NO300125B1 - Stabil væskeformig silikasol, samt fremgangsmåte ved fremstilling derav - Google Patents
Stabil væskeformig silikasol, samt fremgangsmåte ved fremstilling derav Download PDFInfo
- Publication number
- NO300125B1 NO300125B1 NO891124A NO891124A NO300125B1 NO 300125 B1 NO300125 B1 NO 300125B1 NO 891124 A NO891124 A NO 891124A NO 891124 A NO891124 A NO 891124A NO 300125 B1 NO300125 B1 NO 300125B1
- Authority
- NO
- Norway
- Prior art keywords
- sol
- silica
- weight
- water
- sio
- Prior art date
Links
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 title claims description 133
- 239000007788 liquid Substances 0.000 title claims description 48
- 238000000034 method Methods 0.000 title claims description 47
- 230000008569 process Effects 0.000 title claims description 4
- 238000002360 preparation method Methods 0.000 title description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 181
- 239000002245 particle Substances 0.000 claims description 159
- 239000008119 colloidal silica Substances 0.000 claims description 72
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 71
- 235000012239 silicon dioxide Nutrition 0.000 claims description 70
- 239000000203 mixture Substances 0.000 claims description 56
- 239000000377 silicon dioxide Substances 0.000 claims description 50
- 230000002378 acidificating effect Effects 0.000 claims description 33
- 229910052681 coesite Inorganic materials 0.000 claims description 26
- 229910052906 cristobalite Inorganic materials 0.000 claims description 26
- 150000007530 organic bases Chemical class 0.000 claims description 26
- 229910052682 stishovite Inorganic materials 0.000 claims description 26
- 229910052905 tridymite Inorganic materials 0.000 claims description 26
- 239000007864 aqueous solution Substances 0.000 claims description 24
- 239000000292 calcium oxide Substances 0.000 claims description 24
- 239000000243 solution Substances 0.000 claims description 23
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 21
- 159000000003 magnesium salts Chemical class 0.000 claims description 19
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims description 18
- 159000000007 calcium salts Chemical class 0.000 claims description 18
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims description 16
- 239000000395 magnesium oxide Substances 0.000 claims description 15
- 238000002296 dynamic light scattering Methods 0.000 claims description 13
- 238000002156 mixing Methods 0.000 claims description 13
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 claims description 12
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 11
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims description 10
- 235000019353 potassium silicate Nutrition 0.000 claims description 9
- 239000002253 acid Substances 0.000 claims description 8
- 239000003960 organic solvent Substances 0.000 claims description 7
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 6
- 229910052783 alkali metal Inorganic materials 0.000 claims description 6
- 150000001340 alkali metals Chemical group 0.000 claims description 6
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims description 5
- 239000003729 cation exchange resin Substances 0.000 claims description 5
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 claims description 4
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 claims description 4
- WGTYBPLFGIVFAS-UHFFFAOYSA-M tetramethylammonium hydroxide Chemical compound [OH-].C[N+](C)(C)C WGTYBPLFGIVFAS-UHFFFAOYSA-M 0.000 claims description 4
