PL (1) | PL1767528T3 (enExample) |
| RU (1) | RU2386619C2 (enExample) |
| TW (1) | TWI357899B (enExample) |
| UA (1) | UA83910C2 (enExample) |
| WO (1) | WO2005095352A1 (enExample) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7465805B2 (en) | 2004-10-05 | 2008-12-16 | Syngenta Limited | Isoxazoline derivatives and their use as herbicides |
| PL1829868T3 (pl) * | 2004-12-20 | 2015-03-31 | Ihara Chemical Ind Co | Sposób wytwarzania soli (4,5-dihydroizoksazol-3-ilo)tiokarboksyamidyny |
| JP2007031342A (ja) * | 2005-07-27 | 2007-02-08 | Ihara Chem Ind Co Ltd | ５−ヒドロキシ−１−アルキルピラゾール誘導体の製造方法 |
| KR101401139B1 (ko) * | 2006-02-14 | 2014-05-29 | 이하라케미칼 고교가부시키가이샤 | 5-알콕시-4-히드록시메틸피라졸 화합물의 제조방법 |
| KR20100017372A (ko) * | 2007-05-25 | 2010-02-16 | 애보트 게엠베하 운트 콤파니 카게 | 향대사성 글루타메이트 수용체 2（ｍｇｌｕ2 수용체）의 포지티브 조절자로서의 헤테로사이클릭 화합물 |
| GB0916267D0 (en) | 2009-09-16 | 2009-10-28 | Syngenta Ltd | Herbicidal compounds |
| US20120238760A1 (en) | 2009-11-26 | 2012-09-20 | Basf Se | Method for Producing 5,5-Disubstituted 2-Isoxazolines |
| CA2781404A1 (en) * | 2009-11-26 | 2011-06-03 | Basf Se | Method for producing 5,5-disubstituted 4,5-dihydroisoxazol-3-thiocarboxamidine salts |
| WO2011144549A1 (en) | 2010-05-20 | 2011-11-24 | Bayer Cropscience Ag | Method for manufacturing 1 - alkyl - 3 - difluormethyl - 5 - hydroxypyrazoles |
| CA2843415C (en) | 2011-07-29 | 2019-12-31 | University Of Saskatchewan | Polymer-based resonator antennas |
| CN103387541B (zh) * | 2012-05-10 | 2016-02-10 | 中国中化股份有限公司 | 一种取代吡唑醚类化合物的制备方法 |
| KR101901556B1 (ko) | 2015-11-16 | 2018-09-21 | 론자 리미티드 | 1-메틸-3-(트리플루오로메틸)-1h-피라졸-5-올을 제조하는 방법 |
| TW201835036A (zh) | 2017-02-27 | 2018-10-01 | 瑞士商隆薩有限公司 | 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法 |
| US10844024B1 (en) | 2017-12-27 | 2020-11-24 | Kumiai Chemical Industry Co., Ltd. | Method for producing thiocarboxamidine salt compound |
| WO2019230831A1 (ja) * | 2018-05-31 | 2019-12-05 | クミアイ化学工業株式会社 | 含フッ素ピラゾール誘導体の製造方法及びその中間体 |
| AR119524A1 (es) | 2019-07-30 | 2021-12-22 | Adama Agan Ltd | Proceso e intermediarios para la preparación de piroxasulfona |
| EP4053125B1 (en) | 2019-10-31 | 2024-12-04 | Kumiai Chemical Industry Co., Ltd. | Process for the production of a pyroxasulfone herbicide |
| CN115335375B (zh) | 2020-03-05 | 2026-05-15 | 安道麦阿甘有限公司 | 制备砜吡草唑的方法和中间体 |
| CN111574511A (zh) * | 2020-06-28 | 2020-08-25 | 安徽久易农业股份有限公司 | 一种砜吡草唑的合成方法及其应用 |
| EP4177245A1 (en) | 2020-07-10 | 2023-05-10 | Adama Agan Ltd. | Process and intermediates for the preparation of fenoxasulfone |
| CN112110912B (zh) * | 2020-07-31 | 2022-07-05 | 绍兴贝斯美化工股份有限公司 | 一种合成硫醚类中间体的方法 |
| US20240391909A1 (en) | 2021-10-29 | 2024-11-28 | Kumiai Chemical Industry Co., Ltd. | Disulfide compound, polysulfide compound, and use thereof |
| AR127776A1 (es) | 2021-11-28 | 2024-02-28 | Adama Agan Ltd | Composiciones de concentrado en suspensión de alta carga |
| CN114716428B (zh) * | 2022-05-06 | 2024-02-06 | 山东潍坊润丰化工股份有限公司 | 制备砜吡草唑中间体的方法 |
| CN115850178B (zh) * | 2022-12-28 | 2025-04-04 | 宁夏格瑞精细化工有限公司 | 一种1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的制备方法 |
| CN117417333B (zh) * | 2023-10-07 | 2026-02-17 | 安徽久易农业股份有限公司 | 一种砜吡草唑的合成工艺 |
| CN120590326B (zh) * | 2025-06-05 | 2025-12-23 | 济南万兴达化工有限公司 | 一种1-甲基-3-（三氟甲基）-1h-吡唑-5-醇的制备方法 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2037488C1 (ru) * | 1989-03-02 | 1995-06-19 | Рон-Пуленк Агрошими | Производные 3-циано-5-алкокси-1-арилпиразолов и композиция на их основе |
| WO2001064651A1 (en) * | 2000-03-02 | 2001-09-07 | Bayer Cropscience S.A. | 3-thiomethylpyrazoles as pesticides |
