JP6310860B2 - バナジウム系フリット材料、結合剤、及び/又は溶媒、並びにその製造方法 - Google Patents
バナジウム系フリット材料、結合剤、及び/又は溶媒、並びにその製造方法 Download PDFInfo
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- JP6310860B2 JP6310860B2 JP2014550408A JP2014550408A JP6310860B2 JP 6310860 B2 JP6310860 B2 JP 6310860B2 JP 2014550408 A JP2014550408 A JP 2014550408A JP 2014550408 A JP2014550408 A JP 2014550408A JP 6310860 B2 JP6310860 B2 JP 6310860B2
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- 239000000463 material Substances 0.000 title claims description 191
- 239000011230 binding agent Substances 0.000 title claims description 66
- 238000004519 manufacturing process Methods 0.000 title claims description 17
- 229910052720 vanadium Inorganic materials 0.000 title description 26
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 title description 23
- 239000002904 solvent Substances 0.000 title description 3
- 239000000203 mixture Substances 0.000 claims description 96
- 239000011521 glass Substances 0.000 claims description 92
- 239000000758 substrate Substances 0.000 claims description 82
- QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Chemical compound [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 claims description 55
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 52
- 238000000034 method Methods 0.000 claims description 32
- 239000011787 zinc oxide Substances 0.000 claims description 26
- -1 polypropylene carbonate Polymers 0.000 claims description 19
- XHCLAFWTIXFWPH-UHFFFAOYSA-N [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] XHCLAFWTIXFWPH-UHFFFAOYSA-N 0.000 claims description 15
- 229910001935 vanadium oxide Inorganic materials 0.000 claims description 15
- 229920000379 polypropylene carbonate Polymers 0.000 claims description 6
- 239000003566 sealing material Substances 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims 1
- 239000000654 additive Substances 0.000 description 59
- 238000010438 heat treatment Methods 0.000 description 36
- 238000002844 melting Methods 0.000 description 34
- 230000008018 melting Effects 0.000 description 34
- 229910004298 SiO 2 Inorganic materials 0.000 description 27
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 26
- 150000001875 compounds Chemical class 0.000 description 19
- 230000000996 additive effect Effects 0.000 description 16
- 238000007789 sealing Methods 0.000 description 14
- 229910021591 Copper(I) chloride Inorganic materials 0.000 description 10
- OXBLHERUFWYNTN-UHFFFAOYSA-M copper(I) chloride Chemical compound [Cu]Cl OXBLHERUFWYNTN-UHFFFAOYSA-M 0.000 description 10
- 239000005341 toughened glass Substances 0.000 description 10
- 238000002425 crystallisation Methods 0.000 description 9
- 230000008025 crystallization Effects 0.000 description 9
- 239000000155 melt Substances 0.000 description 9
- 230000002093 peripheral effect Effects 0.000 description 9
- 238000002485 combustion reaction Methods 0.000 description 8
- 230000008569 process Effects 0.000 description 7
- 239000013067 intermediate product Substances 0.000 description 6
- 238000002411 thermogravimetry Methods 0.000 description 6
- 229910005793 GeO 2 Inorganic materials 0.000 description 5
- 101100496858 Mus musculus Colec12 gene Proteins 0.000 description 5
- 229910021607 Silver chloride Inorganic materials 0.000 description 5
- 229910008449 SnF 2 Inorganic materials 0.000 description 5
- 229910006404 SnO 2 Inorganic materials 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 230000014759 maintenance of location Effects 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 5
- 229910000679 solder Inorganic materials 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 4
- 238000002835 absorbance Methods 0.000 description 4
- AYJRCSIUFZENHW-UHFFFAOYSA-L barium carbonate Chemical compound [Ba+2].[O-]C([O-])=O AYJRCSIUFZENHW-UHFFFAOYSA-L 0.000 description 4
- GNTDGMZSJNCJKK-UHFFFAOYSA-N divanadium pentaoxide Chemical compound O=[V](=O)O[V](=O)=O GNTDGMZSJNCJKK-UHFFFAOYSA-N 0.000 description 4
- 238000010304 firing Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 125000006850 spacer group Chemical group 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- PRPINYUDVPFIRX-UHFFFAOYSA-N 1-naphthaleneacetic acid Chemical compound C1=CC=C2C(CC(=O)O)=CC=CC2=C1 PRPINYUDVPFIRX-UHFFFAOYSA-N 0.000 description 3
