CN1938278B - 5-羟基-4-硫甲基吡唑化合物的制备方法 - Google Patents

5-羟基-4-硫甲基吡唑化合物的制备方法 Download PDF

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Publication number
CN1938278B
CN1938278B CN2005800106359A CN200580010635A CN1938278B CN 1938278 B CN1938278 B CN 1938278B CN 2005800106359 A CN2005800106359 A CN 2005800106359A CN 200580010635 A CN200580010635 A CN 200580010635A CN 1938278 B CN1938278 B CN 1938278B
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China
Prior art keywords
hydroxyl
branched
carbonyl
straight
methyl
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Expired - Lifetime
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CN2005800106359A
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Chinese (zh)
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CN1938278A (zh
Inventor
内田幸生
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Kumiai Chemical Industry Co Ltd
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Ihara Chemical Industry Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/28—Two oxygen or sulfur atoms
    • C07D231/30—Two oxygen or sulfur atoms attached in positions 3 and 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN2005800106359A 2004-03-31 2005-03-31 5-羟基-4-硫甲基吡唑化合物的制备方法 Expired - Lifetime CN1938278B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP102963/2004 2004-03-31
JP2004102963A JP4621939B2 (ja) 2004-03-31 2004-03-31 ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法
PCT/JP2005/006806 WO2005095352A1 (ja) 2004-03-31 2005-03-31 ５－ヒドロキシ－４－チオメチルピラゾール化合物の製造方法

Publications (2)

Publication Number Publication Date
CN1938278A CN1938278A (zh) 2007-03-28
CN1938278B true CN1938278B (zh) 2012-12-12

Family

ID=35063690

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2005800106359A Expired - Lifetime CN1938278B (zh) 2004-03-31 2005-03-31 5-羟基-4-硫甲基吡唑化合物的制备方法

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Country Link
US (1) US7488831B2 (enExample)
EP (1) EP1767528B1 (enExample)
JP (1) JP4621939B2 (enExample)
KR (1) KR101205731B1 (enExample)
CN (1) CN1938278B (enExample)
AU (1) AU2005228017B2 (enExample)
BR (1) BRPI0509353B1 (enExample)
CA (1) CA2560936C (enExample)
CR (1) CR8640A (enExample)
ES (1) ES2508765T3 (enExample)
IL (1) IL178233A (enExample)
IN (1) IN2006DE05581A (enExample)
MX (1) MX280092B (enExample)
NZ (1) NZ550143A (enExample)
PL (1) PL1767528T3 (enExample)
RU (1) RU2386619C2 (enExample)
TW (1) TWI357899B (enExample)
UA (1) UA83910C2 (enExample)
WO (1) WO2005095352A1 (enExample)

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US7465805B2 (en) 2004-10-05 2008-12-16 Syngenta Limited Isoxazoline derivatives and their use as herbicides
PL1829868T3 (pl) * 2004-12-20 2015-03-31 Ihara Chemical Ind Co Sposób wytwarzania soli (4,5-dihydroizoksazol-3-ilo)tiokarboksyamidyny
JP2007031342A (ja) * 2005-07-27 2007-02-08 Ihara Chem Ind Co Ltd ５−ヒドロキシ−１−アルキルピラゾール誘導体の製造方法
KR101401139B1 (ko) * 2006-02-14 2014-05-29 이하라케미칼 고교가부시키가이샤 5-알콕시-4-히드록시메틸피라졸 화합물의 제조방법
KR20100017372A (ko) * 2007-05-25 2010-02-16 애보트 게엠베하 운트 콤파니 카게 향대사성 글루타메이트 수용체 2（ｍｇｌｕ2 수용체）의 포지티브 조절자로서의 헤테로사이클릭 화합물
GB0916267D0 (en) 2009-09-16 2009-10-28 Syngenta Ltd Herbicidal compounds
US20120238760A1 (en) 2009-11-26 2012-09-20 Basf Se Method for Producing 5,5-Disubstituted 2-Isoxazolines
CA2781404A1 (en) * 2009-11-26 2011-06-03 Basf Se Method for producing 5,5-disubstituted 4,5-dihydroisoxazol-3-thiocarboxamidine salts
WO2011144549A1 (en) 2010-05-20 2011-11-24 Bayer Cropscience Ag Method for manufacturing 1 - alkyl - 3 - difluormethyl - 5 - hydroxypyrazoles
CA2843415C (en) 2011-07-29 2019-12-31 University Of Saskatchewan Polymer-based resonator antennas
CN103387541B (zh) * 2012-05-10 2016-02-10 中国中化股份有限公司 一种取代吡唑醚类化合物的制备方法
KR101901556B1 (ko) 2015-11-16 2018-09-21 론자 리미티드 1-메틸-3-(트리플루오로메틸)-1h-피라졸-5-올을 제조하는 방법
TW201835036A (zh) 2017-02-27 2018-10-01 瑞士商隆薩有限公司 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法
US10844024B1 (en) 2017-12-27 2020-11-24 Kumiai Chemical Industry Co., Ltd. Method for producing thiocarboxamidine salt compound
WO2019230831A1 (ja) * 2018-05-31 2019-12-05 クミアイ化学工業株式会社 含フッ素ピラゾール誘導体の製造方法及びその中間体
AR119524A1 (es) 2019-07-30 2021-12-22 Adama Agan Ltd Proceso e intermediarios para la preparación de piroxasulfona
EP4053125B1 (en) 2019-10-31 2024-12-04 Kumiai Chemical Industry Co., Ltd. Process for the production of a pyroxasulfone herbicide
CN115335375B (zh) 2020-03-05 2026-05-15 安道麦阿甘有限公司 制备砜吡草唑的方法和中间体
CN111574511A (zh) * 2020-06-28 2020-08-25 安徽久易农业股份有限公司 一种砜吡草唑的合成方法及其应用
EP4177245A1 (en) 2020-07-10 2023-05-10 Adama Agan Ltd. Process and intermediates for the preparation of fenoxasulfone
CN112110912B (zh) * 2020-07-31 2022-07-05 绍兴贝斯美化工股份有限公司 一种合成硫醚类中间体的方法
US20240391909A1 (en) 2021-10-29 2024-11-28 Kumiai Chemical Industry Co., Ltd. Disulfide compound, polysulfide compound, and use thereof
AR127776A1 (es) 2021-11-28 2024-02-28 Adama Agan Ltd Composiciones de concentrado en suspensión de alta carga
CN114716428B (zh) * 2022-05-06 2024-02-06 山东潍坊润丰化工股份有限公司 制备砜吡草唑中间体的方法
CN115850178B (zh) * 2022-12-28 2025-04-04 宁夏格瑞精细化工有限公司 一种1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的制备方法
CN117417333B (zh) * 2023-10-07 2026-02-17 安徽久易农业股份有限公司 一种砜吡草唑的合成工艺
CN120590326B (zh) * 2025-06-05 2025-12-23 济南万兴达化工有限公司 一种1-甲基-3-（三氟甲基）-1h-吡唑-5-醇的制备方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001064651A1 (en) * 2000-03-02 2001-09-07 Bayer Cropscience S.A. 3-thiomethylpyrazoles as pesticides
WO2003000686A1 (en) * 2001-06-21 2003-01-03 Kumiai Chemical Industry Co., Ltd. Isoxazoline derivatives and herbicides
WO2004014138A1 (ja) * 2002-08-07 2004-02-19 Kumiai Chemical Industry Co., Ltd. 除草剤組成物
CN1491217A (zh) * 2001-02-08 2004-04-21 ��Ԩ��ѧ��ҵ��ʽ���� 异噁唑啉衍生物和含有它们作为活性组分的除草剂
CN1678588A (zh) * 2002-08-01 2005-10-05 庵原化学工业株式会社 吡唑衍生物及其生产方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4918085A (en) * 1989-03-02 1990-04-17 Rhone-Poulenc Ag Company Pesticidal 3-cyano-5-alkoxy-1-arylpyrazoles, compositions and use