| EP1364946A1 (en) * | 2001-02-08 | 2003-11-26 | Kumiai Chemical Industry Co., Ltd. | Isoxazoline derivative and herbicide comprising the same as active ingredient |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1405853B1 (en) * | 2001-06-21 | 2010-11-03 | Kumiai Chemical Industry Co., Ltd. | Isoxazoline derivatives and herbicides |
| CN100548989C (zh) * | 2002-08-01 | 2009-10-14 | 庵原化学工业株式会社 | 吡唑衍生物及其生产方法 |
| UA78071C2 (en) * | 2002-08-07 | 2007-02-15 | Kumiai Chemical Industry Co | Herbicidal composition |
-
2004
- 2004-03-31 JP JP2004102963A patent/JP4621939B2/ja not_active Expired - Lifetime
-
2005
- 2005-03-31 CN CN2005800106359A patent/CN1938278B/zh not_active Expired - Lifetime
- 2005-03-31 UA UAA200611331A patent/UA83910C2/ru unknown
- 2005-03-31 TW TW094110223A patent/TWI357899B/zh not_active IP Right Cessation
- 2005-03-31 CA CA2560936A patent/CA2560936C/en not_active Expired - Lifetime
- 2005-03-31 EP EP05728918.3A patent/EP1767528B1/en not_active Expired - Lifetime
- 2005-03-31 AU AU2005228017A patent/AU2005228017B2/en not_active Expired
- 2005-03-31 BR BRPI0509353A patent/BRPI0509353B1/pt active IP Right Grant
- 2005-03-31 RU RU2006138241/04A patent/RU2386619C2/ru active
- 2005-03-31 US US10/594,710 patent/US7488831B2/en not_active Expired - Lifetime
- 2005-03-31 MX MXPA06011130 patent/MX280092B/es active IP Right Grant
- 2005-03-31 PL PL05728918T patent/PL1767528T3/pl unknown
- 2005-03-31 ES ES05728918.3T patent/ES2508765T3/es not_active Expired - Lifetime
- 2005-03-31 NZ NZ550143A patent/NZ550143A/en not_active IP Right Cessation
- 2005-03-31 WO PCT/JP2005/006806 patent/WO2005095352A1/ja not_active Ceased
- 2005-03-31 KR KR1020067019480A patent/KR101205731B1/ko not_active Expired - Lifetime
-
2006
- 2006-09-20 CR CR8640A patent/CR8640A/es unknown
- 2006-09-21 IL IL178233A patent/IL178233A/en active IP Right Grant
- 2006-09-25 IN IN5581DE2006 patent/IN2006DE05581A/en unknown
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2037488C1 (ru) * | 1989-03-02 | 1995-06-19 | Рон-Пуленк Агрошими | Производные 3-циано-5-алкокси-1-арилпиразолов и композиция на их основе |
| WO2001064651A1 (en) * | 2000-03-02 | 2001-09-07 | Bayer Cropscience S.A. | 3-thiomethylpyrazoles as pesticides |
| EP1364946A1 (en) * | 2001-02-08 | 2003-11-26 | Kumiai Chemical Industry Co., Ltd. | Isoxazoline derivative and herbicide comprising the same as active ingredient |
Also Published As
| Publication number | Publication date |
|---|---|
| US7488831B2 (en) | 2009-02-10 |
| PL1767528T3 (pl) | 2015-03-31 |
| AU2005228017A1 (en) | 2005-10-13 |
| JP2005289824A (ja) | 2005-10-20 |
| NZ550143A (en) | 2010-04-30 |
| MXPA06011130A (es) | 2007-01-25 |
| TW200536832A (en) | 2005-11-16 |
| EP1767528A4 (en) | 2010-04-21 |
| WO2005095352A1 (ja) | 2005-10-13 |
| BRPI0509353B1 (pt) | 2019-01-02 |
| EP1767528B1 (en) | 2014-09-17 |
| RU2006138241A (ru) | 2008-05-10 |
| US20070185334A1 (en) | 2007-08-09 |
| JP4621939B2 (ja) | 2011-02-02 |
| KR20070003964A (ko) | 2007-01-05 |
| AU2005228017B2 (en) | 2010-09-30 |
| MX280092B (es) | 2010-10-18 |
| TWI357899B (en) | 2012-02-11 |
| CA2560936A1 (en) | 2005-10-13 |
| KR101205731B1 (ko) | 2012-11-28 |
| CA2560936C (en) | 2013-01-08 |
| BRPI0509353A (pt) | 2007-09-11 |
| IN2006DE05581A (enExample) | 2007-08-31 |
| CN1938278B (zh) | 2012-12-12 |
| CN1938278A (zh) | 2007-03-28 |
| IL178233A (en) | 2014-02-27 |
| UA83910C2 (ru) | 2008-08-26 |
| EP1767528A1 (en) | 2007-03-28 |
| CR8640A (es) | 2007-08-28 |
| ES2508765T3 (es) | 2014-10-16 |
| IL178233A0 (en) | 2006-12-31 |
| BRPI0509353A8 (pt) | 2017-09-19 |
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