JPH0262498B2 - - Google Patents
Info
- Publication number
- JPH0262498B2 JPH0262498B2 JP61050170A JP5017086A JPH0262498B2 JP H0262498 B2 JPH0262498 B2 JP H0262498B2 JP 61050170 A JP61050170 A JP 61050170A JP 5017086 A JP5017086 A JP 5017086A JP H0262498 B2 JPH0262498 B2 JP H0262498B2
- Authority
- JP
- Japan
- Prior art keywords
- sol
- titanium oxide
- acid
- present
- gel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 49
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 28
- 239000002245 particle Substances 0.000 claims description 26
- 239000002253 acid Substances 0.000 claims description 14
- 238000004519 manufacturing process Methods 0.000 claims description 12
- 150000003868 ammonium compounds Chemical class 0.000 claims description 7
- 150000003609 titanium compounds Chemical class 0.000 claims description 7
- 229910010413 TiO 2 Inorganic materials 0.000 description 16
- 238000000034 method Methods 0.000 description 12
- 238000010335 hydrothermal treatment Methods 0.000 description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 8
- 239000007864 aqueous solution Substances 0.000 description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 6
- 238000002441 X-ray diffraction Methods 0.000 description 6
- 229910017604 nitric acid Inorganic materials 0.000 description 6
- 239000006185 dispersion Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- 239000004408 titanium dioxide Substances 0.000 description 5
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 5
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 description 4
- 239000001099 ammonium carbonate Substances 0.000 description 4
- 238000001914 filtration Methods 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- QDZRBIRIPNZRSG-UHFFFAOYSA-N titanium nitrate Chemical compound [O-][N+](=O)O[Ti](O[N+]([O-])=O)(O[N+]([O-])=O)O[N+]([O-])=O QDZRBIRIPNZRSG-UHFFFAOYSA-N 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 235000011054 acetic acid Nutrition 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 238000001493 electron microscopy Methods 0.000 description 3
- 239000010445 mica Substances 0.000 description 3
- 229910052618 mica group Inorganic materials 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- -1 titanium alkoxide Chemical class 0.000 description 3
- 229910000013 Ammonium bicarbonate Inorganic materials 0.000 description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 2
- AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Chemical compound OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 229910052783 alkali metal Inorganic materials 0.000 description 2
- 235000012538 ammonium bicarbonate Nutrition 0.000 description 2
- 235000012501 ammonium carbonate Nutrition 0.000 description 2
- 235000011114 ammonium hydroxide Nutrition 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000010408 film Substances 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000012209 synthetic fiber Substances 0.000 description 2
- 229920002994 synthetic fiber Polymers 0.000 description 2
- 239000010936 titanium Substances 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 229910000288 alkali metal carbonate Inorganic materials 0.000 description 1
- 150000008041 alkali metal carbonates Chemical class 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000002178 crystalline material Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 239000012770 industrial material Substances 0.000 description 1
- YDZQQRWRVYGNER-UHFFFAOYSA-N iron;titanium;trihydrate Chemical compound O.O.O.[Ti].[Fe] YDZQQRWRVYGNER-UHFFFAOYSA-N 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000011824 nuclear material Substances 0.000 description 1
- 239000011224 oxide ceramic Substances 0.000 description 1
- DCKVFVYPWDKYDN-UHFFFAOYSA-L oxygen(2-);titanium(4+);sulfate Chemical compound [O-2].[Ti+4].[O-]S([O-])(=O)=O DCKVFVYPWDKYDN-UHFFFAOYSA-L 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- LLZRNZOLAXHGLL-UHFFFAOYSA-J titanic acid Chemical compound O[Ti](O)(O)O LLZRNZOLAXHGLL-UHFFFAOYSA-J 0.000 description 1
- 150000003608 titanium Chemical class 0.000 description 1
- 229910000348 titanium sulfate Inorganic materials 0.000 description 1