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001064651A1 (en) * 2000-03-02 2001-09-07 Bayer Cropscience S.A. 3-thiomethylpyrazoles as pesticides
CN1491217A (zh) * 2001-02-08 2004-04-21 ��Ԩ��ѧ��ҵ��ʽ���� 异噁唑啉衍生物和含有它们作为活性组分的除草剂
WO2003000686A1 (en) * 2001-06-21 2003-01-03 Kumiai Chemical Industry Co., Ltd. Isoxazoline derivatives and herbicides
CN1678588A (zh) * 2002-08-01 2005-10-05 庵原化学工业株式会社 吡唑衍生物及其生产方法
WO2004014138A1 (ja) * 2002-08-07 2004-02-19 Kumiai Chemical Industry Co., Ltd. 除草剤組成物

Also Published As

Publication number Publication date
US7488831B2 (en) 2009-02-10
PL1767528T3 (pl) 2015-03-31
AU2005228017A1 (en) 2005-10-13
JP2005289824A (ja) 2005-10-20
NZ550143A (en) 2010-04-30
MXPA06011130A (es) 2007-01-25
RU2386619C2 (ru) 2010-04-20
TW200536832A (en) 2005-11-16
EP1767528A4 (en) 2010-04-21
WO2005095352A1 (ja) 2005-10-13
BRPI0509353B1 (pt) 2019-01-02
EP1767528B1 (en) 2014-09-17
RU2006138241A (ru) 2008-05-10
US20070185334A1 (en) 2007-08-09
JP4621939B2 (ja) 2011-02-02
KR20070003964A (ko) 2007-01-05
AU2005228017B2 (en) 2010-09-30
MX280092B (es) 2010-10-18
TWI357899B (en) 2012-02-11
CA2560936A1 (en) 2005-10-13
KR101205731B1 (ko) 2012-11-28
CA2560936C (en) 2013-01-08
BRPI0509353A (pt) 2007-09-11
IN2006DE05581A (enExample) 2007-08-31
CN1938278A (zh) 2007-03-28
IL178233A (en) 2014-02-27
UA83910C2 (ru) 2008-08-26
EP1767528A1 (en) 2007-03-28
CR8640A (es) 2007-08-28
ES2508765T3 (es) 2014-10-16
IL178233A0 (en) 2006-12-31
BRPI0509353A8 (pt) 2017-09-19

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SE01 Entry into force of request for substantive examination
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GR01 Patent grant
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Effective date of registration: 20210203

Address after: Tokyo, Japan

Patentee after: Kumiai Chemical Industry Co.,Ltd.

Address before: Tokyo, Japan

Patentee before: Ihara Chemical Industry Co.,Ltd.

TR01 Transfer of patent right
CX01 Expiry of patent term

Granted publication date: 20121212

CX01 Expiry of patent term