- ZLRANBHTTCVNCE-UHFFFAOYSA-N 2-phenyl-3-(trifluoromethyl)pyridine Chemical compound FC(F)(F)C1=CC=CN=C1C1=CC=CC=C1 ZLRANBHTTCVNCE-UHFFFAOYSA-N 0.000 claims description 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 2
- UEEJHVSXFDXPFK-UHFFFAOYSA-N N-dimethylaminoethanol Chemical compound CN(C)CCO UEEJHVSXFDXPFK-UHFFFAOYSA-N 0.000 claims description 2
- OPKOKAMJFNKNAS-UHFFFAOYSA-N N-methylethanolamine Chemical compound CNCCO OPKOKAMJFNKNAS-UHFFFAOYSA-N 0.000 claims description 2
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 2
- 239000004111 Potassium silicate Substances 0.000 claims description 2
- 239000004115 Sodium Silicate Substances 0.000 claims description 2
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 2
- 235000011148 calcium chloride Nutrition 0.000 claims description 2
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 2
- 229910001629 magnesium chloride Inorganic materials 0.000 claims description 2
- NNHHDJVEYQHLHG-UHFFFAOYSA-N potassium silicate Chemical compound [K+].[K+].[O-][Si]([O-])=O NNHHDJVEYQHLHG-UHFFFAOYSA-N 0.000 claims description 2
- 229910052913 potassium silicate Inorganic materials 0.000 claims description 2
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 2
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 3
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims 2
- YIXJRHPUWRPCBB-UHFFFAOYSA-N magnesium nitrate Chemical compound [Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O YIXJRHPUWRPCBB-UHFFFAOYSA-N 0.000 claims 2
- CBOCVOKPQGJKKJ-UHFFFAOYSA-L Calcium formate Chemical compound [Ca+2].[O-]C=O.[O-]C=O CBOCVOKPQGJKKJ-UHFFFAOYSA-L 0.000 claims 1
- WUGQZFFCHPXWKQ-UHFFFAOYSA-N Propanolamine Chemical compound NCCCO WUGQZFFCHPXWKQ-UHFFFAOYSA-N 0.000 claims 1
- 239000000908 ammonium hydroxide Substances 0.000 claims 1
- VSGNNIFQASZAOI-UHFFFAOYSA-L calcium acetate Chemical compound [Ca+2].CC([O-])=O.CC([O-])=O VSGNNIFQASZAOI-UHFFFAOYSA-L 0.000 claims 1
- 239000001639 calcium acetate Substances 0.000 claims 1
- 229960005147 calcium acetate Drugs 0.000 claims 1
- 235000011092 calcium acetate Nutrition 0.000 claims 1
- 239000001110 calcium chloride Substances 0.000 claims 1
- 229910001628 calcium chloride Inorganic materials 0.000 claims 1
- 229940044172 calcium formate Drugs 0.000 claims 1
- 235000019255 calcium formate Nutrition 0.000 claims 1
- 239000004281 calcium formate Substances 0.000 claims 1
- RSIPQRDGPVEGLE-UHFFFAOYSA-L calcium;disulfamate Chemical compound [Ca+2].NS([O-])(=O)=O.NS([O-])(=O)=O RSIPQRDGPVEGLE-UHFFFAOYSA-L 0.000 claims 1
- UEGPKNKPLBYCNK-UHFFFAOYSA-L magnesium acetate Chemical compound [Mg+2].CC([O-])=O.CC([O-])=O UEGPKNKPLBYCNK-UHFFFAOYSA-L 0.000 claims 1
- 239000011654 magnesium acetate Substances 0.000 claims 1
- 235000011285 magnesium acetate Nutrition 0.000 claims 1
- 229940069446 magnesium acetate Drugs 0.000 claims 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims 1
- 235000019341 magnesium sulphate Nutrition 0.000 claims 1
- GMDNUWQNDQDBNQ-UHFFFAOYSA-L magnesium;diformate Chemical compound [Mg+2].[O-]C=O.[O-]C=O GMDNUWQNDQDBNQ-UHFFFAOYSA-L 0.000 claims 1
- YZVJHCGMTYDKFR-UHFFFAOYSA-L magnesium;disulfamate Chemical compound [Mg+2].NS([O-])(=O)=O.NS([O-])(=O)=O YZVJHCGMTYDKFR-UHFFFAOYSA-L 0.000 claims 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 41
- 239000000499 gel Substances 0.000 description 28
- 229910052751 metal Inorganic materials 0.000 description 28
