JPWO2018008088A1 - 基板処理装置、ガスノズルおよび半導体装置の製造方法 - Google Patents
基板処理装置、ガスノズルおよび半導体装置の製造方法 Download PDFInfo
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Abstract
[解決手段] 複数枚の基板を処理する処理室と、処理室内にガスを供給するノズルと、を備え、ノズルは、縦方向に開口したスリットを有し、スリットは、ノズルの先端部の頂点まで形成されている。
Description
複数枚の基板を処理する処理室と、
前記処理室内にガスを供給するノズルと、を備え、
前記ノズルは、
縦方向に開口したスリットを有し、
前記スリットは、前記ガスノズルの先端部の頂点まで形成されている技術が提供される。
複数枚のウエハWがボート26に装填(ウエハチャージ)されると、ボート26は、ボートエレベータ32によって処理室14内に搬入(ボートロード)され、反応管10の下部開口は蓋部22によって気密に閉塞(シール)された状態となる。
処理室14内が所定の圧力(真空度)となるように、真空ポンプ52によって真空排気(減圧排気)される。処理室14内の圧力は、圧力センサ48で測定され、この測定された圧力情報に基づきAPCバルブ50がフィードバック制御される。また、処理室14内のウエハWが所定の温度となるように、ヒータ12によって加熱される。この際、処理室14が所定の温度分布となるように、温度検出部16が検出した温度情報に基づきヒータ12への通電具合がフィードバック制御される。また、回転機構30によるボート26およびウエハWの回転を開始する。
[原料ガス供給工程]
処理室14内の温度が予め設定された処理温度に安定すると、処理室14内のウエハWに対してHCDSガスを供給する。HCDSガスは、MFC38aにて所望の流量となるように制御され、ガス供給管36a、ノズル44aおよびスリット10Dを介して処理室14内に供給される。
次に、HCDSガスの供給を停止し、真空ポンプ52により処理室14内を真空排気する。この時、不活性ガス供給部から不活性ガスとしてN2ガスを処理室14内に供給しても良い(不活性ガスパージ)。
次に、処理室14内のウエハWに対してNH3ガスを供給する。NH3ガスは、MFC38bにて所望の流量となるように制御され、ガス供給管36b、ノズル44bおよびスリット10Dを介して処理室14内に供給される。
次に、NH3ガスの供給を停止し、真空ポンプ52により処理室14内を真空排気する。この時、不活性ガス供給部からN2ガスを処理室14内に供給しても良い(不活性ガスパージ)。
所定膜厚の膜を形成した後、不活性ガス供給部からN2ガスが供給され、処理室14内の雰囲気がN2ガスに置換されると共に、処理室14の圧力が常圧に復帰される。その後、ボートエレベータ32により蓋部22が降下されて、ボート26が反応管10から搬出(ボートアンロード)される。その後、処理済ウエハWはボート26より取出される(ウエハディスチャージ)。
処理温度(ウエハ温度):300℃〜700℃、
処理圧力(処理室内圧力):1Pa〜4000Pa、
HCDSガス:100sccm〜10000sccm、
NH3ガス:100sccm〜10000sccm、
N2ガス:100sccm〜10000sccm、
それぞれの処理条件を、それぞれの範囲内の値に設定することで、成膜処理を適正に進行させることが可能となる。
本実施形態によれば、以下に示す1つ又は複数の効果が得られる。
(2)ガス供給口をスリット形状とすることにより、ガス流量を増加させてもノズル内圧の上昇を抑制することができ、また、ガス流量を増加させることができるため、プロセスウインドウを広げることができ、成膜の品質を向上させることができる。また、ノズル内圧が上昇すると、ノズル内でガスが成膜してしまい、パーティクルの発生源となってしまうことがある。本発明のノズルによれば、ノズル内圧の上昇を抑制できるため、パーティクルの発生を抑制することができる。
(3)ガスを2段階で整流させることにより、面間の均一性を向上させることができる。ノズルから供給されたガスは、
ノズルスリットで整流されて均一に流れ、さらに供給バッファ室のスリットでもう一段階整流されることにより、上下方向に均一の濃度でウエハに供給することができる。
本実施形態におけるノズルは、上述の態様に限定されず、以下に示す変形例のような態様に変更することができる。
図7(A)に示すように、スリット45aは先端部の頂点までではなく、頂点を超えて後ろ側(反対側)まで形成しても良い。このような構成により、ガスが滞留しやすいバッファ室10Aの上部の角部へもガスを直接供給できるため、角部におけるガスの滞留を抑制することができ、膜の品質を向上させることができる。
図7(B)に示すように、スリット45aの上方(例えば、スリット45a上部の1/3程度)の幅を下方の幅よりも大きく形成しても良い。このような構成により、上部におけるガス流量を増加させることができ、面間均一性を向上させることができる。
