CN1938278B - 5-羟基-4-硫甲基吡唑化合物的制备方法 - Google Patents

5-羟基-4-硫甲基吡唑化合物的制备方法 Download PDF

Info

Publication number
CN1938278B
CN1938278B CN2005800106359A CN200580010635A CN1938278B CN 1938278 B CN1938278 B CN 1938278B CN 2005800106359 A CN2005800106359 A CN 2005800106359A CN 200580010635 A CN200580010635 A CN 200580010635A CN 1938278 B CN1938278 B CN 1938278B
Authority
CN
China
Prior art keywords
hydroxyl
branched
carbonyl
straight
methyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN2005800106359A
Other languages
English (en)
Chinese (zh)
Other versions
CN1938278A (zh
Inventor
内田幸生
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kumiai Chemical Industry Co Ltd
Original Assignee
Ihara Chemical Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=35063690&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CN1938278(B) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Ihara Chemical Industry Co Ltd filed Critical Ihara Chemical Industry Co Ltd
Publication of CN1938278A publication Critical patent/CN1938278A/zh
Application granted granted Critical
Publication of CN1938278B publication Critical patent/CN1938278B/zh
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/28—Two oxygen or sulfur atoms
    • C07D231/30—Two oxygen or sulfur atoms attached in positions 3 and 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN2005800106359A 2004-03-31 2005-03-31 5-羟基-4-硫甲基吡唑化合物的制备方法 Expired - Lifetime CN1938278B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP102963/2004 2004-03-31
JP2004102963A JP4621939B2 (ja) 2004-03-31 2004-03-31 ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法
PCT/JP2005/006806 WO2005095352A1 (ja) 2004-03-31 2005-03-31 ５－ヒドロキシ－４－チオメチルピラゾール化合物の製造方法

Publications (2)

Publication Number Publication Date
CN1938278A CN1938278A (zh) 2007-03-28
CN1938278B true CN1938278B (zh) 2012-12-12

Family

ID=35063690

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2005800106359A Expired - Lifetime CN1938278B (zh) 2004-03-31 2005-03-31 5-羟基-4-硫甲基吡唑化合物的制备方法

Country Status (19)

Country Link
US (1) US7488831B2 (enExample)
EP (1) EP1767528B1 (enExample)
JP (1) JP4621939B2 (enExample)
KR (1) KR101205731B1 (enExample)
CN (1) CN1938278B (enExample)
AU (1) AU2005228017B2 (enExample)
BR (1) BRPI0509353B1 (enExample)
CA (1) CA2560936C (enExample)
CR (1) CR8640A (enExample)
ES (1) ES2508765T3 (enExample)
IL (1) IL178233A (enExample)
IN (1) IN2006DE05581A (enExample)
MX (1) MX280092B (enExample)
NZ (1) NZ550143A (enExample)
PL (1) PL1767528T3 (enExample)
RU (1) RU2386619C2 (enExample)
TW (1) TWI357899B (enExample)
UA (1) UA83910C2 (enExample)
WO (1) WO2005095352A1 (enExample)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2333977T3 (es) 2004-10-05 2010-03-03 Syngenta Limited Derivados de isoxazolina y su uso como herbicidas.
US7714142B2 (en) * 2004-12-20 2010-05-11 Ihara Chemical Industry Co., Ltd. Process for production of (4,5-dihydroisoxazol-3-Y) thio-carboxamidine salts
JP2007031342A (ja) * 2005-07-27 2007-02-08 Ihara Chem Ind Co Ltd ５−ヒドロキシ−１−アルキルピラゾール誘導体の製造方法
KR101401139B1 (ko) * 2006-02-14 2014-05-29 이하라케미칼 고교가부시키가이샤 5-알콕시-4-히드록시메틸피라졸 화합물의 제조방법
RU2479577C2 (ru) * 2007-05-25 2013-04-20 Эбботт Гмбх Унд Ко.Кг Гетероциклические соединения в качестве положительных модуляторов метаботропного глутаматного рецептора 2 (рецептора mglu2)
GB0916267D0 (en) 2009-09-16 2009-10-28 Syngenta Ltd Herbicidal compounds
BR112012012584B1 (pt) * 2009-11-26 2017-10-31 Basf Se A process for preparing 5,5-disubstituted 4,5-dihydroisoxazol-3-thiocarboxamidine salts
EP2504321B1 (de) 2009-11-26 2014-04-16 Basf Se Verfahren zur herstellung 5,5-disubstituierter 2-isoxazoline
WO2011144549A1 (en) * 2010-05-20 2011-11-24 Bayer Cropscience Ag Method for manufacturing 1 - alkyl - 3 - difluormethyl - 5 - hydroxypyrazoles
EP2737575B1 (en) 2011-07-29 2024-05-01 University of Saskatchewan Polymer-based resonator antennas
CN103387541B (zh) * 2012-05-10 2016-02-10 中国中化股份有限公司 一种取代吡唑醚类化合物的制备方法
WO2017084995A1 (en) 2015-11-16 2017-05-26 Lonza Ltd Method for preparation of 1-methyl-3-(trifluoromethyl)-1hpyrazol-5-ol
TW201835036A (zh) 2017-02-27 2018-10-01 瑞士商隆薩有限公司 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法
BR112020012995B1 (pt) * 2017-12-27 2021-08-24 Kumiai Chemical Industry Co., Ltd Processo para produzir um composto de sal de (4,5-dihidroisoxasol-3-il)tiocarboxamidina
WO2019230831A1 (ja) * 2018-05-31 2019-12-05 クミアイ化学工業株式会社 含フッ素ピラゾール誘導体の製造方法及びその中間体
CN114450270B (zh) 2019-07-30 2025-05-06 安道麦阿甘有限公司 砜吡草唑的制备方法和中间体
IL292532B1 (en) 2019-10-31 2024-04-01 Kumiai Chemical Industry Co Process for producing herbicide and intermediate thereof
BR112022017794A2 (pt) 2020-03-05 2022-10-25 Adama Agan Ltd Processo e intermediários para a preparação de piroxassulfona
CN111574511A (zh) * 2020-06-28 2020-08-25 安徽久易农业股份有限公司 一种砜吡草唑的合成方法及其应用
EP4177252A3 (en) 2020-07-10 2023-08-09 Adama Agan Ltd. Process and intermediates for the preparation of pyroxasulfone, fenoxasulfone and various sulfone analogs of 5,5-dimethyl-4h-1,2-oxazole
CN112110912B (zh) * 2020-07-31 2022-07-05 绍兴贝斯美化工股份有限公司 一种合成硫醚类中间体的方法
TW202334128A (zh) 2021-10-29 2023-09-01 日商組合化學工業股份有限公司 二硫化物化合物、多硫化物化合物及其用途
AR127776A1 (es) 2021-11-28 2024-02-28 Adama Agan Ltd Composiciones de concentrado en suspensión de alta carga
CN114716428B (zh) * 2022-05-06 2024-02-06 山东潍坊润丰化工股份有限公司 制备砜吡草唑中间体的方法
CN115850178B (zh) * 2022-12-28 2025-04-04 宁夏格瑞精细化工有限公司 一种1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的制备方法
CN117417333A (zh) * 2023-10-07 2024-01-19 安徽久易农业股份有限公司 一种砜吡草唑的合成工艺
CN120590326B (zh) * 2025-06-05 2025-12-23 济南万兴达化工有限公司 一种1-甲基-3-（三氟甲基）-1h-吡唑-5-醇的制备方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001064651A1 (en) * 2000-03-02 2001-09-07 Bayer Cropscience S.A. 3-thiomethylpyrazoles as pesticides
WO2003000686A1 (en) * 2001-06-21 2003-01-03 Kumiai Chemical Industry Co., Ltd. Isoxazoline derivatives and herbicides
WO2004014138A1 (ja) * 2002-08-07 2004-02-19 Kumiai Chemical Industry Co., Ltd. 除草剤組成物
CN1491217A (zh) * 2001-02-08 2004-04-21 ��Ԩ��ѧ��ҵ��ʽ���� 异噁唑啉衍生物和含有它们作为活性组分的除草剂
CN1678588A (zh) * 2002-08-01 2005-10-05 庵原化学工业株式会社 吡唑衍生物及其生产方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4918085A (en) * 1989-03-02 1990-04-17 Rhone-Poulenc Ag Company Pesticidal 3-cyano-5-alkoxy-1-arylpyrazoles, compositions and use

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001064651A1 (en) * 2000-03-02 2001-09-07 Bayer Cropscience S.A. 3-thiomethylpyrazoles as pesticides
CN1491217A (zh) * 2001-02-08 2004-04-21 ��Ԩ��ѧ��ҵ��ʽ���� 异噁唑啉衍生物和含有它们作为活性组分的除草剂
WO2003000686A1 (en) * 2001-06-21 2003-01-03 Kumiai Chemical Industry Co., Ltd. Isoxazoline derivatives and herbicides
CN1678588A (zh) * 2002-08-01 2005-10-05 庵原化学工业株式会社 吡唑衍生物及其生产方法
WO2004014138A1 (ja) * 2002-08-07 2004-02-19 Kumiai Chemical Industry Co., Ltd. 除草剤組成物