- 239000002184 metal Substances 0.000 description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 25
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 23
- 238000003756 stirring Methods 0.000 description 21
- 238000010438 heat treatment Methods 0.000 description 19
- 150000001450 anions Chemical class 0.000 description 16
- 150000001768 cations Chemical class 0.000 description 15
- 150000003839 salts Chemical class 0.000 description 15
- 239000011734 sodium Substances 0.000 description 14
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 13
- 239000011521 glass Substances 0.000 description 13
- 239000011575 calcium Substances 0.000 description 12
- 150000002739 metals Chemical class 0.000 description 11
- 239000000047 product Substances 0.000 description 11
- 229910052791 calcium Inorganic materials 0.000 description 10
- -1 e.g. Sr Chemical class 0.000 description 9
- 239000000126 substance Substances 0.000 description 9
- 238000007792 addition Methods 0.000 description 8
- 229910052749 magnesium Inorganic materials 0.000 description 8
- 239000011777 magnesium Substances 0.000 description 8
- 239000002609 medium Substances 0.000 description 8
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical class [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 7
- 239000008199 coating composition Substances 0.000 description 7
- 239000000835 fiber Substances 0.000 description 7
- 239000012634 fragment Substances 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- 238000000108 ultra-filtration Methods 0.000 description 7
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 6
- 230000001070 adhesive effect Effects 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 6
- 239000003153 chemical reaction reagent Substances 0.000 description 6
- 150000004760 silicates Chemical class 0.000 description 6
- 239000000853 adhesive Substances 0.000 description 5
- 229910044991 metal oxide Inorganic materials 0.000 description 5
- 150000004706 metal oxides Chemical class 0.000 description 5
- JLVVSXFLKOJNIY-UHFFFAOYSA-N Magnesium ion Chemical compound [Mg+2] JLVVSXFLKOJNIY-UHFFFAOYSA-N 0.000 description 4
- 239000002585 base Substances 0.000 description 4
- 229910001424 calcium ion Inorganic materials 0.000 description 4
- 238000005341 cation exchange Methods 0.000 description 4
- 230000008859 change Effects 0.000 description 4
- 229910001425 magnesium ion Inorganic materials 0.000 description 4
- 239000012528 membrane Substances 0.000 description 4
- 239000011347 resin Substances 0.000 description 4
- 229920005989 resin Polymers 0.000 description 4
- 239000011342 resin composition Substances 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 230000006641 stabilisation Effects 0.000 description 4
- 238000011105 stabilization Methods 0.000 description 4
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 229910000272 alkali metal oxide Inorganic materials 0.000 description 3
- 238000000149 argon plasma sintering Methods 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 238000001879 gelation Methods 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 3
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 3
- 238000001935 peptisation Methods 0.000 description 3
- 239000004033 plastic Substances 0.000 description 3
- 229920003023 plastic Polymers 0.000 description 3
- 230000003014 reinforcing effect Effects 0.000 description 3
- 239000002002 slurry Substances 0.000 description 3
- 239000000758 substrate Substances 0.000 description 3