- 239000011882 ultra-fine particle Substances 0.000 description 1
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5017086A JPS62207718A (ja) | 1986-03-06 | 1986-03-06 | 結晶質酸化チタンゾルの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5017086A JPS62207718A (ja) | 1986-03-06 | 1986-03-06 | 結晶質酸化チタンゾルの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS62207718A JPS62207718A (ja) | 1987-09-12 |
| JPH0262498B2 true JPH0262498B2 (zh) | 1990-12-25 |
Family
ID=12851727
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP5017086A Granted JPS62207718A (ja) | 1986-03-06 | 1986-03-06 | 結晶質酸化チタンゾルの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS62207718A (zh) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2015044738A (ja) * | 2014-10-14 | 2015-03-12 | テイカ株式会社 | 無定形チタニアゾルおよびその製造方法 |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6317221A (ja) * | 1986-07-03 | 1988-01-25 | Taki Chem Co Ltd | 結晶質酸化チタンゾル及びその製造方法 |
| JPS63229139A (ja) * | 1986-10-29 | 1988-09-26 | Catalysts & Chem Ind Co Ltd | 酸化チタンゾルの製造方法 |
| FR2677012B1 (fr) * | 1991-05-31 | 1993-09-03 | Rhone Poulenc Chimie | Dioxyde de titane sous forme de plaquettes et son procede de preparation. |
| US5700451A (en) * | 1995-05-24 | 1997-12-23 | The Procter & Gamble Company | Sunscreen composition |
| EP1167296A4 (en) * | 1999-02-04 | 2005-03-16 | Kawasaki Heavy Ind Ltd | PROCESS FOR PRODUCING TITANIUM OXIDE OF THE ANATASE TYPE AND TITANIUM DIOXIDE COATING MATERIAL |
| KR100396085B1 (ko) * | 1999-12-21 | 2003-08-27 | 주식회사 포스코 | 이산화티탄 분말 및 그의 제조 방법 |
| JP2001262007A (ja) * | 2000-03-17 | 2001-09-26 | Mitsubishi Gas Chem Co Inc | チタニア塗布液及びその製造方法、並びにチタニア膜及びその形成方法 |
| KR100381921B1 (ko) * | 2000-07-21 | 2003-04-26 | 김정환 | 티타니아 코팅액 및 그의 제조방법 |
| KR100421243B1 (ko) * | 2000-12-01 | 2004-03-12 | (주) 에이엔티케미칼 | 수열합성 방법에 의해 결정성 및 분산성이 뛰어난아나타제형 광촉매용 산화티탄졸을 제조하는 방법 |
| KR100404449B1 (ko) * | 2001-02-16 | 2003-11-05 | 한상목 | 침전제 적하법을 이용한 이산화티탄 분말의 제조방법 |
| CA2439348A1 (en) * | 2001-02-27 | 2002-09-06 | Ecodevice Laboratory Co., Ltd. | Bleaching composition and method of bleaching teeth |
| KR100444892B1 (ko) * | 2001-06-01 | 2004-08-18 | 티오켐 주식회사 | 금속이 첨가된 고활성 광촉매 산화티탄-졸 제조 방법 |
| TWI240700B (en) | 2001-07-19 | 2005-10-01 | Sumitomo Chemical Co | Ceramics dispersion liquid, method for producing the same, and hydrophilic coating agent using the same |
| KR100436240B1 (ko) * | 2001-11-01 | 2004-06-16 | 김대승 | 항균금속성분을 함유하는 이산화티타늄 광촉매 및 그의 제조방법 |
| JP4184060B2 (ja) * | 2002-02-07 | 2008-11-19 | 学校法人日本大学 | ゾルの製造方法および基材の撥水処理方法 |
| JP4374869B2 (ja) | 2002-05-27 | 2009-12-02 | 住友化学株式会社 | セラミックス分散液の製造方法 |
| JP2004026553A (ja) | 2002-06-25 | 2004-01-29 | Sumitomo Chem Co Ltd | 酸化チタン分散液およびその保存容器 |
| JP2004196626A (ja) | 2002-12-20 | 2004-07-15 | Sumitomo Chem Co Ltd | 酸化チタンの製造方法 |
| KR100611632B1 (ko) * | 2003-11-14 | 2006-08-11 | (주)지엔씨글로텍 | 광촉매 조성물 및 그 제조방법 |
| JP4705361B2 (ja) * | 2004-11-19 | 2011-06-22 | 日揮触媒化成株式会社 | ジルコニアゾルの製造方法 |
| DE102006032755A1 (de) * | 2006-07-14 | 2008-01-17 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. | Stabile Suspensionen von kristallinen TiO2-Partikeln aus hydrothermal behandelten Sol-Gel-Vorstufenpulvern |
| EP2074064A4 (en) | 2006-09-21 | 2013-06-05 | Tokusen U S A Inc | LOW TEMPERATURE PROCESS FOR PRODUCING TITANIUM DIOXIDE PARTICLES OF A NANOMETER SIZE |
| CN102216221B (zh) | 2008-11-12 | 2014-09-10 | 日产化学工业株式会社 | 氧化钛溶胶的制造方法 |
| JP5223828B2 (ja) * | 2009-09-18 | 2013-06-26 | 堺化学工業株式会社 | アナタース型超微粒子酸化チタン、アナタース型超微粒子酸化チタンを含有する分散体、及び該酸化チタンの製造方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4843439A (zh) * | 1971-09-30 | 1973-06-23 | ||
| JPS5950604A (ja) * | 1982-09-16 | 1984-03-23 | Seiko Instr & Electronics Ltd | 発振回路 |
-
1986
- 1986-03-06 JP JP5017086A patent/JPS62207718A/ja active Granted
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4843439A (zh) * | 1971-09-30 | 1973-06-23 | ||
| JPS5950604A (ja) * | 1982-09-16 | 1984-03-23 | Seiko Instr & Electronics Ltd | 発振回路 |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2015044738A (ja) * | 2014-10-14 | 2015-03-12 | テイカ株式会社 | 無定形チタニアゾルおよびその製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS62207718A (ja) | 1987-09-12 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |