JP4621939B2 - ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法 - Google Patents

５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法 Download PDF

Info

Publication number
JP4621939B2
JP4621939B2 JP2004102963A JP2004102963A JP4621939B2 JP 4621939 B2 JP4621939 B2 JP 4621939B2 JP 2004102963 A JP2004102963 A JP 2004102963A JP 2004102963 A JP2004102963 A JP 2004102963A JP 4621939 B2 JP4621939 B2 JP 4621939B2
Authority
JP
Japan
Prior art keywords
group
hydroxy
mmol
branched
linear
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP2004102963A
Other languages
English (en)
Japanese (ja)
Other versions
JP2005289824A (ja
Inventor
幸生 内田
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ihara Chemical Industry Co Ltd
Original Assignee
Ihara Chemical Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=35063690&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=JP4621939(B2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Ihara Chemical Industry Co Ltd filed Critical Ihara Chemical Industry Co Ltd
Priority to JP2004102963A priority Critical patent/JP4621939B2/ja
Priority to TW094110223A priority patent/TWI357899B/zh
Priority to MXPA06011130 priority patent/MX280092B/es
Priority to CA2560936A priority patent/CA2560936C/en
Priority to PCT/JP2005/006806 priority patent/WO2005095352A1/ja
Priority to KR1020067019480A priority patent/KR101205731B1/ko
Priority to PL05728918T priority patent/PL1767528T3/pl
Priority to EP05728918.3A priority patent/EP1767528B1/en
Priority to CN2005800106359A priority patent/CN1938278B/zh
Priority to US10/594,710 priority patent/US7488831B2/en
Priority to NZ550143A priority patent/NZ550143A/en
Priority to ES05728918.3T priority patent/ES2508765T3/es
Priority to AU2005228017A priority patent/AU2005228017B2/en
Priority to BRPI0509353A priority patent/BRPI0509353B1/pt
Priority to RU2006138241/04A priority patent/RU2386619C2/ru
Priority to UAA200611331A priority patent/UA83910C2/ru
Publication of JP2005289824A publication Critical patent/JP2005289824A/ja
Priority to CR8640A priority patent/CR8640A/es
Priority to IL178233A priority patent/IL178233A/en
Priority to IN5581DE2006 priority patent/IN2006DE05581A/en
Publication of JP4621939B2 publication Critical patent/JP4621939B2/ja
Application granted granted Critical
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/28—Two oxygen or sulfur atoms
    • C07D231/30—Two oxygen or sulfur atoms attached in positions 3 and 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2004102963A 2004-03-31 2004-03-31 ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法 Expired - Lifetime JP4621939B2 (ja)

Priority Applications (19)