- 229910052718 tin Inorganic materials 0.000 description 3
- 229910052719 titanium Inorganic materials 0.000 description 3
- 239000002023 wood Substances 0.000 description 3
- 229910052725 zinc Inorganic materials 0.000 description 3
- 239000011701 zinc Substances 0.000 description 3
- 238000004438 BET method Methods 0.000 description 2
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 2
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 150000001242 acetic acid derivatives Chemical class 0.000 description 2
- 150000004645 aluminates Chemical class 0.000 description 2
- 150000001412 amines Chemical class 0.000 description 2
- 229910052788 barium Inorganic materials 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 229910052804 chromium Inorganic materials 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 238000010410 dusting Methods 0.000 description 2
- 239000003792 electrolyte Substances 0.000 description 2
- 238000001493 electron microscopy Methods 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 150000004675 formic acid derivatives Chemical class 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000012784 inorganic fiber Substances 0.000 description 2
- 229910052745 lead Inorganic materials 0.000 description 2
- 235000011147 magnesium chloride Nutrition 0.000 description 2
- 229910052748 manganese Inorganic materials 0.000 description 2
- 229910000000 metal hydroxide Inorganic materials 0.000 description 2
- 150000004692 metal hydroxides Chemical class 0.000 description 2
- 229910021645 metal ion Inorganic materials 0.000 description 2
- 239000012982 microporous membrane Substances 0.000 description 2
- 230000005012 migration Effects 0.000 description 2
- 238000013508 migration Methods 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 229910052759 nickel Inorganic materials 0.000 description 2
- 150000002823 nitrates Chemical class 0.000 description 2
- 239000000123 paper Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 125000001453 quaternary ammonium group Chemical group 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 125000005402 stannate group Chemical group 0.000 description 2
- 229910052712 strontium Inorganic materials 0.000 description 2
- IIACRCGMVDHOTQ-UHFFFAOYSA-N sulfamic acid Chemical class NS(O)(=O)=O IIACRCGMVDHOTQ-UHFFFAOYSA-N 0.000 description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 2
- 238000004381 surface treatment Methods 0.000 description 2
- 229910052726 zirconium Inorganic materials 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910001413 alkali metal ion Inorganic materials 0.000 description 1
- 229910052910 alkali metal silicate Inorganic materials 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
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- 239000012736 aqueous medium Substances 0.000 description 1
- 239000000440 bentonite Substances 0.000 description 1
- 229910000278 bentonite Inorganic materials 0.000 description 1
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
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- 150000003841 chloride salts Chemical class 0.000 description 1
- KRVSOGSZCMJSLX-UHFFFAOYSA-L chromic acid Substances O[Cr](O)(=O)=O KRVSOGSZCMJSLX-UHFFFAOYSA-L 0.000 description 1
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- TVQLLNFANZSCGY-UHFFFAOYSA-N disodium;dioxido(oxo)tin Chemical compound [Na+].[Na+].[O-][Sn]([O-])=O TVQLLNFANZSCGY-UHFFFAOYSA-N 0.000 description 1
