JP7165488B2 - 新規な甘味組成物 - Google Patents
新規な甘味組成物 Download PDFInfo
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- JP7165488B2 JP7165488B2 JP2016575765A JP2016575765A JP7165488B2 JP 7165488 B2 JP7165488 B2 JP 7165488B2 JP 2016575765 A JP2016575765 A JP 2016575765A JP 2016575765 A JP2016575765 A JP 2016575765A JP 7165488 B2 JP7165488 B2 JP 7165488B2
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- sweetening composition
- sorbitol
- composition according
- chewing gum
- chewing
- Prior art date
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- 239000008371 vanilla flavor Substances 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/30—Artificial sweetening agents
- A23L27/33—Artificial sweetening agents containing sugars or derivatives
- A23L27/34—Sugar alcohols
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G4/00—Chewing gum
- A23G4/06—Chewing gum characterised by the composition containing organic or inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G4/00—Chewing gum
- A23G4/06—Chewing gum characterised by the composition containing organic or inorganic compounds
- A23G4/08—Chewing gum characterised by the composition containing organic or inorganic compounds of the chewing gum base
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G4/00—Chewing gum
- A23G4/06—Chewing gum characterised by the composition containing organic or inorganic compounds
- A23G4/10—Chewing gum characterised by the composition containing organic or inorganic compounds characterised by the carbohydrates used, e.g. polysaccharides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/30—Artificial sweetening agents
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
- A23P10/28—Tabletting; Making food bars by compression of a dry powdered mixture
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
- A61K31/047—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates having two or more hydroxy groups, e.g. sorbitol
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
- A61K47/26—Carbohydrates, e.g. sugar alcohols, amino sugars, nucleic acids, mono-, di- or oligo-saccharides; Derivatives thereof, e.g. polysorbates, sorbitan fatty acid esters or glycyrrhizin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/0053—Mouth and digestive tract, i.e. intraoral and peroral administration
- A61K9/0056—Mouth soluble or dispersible forms; Suckable, eatable, chewable coherent forms; Forms rapidly disintegrating in the mouth; Lozenges; Lollipops; Bite capsules; Baked products; Baits or other oral forms for animals
- A61K9/0058—Chewing gums
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/20—Pills, tablets, discs, rods