Also Published As

Publication number Publication date
US20070185334A1 (en) 2007-08-09
BRPI0509353A (pt) 2007-09-11
JP4621939B2 (ja) 2011-02-02
MX280092B (es) 2010-10-18
ES2508765T3 (es) 2014-10-16
CA2560936A1 (en) 2005-10-13
IL178233A0 (en) 2006-12-31
KR20070003964A (ko) 2007-01-05
AU2005228017B2 (en) 2010-09-30
NZ550143A (en) 2010-04-30
BRPI0509353B1 (pt) 2019-01-02
EP1767528A1 (en) 2007-03-28
AU2005228017A1 (en) 2005-10-13
CN1938278A (zh) 2007-03-28
KR101205731B1 (ko) 2012-11-28
BRPI0509353A8 (pt) 2017-09-19
RU2386619C2 (ru) 2010-04-20
EP1767528B1 (en) 2014-09-17
MXPA06011130A (es) 2007-01-25
PL1767528T3 (pl) 2015-03-31
IL178233A (en) 2014-02-27
WO2005095352A1 (ja) 2005-10-13
IN2006DE05581A (enExample) 2007-08-31
RU2006138241A (ru) 2008-05-10
JP2005289824A (ja) 2005-10-20
TWI357899B (en) 2012-02-11
EP1767528A4 (en) 2010-04-21
UA83910C2 (ru) 2008-08-26
TW200536832A (en) 2005-11-16
CR8640A (es) 2007-08-28
CA2560936C (en) 2013-01-08
US7488831B2 (en) 2009-02-10

Similar Documents

Publication Publication Date Title
CN1938278B (zh) 5-羟基-4-硫甲基吡唑化合物的制备方法
JP5373788B2 (ja) Ｆｘｒを調節するための化合物および方法
KR20010014002A (ko) Ｘａ 인자 억제제인 신규한 구아니딘 유사체
WO2007092751A2 (en) Compounds and methods for modulating fx-receptors
PL216029B1 (pl) Sposób wytwarzania 3-chlorowco-4,5-dihydro-1H-pirazoli
Schlosser et al. Switchable Reactivity: The Site‐Selective Functionalization of Trifluoromethyl‐Substituted Pyrazoles
JP5052495B2 (ja) ５−アルコキシ−４−ヒドロキシメチルピラゾール化合物の製造方法
CN107235967B (zh) 抗肿瘤药物替加氟的合成工艺
CN106146518A (zh) 一种布鲁顿酪氨酸激酶抑制剂中间体及其制备方法
JP2007246396A (ja) ５−ジフルオロメトキシ−４−チオメチルピラゾール化合物の製造方法
JP2008509182A5 (enExample)
CN101921231A (zh) 氟虫腈磺酰胺衍生物及其制备方法
Li et al. Regioselective [3+ 2] cycloaddition of diazo reagents and internal alkynes: Accessing regiosomers of highly substituted trifluoromethylpyrazoles
CN104628647A (zh) 3-甲基-1-(3,4-二甲基苯基)-2-吡唑啉-5-酮的制备方法
EP4378929A1 (en) Synthesis of aromatic boronic acids
JP4320477B2 (ja) トリアゾール化合物
JP5406581B2 (ja) アントラニルアミド系化合物の製造方法
JP4194984B2 (ja) フェニルナフチルイミダゾール化合物
HRP20000564A2 (en) Process for making 5-lipoxygenase inhibitors having varied heterocyclic ring systems
JPS62246554A (ja) １，２，４−トリアゾリン−５−オン誘導体及びその製造方法
HU214633B (hu) Eljárás szalicilsav-származékok előállítására
MX2008010004A (en) Compounds and methods for modulating fx-receptors
JP2014037389A (ja) エステル化合物の製造方法およびアゾリルメチルシクロペンタノール化合物の製造方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
TR01 Transfer of patent right

Effective date of registration: 20210203

Address after: Tokyo, Japan

Patentee after: Kumiai Chemical Industry Co.,Ltd.

Address before: Tokyo, Japan

Patentee before: Ihara Chemical Industry Co.,Ltd.

TR01 Transfer of patent right
CX01 Expiry of patent term

Granted publication date: 20121212

CX01 Expiry of patent term