JP7137156B2 - 細長い粒子形状を有するシリカゾルの製造方法 - Google Patents

細長い粒子形状を有するシリカゾルの製造方法 Download PDF

Info

Publication number
JP7137156B2
JP7137156B2 JP2020501086A JP2020501086A JP7137156B2 JP 7137156 B2 JP7137156 B2 JP 7137156B2 JP 2020501086 A JP2020501086 A JP 2020501086A JP 2020501086 A JP2020501086 A JP 2020501086A JP 7137156 B2 JP7137156 B2 JP 7137156B2
Authority
JP
Japan
Prior art keywords
silica sol
acid
producing
exchange resin
raw material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2020501086A
Other languages
English (en)
Japanese (ja)
Other versions
JPWO2019163992A5 (https=
JPWO2019163992A1 (ja
Inventor
智 村上
拓也 福岡
和也 黒岩
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nissan Chemical Corp
Original Assignee
Nissan Chemical Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nissan Chemical Corp filed Critical Nissan Chemical Corp
Publication of JPWO2019163992A1 publication Critical patent/JPWO2019163992A1/ja
Publication of JPWO2019163992A5 publication Critical patent/JPWO2019163992A5/ja
Application granted granted Critical
Publication of JP7137156B2 publication Critical patent/JP7137156B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/141Preparation of hydrosols or aqueous dispersions
    • C01B33/142Preparation of hydrosols or aqueous dispersions by acidic treatment of silicates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/141Preparation of hydrosols or aqueous dispersions
    • C01B33/142Preparation of hydrosols or aqueous dispersions by acidic treatment of silicates
    • C01B33/143Preparation of hydrosols or aqueous dispersions by acidic treatment of silicates of aqueous solutions of silicates
    • C01B33/1435Preparation of hydrosols or aqueous dispersions by acidic treatment of silicates of aqueous solutions of silicates using ion exchangers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00Manufacture or treatment of nanostructures
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/02Amorphous compounds
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/04Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/10Particle morphology extending in one dimension, e.g. needle-like
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/62Submicrometer sized, i.e. from 0.1-1 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/64Nanometer sized, i.e. from 1-100 nanometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Silicon Compounds (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
JP2020501086A 2018-02-26 2019-02-25 細長い粒子形状を有するシリカゾルの製造方法 Active JP7137156B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2018032123 2018-02-26
JP2018032123 2018-02-26
PCT/JP2019/007109 WO2019163992A1 (ja) 2018-02-26 2019-02-25 細長い粒子形状を有するシリカゾルの製造方法

Publications (3)

Publication Number Publication Date
JPWO2019163992A1 JPWO2019163992A1 (ja) 2021-03-04
JPWO2019163992A5 JPWO2019163992A5 (https=) 2022-02-18
JP7137156B2 true JP7137156B2 (ja) 2022-09-14

Family

ID=67688116

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2020501086A Active JP7137156B2 (ja) 2018-02-26 2019-02-25 細長い粒子形状を有するシリカゾルの製造方法

Country Status (6)

Country Link
US (1) US11814295B2 (https=)
JP (1) JP7137156B2 (https=)
KR (1) KR102686976B1 (https=)
CN (1) CN111788153B (https=)
TW (1) TWI850216B (https=)
WO (1) WO2019163992A1 (https=)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7455623B2 (ja) * 2020-03-13 2024-03-26 日揮触媒化成株式会社 粒子連結型シリカ微粒子分散液およびその製造方法、並びに研磨用砥粒分散液
CN113845117B (zh) * 2020-06-28 2023-05-26 中国石油天然气股份有限公司 一种油水两亲性二氧化硅纳米粒子及其制备方法
JP7583597B2 (ja) * 2020-12-09 2024-11-14 日揮触媒化成株式会社 異形シリカ系微粒子分散液およびその製造方法
CN116143131A (zh) * 2023-03-02 2023-05-23 衢州博来纳润电子材料有限公司 一种低金属离子含量硼改性酸性硅溶胶的制备方法
WO2025173621A1 (ja) * 2024-02-14 2025-08-21 株式会社トクヤマ 非晶質シリカ粒子の製造方法、非晶質シリカ粒子、それを含む化粧品、及び非晶質シリカ粒子の製造システム

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007153672A (ja) 2005-12-05 2007-06-21 Catalysts & Chem Ind Co Ltd 異方形状シリカゾルの製造方法
WO2008093422A1 (ja) 2007-02-01 2008-08-07 Nissan Chemical Industries, Ltd. 細長い形状を有するシリカゾルの製造方法
JP2010143784A (ja) 2008-12-18 2010-07-01 Adeka Corp 分鎖状シリカ粒子よりなるシリカゾル及びその製造方法
US9783702B1 (en) 2016-10-19 2017-10-10 Rohm And Haas Electronic Materials Cmp Holdings Inc. Aqueous compositions of low abrasive silica particles

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2803134B2 (ja) 1988-03-16 1998-09-24 日産化学工業株式会社 細長い形状のシリカゾル及びその製造法
JPH085657B2 (ja) 1990-11-21 1996-01-24 触媒化成工業株式会社 シリカゾルとその製法
JP3517913B2 (ja) 1993-10-15 2004-04-12 日産化学工業株式会社 細長い形状のシリカゾルの製造法
JP4264701B2 (ja) * 2002-12-11 2009-05-20 日産化学工業株式会社 低アルカリ金属含有水性シリカゾルの製造方法
JP3691048B1 (ja) * 2004-08-09 2005-08-31 日本化学工業株式会社 高純度コロイダルシリカの製造方法
TW200833606A (en) 2007-02-02 2008-08-16 Nissan Chemical Ind Ltd Process for producing silica sol having elongated shape
JP5398963B2 (ja) * 2007-04-23 2014-01-29 日本化学工業株式会社 低ナトリウムで非球状のコロイダルシリカ
CN101397139B (zh) 2008-09-09 2012-01-04 苏州纳迪微电子有限公司 高纯度硅溶胶及其制备方法
JP5457070B2 (ja) * 2009-05-14 2014-04-02 日本化学工業株式会社 コロイダルシリカおよびその製造方法
JP5431120B2 (ja) 2009-11-06 2014-03-05 日本化学工業株式会社 コロイダルシリカの製造方法
TWI549911B (zh) 2011-12-28 2016-09-21 日揮觸媒化成股份有限公司 高純度氧化矽溶膠及其製造方法
JP6414547B2 (ja) * 2013-06-10 2018-10-31 日産化学株式会社 シリカゾル及びシリカゾルの製造方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007153672A (ja) 2005-12-05 2007-06-21 Catalysts & Chem Ind Co Ltd 異方形状シリカゾルの製造方法
WO2008093422A1 (ja) 2007-02-01 2008-08-07 Nissan Chemical Industries, Ltd. 細長い形状を有するシリカゾルの製造方法
JP2010143784A (ja) 2008-12-18 2010-07-01 Adeka Corp 分鎖状シリカ粒子よりなるシリカゾル及びその製造方法
US9783702B1 (en) 2016-10-19 2017-10-10 Rohm And Haas Electronic Materials Cmp Holdings Inc. Aqueous compositions of low abrasive silica particles

Also Published As

Publication number Publication date
TWI850216B (zh) 2024-08-01
WO2019163992A1 (ja) 2019-08-29
US11814295B2 (en) 2023-11-14
US20200392004A1 (en) 2020-12-17
KR102686976B1 (ko) 2024-07-19
JPWO2019163992A1 (ja) 2021-03-04
KR20200124249A (ko) 2020-11-02
TW201936500A (zh) 2019-09-16
CN111788153A (zh) 2020-10-16
CN111788153B (zh) 2023-12-19

Similar Documents

Publication Publication Date Title
JP7137157B2 (ja) 細長い粒子形状を有するシリカゾルの製造方法
JP7137156B2 (ja) 細長い粒子形状を有するシリカゾルの製造方法
JP5019076B2 (ja) 細長い形状を有するシリカゾルの製造方法
EP2678399B1 (de) Verfahren zur herstellung wässriger kolloidaler silikasole hoher reinheit aus alkalimetallsilikatlösungen
JP5221517B2 (ja) アルミ改質コロイダルシリカ及びその製造方法
CN110139829B (zh) 聚铝盐及其在制备高纯度胶体铝-二氧化硅复合颗粒和沸石中的用途
JP4222582B2 (ja) 高純度シリカゾルの製造方法
JP5905767B2 (ja) 中性コロイダルシリカ分散液の分散安定化方法及び分散安定性に優れた中性コロイダルシリカ分散液
JP3837754B2 (ja) 結晶性酸化第二セリウムの製造方法
MX2013004813A (es) Sintesis de titanato de sodio.
JP3758391B2 (ja) 高純度シリカ水性ゾル及びその製造方法
DE102011004534A1 (de) Verfahren zur Herstellung wässriger kolloidaler Silikasole hoher Reinheit aus Alkalimetallsilikatlösungen
JP6209072B2 (ja) シリカ粒子の製造方法
JPH0217932A (ja) 改質無機質粒子及びその製法
KR20060048901A (ko) 고순도 콜로이드실리카의 제조 방법
TWI900801B (zh) 鏈狀之膠體二氧化矽粒子分散溶膠及其製造方法
WO2015068828A1 (ja) チューブ状アルミニウムケイ酸塩
WO2015068830A1 (ja) チューブ状アルミニウムケイ酸塩の製造方法
JP2015117148A (ja) チューブ状アルミニウムケイ酸塩及びアルミニウムケイ酸塩の製造方法

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20220209

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20220209

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20220803

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20220816

R151 Written notification of patent or utility model registration

Ref document number: 7137156

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R151