図7(C)に示すように、スリット45aの上端は開放されていても良い。このとき、スリット45aは上端まで形成されていなくても良い。このような構成により、上部におけるガス流量を増加させることができ、面間均一性を向上させることができる。また、ノズル内のガス滞留を抑制することができ、膜の特性を向上させることができる。
図7(D)に示すように、スリットは複数に複数に分割されていても良い。このような構成により、ノズルの強度を向上させることができる。
(変形例5)
図12(A)に示すように、上流部74にもスリットを形成しても良い。例えば、下流部72のスリットの幅よりも上流部74のスリットの幅を狭くしても良い。また例えば、上流部74にスリットではなく多孔を形成しても良い。このような構成により、所望の分解状態でガスをウエハWに供給することができる。
図12(B)に示すように、スリット45aの長さをウエハWの配列長よりも短い長さで形成しても良い。例えば、スリット45aの上端の位置がボート26に保持される最上段〜中段のウエハWの高さ位置になるように、また、スリット45aの下端の位置がボート26に保持される最下段のウエハWの高さ位置より低くなるように形成しても良い。言い換えれば、スリット45aの長さは、下段〜中段に保持されたウエハWの配列長をカバーする長さであっても良い。このような構成により、上段に保持されたウエハWへのガスの過剰供給を抑制することができ、面間均一性を向上させることができる。
44a ノズル
45a スリット
Claims (14)
- 縦方向に多段に保持された複数枚の基板を処理する処理室と、
前記処理室内にガスを供給するノズルと、を備え、
前記ノズルは、
縦方向に開口したスリットを有し、
前記スリットは、前記ノズルの先端部の頂点まで形成されている基板処理装置。 - 前記スリットの上端は、複数枚の前記基板の最上段の基板の位置よりも高い位置に形成され、
前記スリットの下端は、複数枚の前記基板の最下段の基板の位置よりも低い位置に形成される請求項1に記載の基板処理装置。 - 前記処理室に隣接して形成されたガス供給室をさらに有し、
前記ノズルは前記ガス供給室内に配置される請求項2に記載の基板処理装置。 - 前記ノズルの内圧は、前記ノズル内でガスが分解する圧力よりも低い圧力である請求項3に記載の基板処理装置。
- 前記スリットの幅は、前記ノズルの内径の0.02倍以上0.2倍以下の範囲である請求項1に記載の基板処理装置。
- 前記ノズルは、
折り返し部と、
前記折り返し部よりも上流側である上流部と、
前記折り返し部よりも下流側である下流部と、を有し、
前記スリットは前記下流部に形成される請求項1に記載の基板処理装置。 - 前記ノズルは、
前記上流部よりもさらに上流側に位置する基部と、
前記基部と前記上流部とを接続する傾斜部と、を有し、
前記基部の中心線は、前記上流部の中心線と前記下流部の中心線との間に位置する請求項6に記載の基板処理装置。 - 前記ノズル内でのガス滞留時間を、ストレートノズル内におけるガス滞留時間よりも長くすることにより、前記下流部の下端に近付くほど分解した状態のガスの量を多くする請求項7に記載の基板処理装置。
- 前記スリットの上端は、複数枚の前記基板の最上段の基板の位置よりも低い位置に形成され、
前記スリットの下端は、複数枚の前記基板の最下段の基板の位置よりも低い位置に形成される請求項8に記載の基板処理装置。 - 前記処理室に隣接して形成され、前記ノズルが配置されるガス供給室と、
前記ガス供給室に設置され、複数のガス供給孔を有する多孔ノズルと、をさらに有し、
前記ノズルは、前記基板の中心と前記多孔ノズルの前記ガス供給孔とを結ぶ線を半径とする仮想円上に前記スリットが位置するように前記ガス供給室内に斜めに設置される請求項7に記載の基板処理装置。 - 前記ノズルは、前記基板の中心と前記基部の中心とを結ぶ線と、前記上流部の中心と前記下流部の中心とを結ぶ線とのなす角度が0度〜90度となるように、前記ガス供給室内に設置される請求項10に記載の基板処理装置。
- 複数枚の基板を処理室内で処理する基板処理装置内に設置され、前記処理室内にガスを供給するノズルであって、
前記ノズルは、
縦方向に開口したスリットを有し、
前記スリットは、前記ノズルの先端部の頂点まで形成されているノズル。 - 前記ノズルは、
折り返し部と、
前記折り返し部よりも上流側である上流部と、
前記折り返し部よりも下流側である下流部と、
前記上流部よりもさらに上流側に位置する基部と、
前記基部と前記上流部とを接続する傾斜部と、を有し、
前記スリットは前記下流部に形成され、
前記基部の中心線は、前記上流部の中心線と前記下流部の中心線との間に位置する請求項12に記載のノズル。 - 複数枚の基板を処理する処理室内に前記基板を搬入する工程と、
縦方向に開口したスリットが先端部の頂点まで形成されているノズルから前記処理室内にガスを供給し、前記処理室内で前記基板を処理する工程と、
を有する半導体装置の製造方法。
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