Application Number Priority Date Filing Date Title
JP2004102963A JP4621939B2 (ja) 2004-03-31 2004-03-31 ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法
NZ550143A NZ550143A (en) 2004-03-31 2005-03-31 Process for producing 5-hydroxy-4-thiomethylpyrazole compound
AU2005228017A AU2005228017B2 (en) 2004-03-31 2005-03-31 Process for producing 5-hydroxy-4-thiomethylpyrazole compound
CA2560936A CA2560936C (en) 2004-03-31 2005-03-31 Process for producing 5-hydroxy-4-thiomethylpyrazole compound
PCT/JP2005/006806 WO2005095352A1 (ja) 2004-03-31 2005-03-31 ５－ヒドロキシ－４－チオメチルピラゾール化合物の製造方法
KR1020067019480A KR101205731B1 (ko) 2004-03-31 2005-03-31 5-히드록시-4-티오메틸피라졸 화합물의 제조 방법
PL05728918T PL1767528T3 (pl) 2004-03-31 2005-03-31 Sposób wytwarzania związku 5-hydroksy-4-tiometylopirazolowego
EP05728918.3A EP1767528B1 (en) 2004-03-31 2005-03-31 Process for producing 5-hydroxy-4-thiomethylpyrazole compound
CN2005800106359A CN1938278B (zh) 2004-03-31 2005-03-31 5-羟基-4-硫甲基吡唑化合物的制备方法
US10/594,710 US7488831B2 (en) 2004-03-31 2005-03-31 Process for producing 5-hydroxy-4-thiomethylpyrazole compound
TW094110223A TWI357899B (en) 2004-03-31 2005-03-31 Process for producing 5-hydroxy-4-thiomethylpyrazo
ES05728918.3T ES2508765T3 (es) 2004-03-31 2005-03-31 Procedimiento para producir un compuesto de 5-hidroxi-4-tiometilpirazol
MXPA06011130 MX280092B (es) 2004-03-31 2005-03-31 Proceso para producir un compuesto de 5 - hidroxi - 4 - tiometilpirazol.
BRPI0509353A BRPI0509353B1 (pt) 2004-03-31 2005-03-31 processo para a produção de um composto de 5-hidróxi-4-tiometilpirazol
RU2006138241/04A RU2386619C2 (ru) 2004-03-31 2005-03-31 Способ получения 5-гидрокси-4-тиометилпиразольного соединения
UAA200611331A UA83910C2 (ru) 2004-03-31 2005-03-31 Способ получения 5-гидрокси-4-тиометилпиразольного соединения
CR8640A CR8640A (es) 2004-03-31 2006-09-20 Proceso para producir un compuesto de 5-hidroxi-4-tiometilpirazol
IL178233A IL178233A (en) 2004-03-31 2006-09-21 Process for making 5-hydroxy-4-thiomethylpyrazole
IN5581DE2006 IN2006DE05581A (enExample) 2004-03-31 2006-09-25

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2004102963A JP4621939B2 (ja) 2004-03-31 2004-03-31 ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法

Publications (2)

Publication Number Publication Date
JP2005289824A JP2005289824A (ja) 2005-10-20
JP4621939B2 true JP4621939B2 (ja) 2011-02-02

Family

ID=35063690

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2004102963A Expired - Lifetime JP4621939B2 (ja) 2004-03-31 2004-03-31 ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法

Country Status (19)