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G2200/00—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents
- A23G2200/06—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents containing beet sugar or cane sugar if specifically mentioned or containing other carbohydrates, e.g. starches, gums, alcohol sugar, polysaccharides, dextrin or containing high or low amount of carbohydrate
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2200/00—Function of food ingredients
- A23V2200/12—Replacer
- A23V2200/132—Sugar replacer
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Food Science & Technology (AREA)
- Molecular Biology (AREA)
- Veterinary Medicine (AREA)
- Inorganic Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Public Health (AREA)
- Medicinal Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Nutrition Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Zoology (AREA)
- Physiology (AREA)
- Confectionery (AREA)
- Seasonings (AREA)
- Medicinal Preparation (AREA)
Description
粉末状ソルビトールは、きわめて吸水性であることを含めて幾つかの欠点を有する。
成し遂げた。
- 最大150J/gのエンタルピー、
- 200~350μmの間の体積平均径、および
- BET法により求められる0.6m2/g未満、好ましくは0.15~0.4m2/g、さらにより優先的には0.20~0.35m2/gの比表面積
を有することを特徴とする甘味組成物に関する。
- 10%~28%、優先的には15%~25%、またさらにより優先的には20%の少なくとも1種類のガムベースと、
- 20%~70%、優先的には30%~60%の上記甘味組成物と、
- 0.1%~5%、優先的には0.5%~3%、さらにより優先的には1%~1.8%の少なくとも1種類のフレーバーと
を含有するチューインガム組成物に関する。
- 乾燥重量を基準にして80%~95%の結晶性粉末状ソルビトール
を含み、かつ
- 最大150J/gのエンタルピー、
- 200~350μmの体積平均径、および
- BET法により求められる0.6m2/g未満、好ましくは0.15~0.4m2/g、さらにより優先的には0.20~0.35m2/gの比表面積
を有することを特徴とする。
より優先的には試料1g当たり最大142Jのエンタルピーを有する。
単位当たり全表面積(As)を意味し、一般に単位m2/gで表される。
ン製の袋に導入する。
きない削減を可能にする。これは、レシピにより少ないガムベースを投入することが、加えられるフレーバーの量に直接に影響を与えるためである。
- 10%~28%、優先的には15%~25%、さらにより優先的には20%の少なくとも1種類のガムベースと、
- 20%~70%、優先的には30%~60%の上記甘味組成物と、
- 0.1%~5%、優先的には0.5%~3%、さらにより優先的には1%~1.8%の少なくとも1種類のフレーバーと
を含有するチューインガム組成物からなり、この割合は前記組成物の総乾燥重量を基準にした乾燥重量によって表される。
ブオーブンまたはオーブン中で加熱することができる。
- 40%~50%の乾燥物質量を有し、かつ80%~95%のグルコース、3.5%~12%のDP2、および0.5%~8%のDP3を含むグルコースシロップの水素化、
- 続いて前記水素化シロップを、50%を超える、好ましくは70%~80%の乾燥物質含量まで濃縮するステップ、
- 結晶化のステップ、より具体的には造粒のステップ、
- 続いて任意選択で熟成、圧延、および最終ふるい分けのステップ
によって得ることができる。
本発明による甘味組成物を生産する方法
45%の乾燥物質を含有し、かつ乾燥重量で95%のグルコース、4%のDP2、および1%のDP3を含むグルコースシロップを、60バールの水素圧下で水素化する。この水素化の間にpHは約4.5の低い値までゆっくり低下する。次いでpHを、無水ベースで2%以下の還元糖濃度までの水素化を終えるように水酸化ナトリウムを水酸化ナトリウム水溶液の形態で加えることによって8まで上昇させる。
- 乾燥物質を、50%を超える、好ましくは70%~80%の乾燥物質含量まで濃縮するステップ、
- 仏国特許第2202862号明細書に記載の条件下で結晶化させるステップ、および
- 最後に圧延
が続く。
本発明による粉末状甘味組成物の特徴
実施例1で述べた生産方法の実施により得られる組成物を分析して、そのすべての物理化学的特性を求め、ブランド名Neosorb(登録商標)で本出願人の会社によって販売されている市販のソルビトール粉末と比較する。
チューインガムの生産における本発明による甘味組成物の使用法
対照は、ブランド名Neosorb(登録商標)で本出願人の会社によって販売されている市販のソルビトール粉末で行われた。