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- AWJWCTOOIBYHON-UHFFFAOYSA-N furo[3,4-b]pyrazine-5,7-dione Chemical compound C1=CN=C2C(=O)OC(=O)C2=N1 AWJWCTOOIBYHON-UHFFFAOYSA-N 0.000 description 1
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- 229910052727 yttrium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C01B33/146—After-treatment of sols
- C01B33/148—Concentration; Drying; Dehydration; Stabilisation; Purification
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C01B33/145—Preparation of hydroorganosols, organosols or dispersions in an organic medium
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
- Silicon Polymers (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP6284988 | 1988-03-16 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO891124D0 NO891124D0 (no) | 1989-03-15 |
| NO891124L NO891124L (no) | 1989-09-18 |
| NO300125B1 true NO300125B1 (no) | 1997-04-14 |
Family
ID=13212169
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO891124A NO300125B1 (no) | 1988-03-16 | 1989-03-15 | Stabil væskeformig silikasol, samt fremgangsmåte ved fremstilling derav |
Country Status (9)
| Country | Link |
|---|---|
| EP (1) | EP0335195B1 (fr) |
| KR (1) | KR960014908B1 (fr) |
| CN (1) | CN1022099C (fr) |
| CA (1) | CA1314457C (fr) |
| DE (1) | DE68911346T2 (fr) |
| DK (1) | DK175640B1 (fr) |
| ES (1) | ES2047051T3 (fr) |
| FI (1) | FI91145C (fr) |
| NO (1) | NO300125B1 (fr) |
Families Citing this family (33)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1992005222A1 (fr) * | 1990-09-21 | 1992-04-02 | Toray Industries, Inc. | Composition de polyester thermoplastique et film produit a partir de ce polyester |
| TW498054B (en) * | 1998-09-10 | 2002-08-11 | Nissan Chemical Ind Ltd | Moniliform silica sol and process for producing the same, and coating composition for ink receiving layer and ink jet recording medium having ink receiving layer |
| CN1912242B (zh) * | 1999-05-04 | 2011-01-12 | 阿克佐诺贝尔公司 | 生产纸的方法 |
| JP4132432B2 (ja) * | 1999-07-02 | 2008-08-13 | 日産化学工業株式会社 | 研磨用組成物 |
| WO2002000550A1 (fr) * | 2000-06-26 | 2002-01-03 | Asahi Kasei Kabushiki Kaisha | Particules inorganiques fines et poreuses |
| JP4198009B2 (ja) * | 2003-08-07 | 2008-12-17 | ジャパンゴアテックス株式会社 | 固体高分子電解質膜及び燃料電池 |
| US20050234136A1 (en) * | 2004-04-19 | 2005-10-20 | Holland Brian T | Colloidal compositions and methods of preparing same |
| JP2007063117A (ja) * | 2005-08-02 | 2007-03-15 | Nissan Chem Ind Ltd | 有機溶媒分散シリカゾル及びその製造方法 |
| US20080108497A1 (en) * | 2006-11-08 | 2008-05-08 | Holland Brian T | Metal-rich siliceous compositions and methods of producing same |
| CN101626979B (zh) * | 2007-02-01 | 2012-01-25 | 日产化学工业株式会社 | 具有细长形状的硅溶胶的制造方法 |
| KR101429318B1 (ko) * | 2007-02-02 | 2014-08-11 | 닛산 가가쿠 고교 가부시키 가이샤 | 반응성 모노머 분산 실리카 졸, 이의 제조방법, 경화용 조성물 및 이의 경화체 |
| JP5525258B2 (ja) * | 2007-05-18 | 2014-06-18 | 日立金属株式会社 | セラミックハニカム構造体の製造方法及びセラミックハニカム構造体 |
| AR066831A1 (es) * | 2007-06-07 | 2009-09-16 | Akzo Nobel Nv | Soles a base de silice |
| AU2011203171B2 (en) * | 2007-06-07 | 2012-01-12 | Akzo Nobel Chemicals International B.V. | Silica-based sols |
| US8845991B2 (en) | 2010-04-08 | 2014-09-30 | Ecolab Usa Inc. | Silica particle manufacturing process |
| TWI427034B (zh) | 2010-12-22 | 2014-02-21 | Ind Tech Res Inst | 無機奈米片材之有機分散液及其製造方法 |
| TWI584867B (zh) * | 2011-09-05 | 2017-06-01 | 日產化學工業股份有限公司 | 經純化的矽酸鹼水溶液及矽溶膠的製造方法 |
| WO2013129093A1 (fr) * | 2012-02-29 | 2013-09-06 | 日産化学工業株式会社 | Sol silicieux dispersé dans un solvant organique et procédé de fabrication dudit sol silicieux dispersé dans un solvant organique |
| CN102838124A (zh) * | 2012-09-21 | 2012-12-26 | 安徽工业大学 | 一种不含金属离子的高纯硅溶胶的制备方法 |
| US9695254B2 (en) | 2012-11-26 | 2017-07-04 | Braskem S.A. | Metallocene catalyst supported by hybrid supporting means, process for producing same, polymerization process for producing an ethylene homopolymer or copolymer with broad or bimodal molar mass distribution, use of the supported metallocene catalyst and ethylene polymer with broad or bimodal molar mass distribution |
| PL3036192T3 (pl) | 2013-08-23 | 2019-03-29 | Akzo Nobel Chemicals International B.V. | Zol krzemionkowy |
| CN105960378B (zh) * | 2014-02-06 | 2020-07-24 | 日产化学工业株式会社 | 二氧化硅系微粒溶胶及其制造方法 |
| CN104745146A (zh) * | 2015-03-23 | 2015-07-01 | 江苏天恒纳米科技股份有限公司 | 含铈掺杂二氧化硅纳米复合磨粒溶胶、抛光液及其制备方法 |
| CN104877401A (zh) * | 2015-05-25 | 2015-09-02 | 天津市职业大学 | 一种玻璃镀膜液的制备方法及应用 |
| JP6894759B2 (ja) * | 2017-05-17 | 2021-06-30 | 株式会社松風 | 歯科用りん酸塩系埋没材 |
| RS65075B1 (sr) * | 2017-09-07 | 2024-02-29 | Nissan Chemical Corp | Izolaciona kompozicija koja sadrži silicijum dioksid |
| CN107777692B (zh) * | 2017-09-29 | 2020-02-18 | 中海油天津化工研究设计院有限公司 | 一种脱硝催化剂用高纯硅溶胶的制备方法 |
| CN107959064A (zh) * | 2017-11-27 | 2018-04-24 | 大同新成新材料股份有限公司 | 一种触变性胶体电解质及其制备方法和胶体蓄电池 |
| CN110194458B (zh) * | 2018-02-24 | 2021-03-23 | 航天特种材料及工艺技术研究所 | 一种硅溶胶及制备方法 |
| US11897774B2 (en) * | 2018-02-26 | 2024-02-13 | Nissan Chemical Corporation | Method for producing silica sol having elongated particle shape |
| CN110217799B (zh) * | 2018-03-02 | 2020-12-18 | 中国石油化工股份有限公司 | 硅溶胶及其制备方法 |
| CN111847462B (zh) * | 2020-08-03 | 2021-03-19 | 马惠琪 | 稳定获取指定粒度高纯硅溶胶的方法 |
| CN115477529A (zh) * | 2022-07-26 | 2022-12-16 | 保利长大工程有限公司 | 一种基于花岗岩石粉的混凝土及其制备方法 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2680721A (en) * | 1952-03-20 | 1954-06-08 | Du Pont | Process of increasing the size of unaggregated silica particles in an aqueous silicasuspension |
| US2900348A (en) * | 1954-02-02 | 1959-08-18 | Grace W R & Co | Preparation of silica sols |
-
1989
- 1989-03-15 NO NO891124A patent/NO300125B1/no not_active IP Right Cessation
- 1989-03-15 CN CN89101368A patent/CN1022099C/zh not_active Expired - Lifetime
- 1989-03-16 EP EP89104743A patent/EP0335195B1/fr not_active Expired - Lifetime
- 1989-03-16 ES ES89104743T patent/ES2047051T3/es not_active Expired - Lifetime
- 1989-03-16 DE DE89104743T patent/DE68911346T2/de not_active Expired - Fee Related
- 1989-03-16 FI FI891243A patent/FI91145C/fi active IP Right Grant
- 1989-03-16 DK DK198901283A patent/DK175640B1/da not_active IP Right Cessation
- 1989-03-16 KR KR1019890003263A patent/KR960014908B1/ko not_active IP Right Cessation
- 1989-03-16 CA CA000593983A patent/CA1314457C/fr not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| CN1036547A (zh) | 1989-10-25 |
| CN1022099C (zh) | 1993-09-15 |
| FI891243A (fi) | 1989-09-17 |
| KR890014384A (ko) | 1989-10-23 |
| NO891124L (no) | 1989-09-18 |
| DK128389A (da) | 1989-09-17 |
| EP0335195A2 (fr) | 1989-10-04 |
| CA1314457C (fr) | 1993-03-16 |
| EP0335195B1 (fr) | 1993-12-15 |
| FI91145C (fi) | 1994-05-25 |
| NO891124D0 (no) | 1989-03-15 |
| ES2047051T3 (es) | 1994-02-16 |
| FI91145B (fi) | 1994-02-15 |
| DK175640B1 (da) | 2005-01-03 |
| FI891243A0 (fi) | 1989-03-16 |
| KR960014908B1 (ko) | 1996-10-21 |
| DK128389D0 (da) | 1989-03-16 |
| EP0335195A3 (fr) | 1991-11-06 |
| DE68911346T2 (de) | 1994-05-11 |
| DE68911346D1 (de) | 1994-01-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MK1K | Patent expired |