Country Link
US (1) US7488831B2 (enExample)
EP (1) EP1767528B1 (enExample)
JP (1) JP4621939B2 (enExample)
KR (1) KR101205731B1 (enExample)
CN (1) CN1938278B (enExample)
AU (1) AU2005228017B2 (enExample)
BR (1) BRPI0509353B1 (enExample)
CA (1) CA2560936C (enExample)
CR (1) CR8640A (enExample)
ES (1) ES2508765T3 (enExample)
IL (1) IL178233A (enExample)
IN (1) IN2006DE05581A (enExample)
MX (1) MX280092B (enExample)
NZ (1) NZ550143A (enExample)
PL (1) PL1767528T3 (enExample)
RU (1) RU2386619C2 (enExample)
TW (1) TWI357899B (enExample)
UA (1) UA83910C2 (enExample)
WO (1) WO2005095352A1 (enExample)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7465805B2 (en) 2004-10-05 2008-12-16 Syngenta Limited Isoxazoline derivatives and their use as herbicides
PL1829868T3 (pl) * 2004-12-20 2015-03-31 Ihara Chemical Ind Co Sposób wytwarzania soli (4,5-dihydroizoksazol-3-ilo)tiokarboksyamidyny
JP2007031342A (ja) * 2005-07-27 2007-02-08 Ihara Chem Ind Co Ltd ５−ヒドロキシ−１−アルキルピラゾール誘導体の製造方法
KR101401139B1 (ko) * 2006-02-14 2014-05-29 이하라케미칼 고교가부시키가이샤 5-알콕시-4-히드록시메틸피라졸 화합물의 제조방법
KR20100017372A (ko) * 2007-05-25 2010-02-16 애보트 게엠베하 운트 콤파니 카게 향대사성 글루타메이트 수용체 2（ｍｇｌｕ2 수용체）의 포지티브 조절자로서의 헤테로사이클릭 화합물
GB0916267D0 (en) 2009-09-16 2009-10-28 Syngenta Ltd Herbicidal compounds
US20120238760A1 (en) 2009-11-26 2012-09-20 Basf Se Method for Producing 5,5-Disubstituted 2-Isoxazolines
CA2781404A1 (en) * 2009-11-26 2011-06-03 Basf Se Method for producing 5,5-disubstituted 4,5-dihydroisoxazol-3-thiocarboxamidine salts
WO2011144549A1 (en) 2010-05-20 2011-11-24 Bayer Cropscience Ag Method for manufacturing 1 - alkyl - 3 - difluormethyl - 5 - hydroxypyrazoles
CA2843415C (en) 2011-07-29 2019-12-31 University Of Saskatchewan Polymer-based resonator antennas
CN103387541B (zh) * 2012-05-10 2016-02-10 中国中化股份有限公司 一种取代吡唑醚类化合物的制备方法
KR101901556B1 (ko) 2015-11-16 2018-09-21 론자 리미티드 1-메틸-3-(트리플루오로메틸)-1h-피라졸-5-올을 제조하는 방법
TW201835036A (zh) 2017-02-27 2018-10-01 瑞士商隆薩有限公司 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法
US10844024B1 (en) 2017-12-27 2020-11-24 Kumiai Chemical Industry Co., Ltd. Method for producing thiocarboxamidine salt compound
WO2019230831A1 (ja) * 2018-05-31 2019-12-05 クミアイ化学工業株式会社 含フッ素ピラゾール誘導体の製造方法及びその中間体
AR119524A1 (es) 2019-07-30 2021-12-22 Adama Agan Ltd Proceso e intermediarios para la preparación de piroxasulfona
EP4053125B1 (en) 2019-10-31 2024-12-04 Kumiai Chemical Industry Co., Ltd. Process for the production of a pyroxasulfone herbicide
CN115335375B (zh) 2020-03-05 2026-05-15 安道麦阿甘有限公司 制备砜吡草唑的方法和中间体
CN111574511A (zh) * 2020-06-28 2020-08-25 安徽久易农业股份有限公司 一种砜吡草唑的合成方法及其应用
EP4177245A1 (en) 2020-07-10 2023-05-10 Adama Agan Ltd. Process and intermediates for the preparation of fenoxasulfone
CN112110912B (zh) * 2020-07-31 2022-07-05 绍兴贝斯美化工股份有限公司 一种合成硫醚类中间体的方法
US20240391909A1 (en) 2021-10-29 2024-11-28 Kumiai Chemical Industry Co., Ltd. Disulfide compound, polysulfide compound, and use thereof
AR127776A1 (es) 2021-11-28 2024-02-28 Adama Agan Ltd Composiciones de concentrado en suspensión de alta carga
CN114716428B (zh) * 2022-05-06 2024-02-06 山东潍坊润丰化工股份有限公司 制备砜吡草唑中间体的方法
CN115850178B (zh) * 2022-12-28 2025-04-04 宁夏格瑞精细化工有限公司 一种1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的制备方法
CN117417333B (zh) * 2023-10-07 2026-02-17 安徽久易农业股份有限公司 一种砜吡草唑的合成工艺
CN120590326B (zh) * 2025-06-05 2025-12-23 济南万兴达化工有限公司 一种1-甲基-3-（三氟甲基）-1h-吡唑-5-醇的制备方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4918085A (en) * 1989-03-02 1990-04-17 Rhone-Poulenc Ag Company Pesticidal 3-cyano-5-alkoxy-1-arylpyrazoles, compositions and use
CO5221057A1 (es) * 2000-03-02 2002-11-28 Aventis Cropscience Sa Componentes y composiciones plagicidas
JP4465133B2 (ja) * 2001-02-08 2010-05-19 クミアイ化学工業株式会社 イソオキサゾリン誘導体及びこれを有効成分とする除草剤
EP1405853B1 (en) * 2001-06-21 2010-11-03 Kumiai Chemical Industry Co., Ltd. Isoxazoline derivatives and herbicides
CN100548989C (zh) * 2002-08-01 2009-10-14 庵原化学工业株式会社 吡唑衍生物及其生产方法
UA78071C2 (en) * 2002-08-07 2007-02-15 Kumiai Chemical Industry Co Herbicidal composition

Also Published As

Publication number Publication date
US7488831B2 (en) 2009-02-10
PL1767528T3 (pl) 2015-03-31
AU2005228017A1 (en) 2005-10-13
JP2005289824A (ja) 2005-10-20
NZ550143A (en) 2010-04-30
MXPA06011130A (es) 2007-01-25
RU2386619C2 (ru) 2010-04-20
TW200536832A (en) 2005-11-16
EP1767528A4 (en) 2010-04-21
WO2005095352A1 (ja) 2005-10-13
BRPI0509353B1 (pt) 2019-01-02
EP1767528B1 (en) 2014-09-17
RU2006138241A (ru) 2008-05-10
US20070185334A1 (en) 2007-08-09
KR20070003964A (ko) 2007-01-05
AU2005228017B2 (en) 2010-09-30
MX280092B (es) 2010-10-18
TWI357899B (en) 2012-02-11
CA2560936A1 (en) 2005-10-13
KR101205731B1 (ko) 2012-11-28
CA2560936C (en) 2013-01-08
BRPI0509353A (pt) 2007-09-11
IN2006DE05581A (enExample) 2007-08-31
CN1938278B (zh) 2012-12-12
CN1938278A (zh) 2007-03-28
IL178233A (en) 2014-02-27
UA83910C2 (ru) 2008-08-26
EP1767528A1 (en) 2007-03-28
CR8640A (es) 2007-08-28
ES2508765T3 (es) 2014-10-16
IL178233A0 (en) 2006-12-31
BRPI0509353A8 (pt) 2017-09-19

Similar Documents

Publication Publication Date Title
JP2005289824A (ja) ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法
WO2004013106A1 (ja) ピラゾール誘導体及びその製造方法
KR101401139B1 (ko) 5-알콕시-4-히드록시메틸피라졸 화합물의 제조방법
JP2012533580A (ja) アリール置換ピラゾールの調製方法
DK1858858T3 (en) PROCEDURE FOR THE PREPARATION OF ALKYLANILIDES
JP2007246396A (ja) ５−ジフルオロメトキシ−４−チオメチルピラゾール化合物の製造方法
JP5406581B2 (ja) アントラニルアミド系化合物の製造方法
KR101308227B1 (ko) 니코틴산 유도체 또는 그의 염의 제조 방법
JP4075357B2 (ja) ４，５−ジ置換−１，２，３−トリアゾール及びその製造法
US9296700B2 (en) Method for purifying a pyrazolinone derivative
JPH0782252A (ja) イミド酸エステル化合物及びｎ−ピラゾリルアミドオキシム化合物の製造方法
US20050096472A1 (en) Process for producing 3-unsubstituted 5-amino-4-nitrosopyrazole compound, and 2-hydroxyimino-3-oxopropionitrile, 3-hydrazono-2-hydroxyiminopropionitrile compound, and processes for producing these
MX2008010361A (es) Proceso para producir compuesto 5-alcoxi-4-hidroximetilpirazol
KR20070007797A (ko) 1,5-디페닐피라졸 카르복실산 유도체의 제조 방법
JPWO2002076962A1 (ja) ３−オキソ−２−（２−チアゾリル）プロパンニトリルの製造方法および中間体
MXPA06009320A (en) Pyrazoline derivatives useful for the treatment of cancer

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20070227

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20100720

R155 Notification before disposition of declining of application

Free format text: JAPANESE INTERMEDIATE CODE: R155

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20101013

R150 Certificate of patent or registration of utility model

Ref document number: 4621939

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

Free format text: JAPANESE INTERMEDIATE CODE: R150

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20131112

Year of fee payment: 3

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

S111 Request for change of ownership or part of ownership

Free format text: JAPANESE INTERMEDIATE CODE: R313111

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

EXPY Cancellation because of completion of term