- 混合(Z-アームミキサー中で45℃で行われる芯(center)の50kgのバッチの生産の分の単位の手順)
0分:溶融したガムベース(50℃で一晩砕いた)とマンニトールとキシリトールを導入する。
3分:Lycasin(登録商標)85/55を加える。
5分:Neosorb(登録商標)ソルビトールまたは水素化した本発明による甘味組成物のいずれかを加える。
9分:グリセロールを加える。
10分:粉末状フレーバーを加える。
12分:液体ミント/バニラフレーバーを加える。
15分:ミキサーから取り出す(生地は約50℃である)。約2kgのブロックを形成し、50%RHおよび20℃で1時間保管する。ブロックは押出のために約48℃であらねばならない。
- 押出(Togum TO-E82装置)。
- ボディの設定温度=36℃。
- ヘッドの設定温度=39℃。
- 圧延(4ステーション:2ステーションでプレカッティング)(Togum TO
-W191装置)。
- マンニトール/タルク(90/10)混合物をチューインガムのストリップに散布する。
- 熟成。
- タブのプレカットシートを約15℃、50%RHで約24時間保管する。
予め得たチューインガムは、チューインガムの試験および等級付けの訓練を受けた15人の審査員によって試験された。
4は最高にしなやかであり、また0は非常に硬いあるいは砕けやすいチューインガムに対応する。
4は非常に強い香味に与えられる等級であり、また0は香味がもはや全くないチューインガムに対応する。
類の試料間で質感に関して、またより具体的にはしなやかさに関して違いに気付かなかった。
チューインガムレシピ中のガムベース含量削減おける本発明による甘味組成物の利点を試験するために、また本発明による前記組成物を他の多価アルコールと比較するために4つの他の試験を行った。これら4つの新しい試験は、ガムベース含量を20%(重量で)に減らして行った。
対照(実施例3の対照組成物)は、チューインガム調製の間、きわめてうまく振る舞う。このガムは、申し分なく弾力性があり、かつ過度に硬くない。失望させる粘着現象がない。
これら予め得たチューインガムは、チューインガムの試験および等級付けの訓練を受けた15人の審査員によって試験された。
4は最高のしなやかさがあり、また0は非常に硬くなった、あるいは砕けやすくなったチューインガムに対応する。
4は、噛み抵抗を示すチューインガムについての等級であり、また0は、噛み始めてすぐに極端に軟らかくなるチューインガムについての等級である。
チューインガムの生産におけるソルビトールシロップと組み合わせた本発明による甘味組
成物の使用
本発明による比表面積の測定
上記で示したように本発明による比表面積は、250μm~841μmの画分で得られる粉末の試料に対して測定される。
試料を調製するために、十分な量の試料を841μmおよび250μmの篩上でふるい分けして、841μm~250μmの間の粒径画分を約3g回収する。
試料を含有するセルをその脱ガス場所に置く。
脱ガスが行われたらすぐに、セルを0.001g以内まで再び計量し、測定場所に置く。次いで分析を、その装置を使用するための取扱説明書を参照することによって行う。
Claims (9)
- - 乾燥重量を基準にして80%~95%の結晶性粉末状ソルビトール及び5%~20%の全還元糖から構成され、前記全還元糖としてマンニトール及びマルチトールを含有し、
- 最大150J/gのエンタルピー、
- 200~350μmの体積加重平均径D4,3、
- BET法により求められる0.6m2/g未満の比表面積
を有することを特徴とする甘味組成物。 - 88%~94.5%の結晶性粉末状ソルビトールを有することを特徴とする、請求項1に記載の甘味組成物。
- エンタルピーが、試料1g当たり最大146Jであることを特徴とする、請求項1または請求項2に記載の甘味組成物。
- 前記ソルビトールが、少なくとも85重量%のγ形結晶からなることを特徴とする、請求項1ないし請求項3のいずれか一項に記載の甘味組成物。
- 相対湿度0%~60%のその重量変化によって求められる吸水性の値が、2.5%~3.4%であることを特徴とする、請求項1ないし請求項4のいずれか一項に記載の甘味組成物。
- 圧縮性が、25%未満であることを特徴とする、請求項1ないし請求項5のいずれか一項に記載の甘味組成物。
- チューインガムの生産における、請求項1ないし請求項6のいずれか一項に記載の甘味組成物の使用。
- - 10%~28%の少なくとも1種類のガムベースと、
- 20%~70%の請求項1ないし請求項6のいずれか一項に記載の甘味組成物と、
- 0.1%~5%の少なくとも1種類のフレーバーと
を含有するチューインガム組成物であって、この割合は前記組成物の総乾燥重量を基準にした乾燥重量によって得られる、組成物。 - 医薬品または食品用途の錠剤の生産における、請求項1ないし請求項6のいずれか一項に記載の甘味組成物の使用。
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FR1456288A FR3023128B1 (fr) | 2014-07-01 | 2014-07-01 | Nouvelle composition edulcorante |
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PCT/FR2015/051820 WO2016001589A1 (fr) | 2014-07-01 | 2015-07-01 | Nouvelle composition edulcorante |
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JP2012501630A (ja) | 2008-09-04 | 2012-01-26 | カーギル インコーポレイテッド | エリスリトールの打錠 |
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