- 239000004593 Epoxy Substances 0.000 description 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 3
- 238000002386 leaching Methods 0.000 description 3
- 230000031700 light absorption Effects 0.000 description 3
- 230000005855 radiation Effects 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- AYJRCSIUFZENHW-DEQYMQKBSA-L barium(2+);oxomethanediolate Chemical compound [Ba+2].[O-][14C]([O-])=O AYJRCSIUFZENHW-DEQYMQKBSA-L 0.000 description 2
- 230000008033 biological extinction Effects 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- 229910001510 metal chloride Inorganic materials 0.000 description 2
- 229910044991 metal oxide Inorganic materials 0.000 description 2
- 150000004706 metal oxides Chemical class 0.000 description 2
- 229920000609 methyl cellulose Polymers 0.000 description 2
- 239000001923 methylcellulose Substances 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- GVNVAWHJIKLAGL-UHFFFAOYSA-N 2-(cyclohexen-1-yl)cyclohexan-1-one Chemical compound O=C1CCCCC1C1=CCCCC1 GVNVAWHJIKLAGL-UHFFFAOYSA-N 0.000 description 1
- 229910015902 Bi 2 O 3 Inorganic materials 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 101150065749 Churc1 gene Proteins 0.000 description 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- 102100038239 Protein Churchill Human genes 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000005347 annealed glass Substances 0.000 description 1
- 206010003549 asthenia Diseases 0.000 description 1
- 230000003416 augmentation Effects 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- CSSYLTMKCUORDA-UHFFFAOYSA-N barium(2+);oxygen(2-) Chemical class [O-2].[Ba+2] CSSYLTMKCUORDA-UHFFFAOYSA-N 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052797 bismuth Inorganic materials 0.000 description 1
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 1
- FJDQFPXHSGXQBY-UHFFFAOYSA-L caesium carbonate Chemical compound [Cs+].[Cs+].[O-]C([O-])=O FJDQFPXHSGXQBY-UHFFFAOYSA-L 0.000 description 1
- 229910000024 caesium carbonate Inorganic materials 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 230000021615 conjugation Effects 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 238000000113 differential scanning calorimetry Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 125000003700 epoxy group Chemical group 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000009477 glass transition Effects 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 230000005802 health problem Effects 0.000 description 1
- 239000005346 heat strengthened glass Substances 0.000 description 1
- 238000002329 infrared spectrum Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 238000010309 melting process Methods 0.000 description 1
- 239000011859 microparticle Substances 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 229910000476 molybdenum oxide Inorganic materials 0.000 description 1
- 229910000484 niobium oxide Inorganic materials 0.000 description 1
- URLJKFSTXLNXLG-UHFFFAOYSA-N niobium(5+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[Nb+5].[Nb+5] URLJKFSTXLNXLG-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- PQQKPALAQIIWST-UHFFFAOYSA-N oxomolybdenum Chemical compound [Mo]=O PQQKPALAQIIWST-UHFFFAOYSA-N 0.000 description 1
- BPUBBGLMJRNUCC-UHFFFAOYSA-N oxygen(2-);tantalum(5+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[Ta+5].[Ta+5] BPUBBGLMJRNUCC-UHFFFAOYSA-N 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920005596 polymer binder Polymers 0.000 description 1
- 239000002491 polymer binding agent Substances 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
- 229910001936 tantalum oxide Inorganic materials 0.000 description 1
- 229910052714 tellurium Inorganic materials 0.000 description 1
- PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 description 1
- LPHBARMWKLYWRA-UHFFFAOYSA-N thallium(iii) oxide Chemical compound [O-2].[O-2].[O-2].[Tl+3].[Tl+3] LPHBARMWKLYWRA-UHFFFAOYSA-N 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 238000001429 visible spectrum Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/24—Fusion seal compositions being frit compositions having non-frit additions, i.e. for use as seals between dissimilar materials, e.g. glass and metal; Glass solders
-
- E—FIXED CONSTRUCTIONS
- E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
- E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
- E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
- E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
- E06B3/677—Evacuating or filling the gap between the panes ; Equilibration of inside and outside pressure; Preventing condensation in the gap between the panes; Cleaning the gap between the panes
- E06B3/6775—Evacuating or filling the gap during assembly
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B23/00—Re-forming shaped glass
- C03B23/20—Uniting glass pieces by fusing without substantial reshaping
- C03B23/24—Making hollow glass sheets or bricks
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C27/00—Joining pieces of glass to pieces of other inorganic material; Joining glass to glass other than by fusing
- C03C27/06—Joining glass to glass by processes other than fusing
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C27/00—Joining pieces of glass to pieces of other inorganic material; Joining glass to glass other than by fusing
- C03C27/06—Joining glass to glass by processes other than fusing
- C03C27/10—Joining glass to glass by processes other than fusing with the aid of adhesive specially adapted for that purpose
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/062—Glass compositions containing silica with less than 40% silica by weight
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/12—Silica-free oxide glass compositions
- C03C3/122—Silica-free oxide glass compositions containing oxides of As, Sb, Bi, Mo, W, V, Te as glass formers
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
- C03C8/04—Frit compositions, i.e. in a powdered or comminuted form containing zinc
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
- C03C8/06—Frit compositions, i.e. in a powdered or comminuted form containing halogen
-
- E—FIXED CONSTRUCTIONS
- E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
- E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
- E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
- E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
- E06B3/6612—Evacuated glazing units
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2207/00—Compositions specially applicable for the manufacture of vitreous enamels
-
- E—FIXED CONSTRUCTIONS
- E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
- E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
- E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
- E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
- E06B3/673—Assembling the units
-
- E—FIXED CONSTRUCTIONS
- E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
- E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
- E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
- E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
- E06B3/673—Assembling the units
- E06B3/67326—Assembling spacer elements with the panes
- E06B3/67334—Assembling spacer elements with the panes by soldering; Preparing the panes therefor
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A30/00—Adapting or protecting infrastructure or their operation
- Y02A30/24—Structural elements or technologies for improving thermal insulation
- Y02A30/249—Glazing, e.g. vacuum glazing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02B—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO BUILDINGS, e.g. HOUSING, HOUSE APPLIANCES OR RELATED END-USER APPLICATIONS
- Y02B80/00—Architectural or constructional elements improving the thermal performance of buildings
- Y02B80/22—Glazing, e.g. vaccum glazing
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Geochemistry & Mineralogy (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Ceramic Engineering (AREA)
- Glass Compositions (AREA)
- Joining Of Glass To Other Materials (AREA)
Description
本出願は、2011年9月21日に出願された米国特許出願第13/238,358号の一部継続出願であり、これは2011年2月22日に出願された米国出願第12/929,875号の一部継続出願で、全体の内容は参照に本明細書として含まれる。
1)発明のある実施形態において、ガラス軟化温度を低下及び/又は結晶化を減少させることに役立つことができる1〜10モル%の間のSnCl2;
2)発明のある実施形態において、ガラス軟化温度を低下させることに役立つことができる1〜5モル%の間のCuCl2;
3)発明のある実施形態において、ガラス軟化温度を低下させることに役立つことができる1〜6モル%の間のMoO3;
4)発明のある実施形態において、基板ガラスに対するガラス流動性及び/又は濡れ性を向上させることに役立つことができる1〜10モル%の間のTeO2;
5)発明のある実施形態において、ガラス軟化温度を上昇及び/又は結晶化温度を上昇させることに役立つことができる0.5〜5モル%の間のTa2O5;
6)発明のある実施形態において、ガラス軟化温度を上昇及び/又は結晶化温度を上昇させることに役立つことができる0.5〜6モル%の間のNb2O5;
7)発明のある実施形態において、軟化性、耐候性、化学的耐久性、及び/又は機械的強度を向上させることに役立つことができる0.5〜5モル%の間のAl2O3;
8)発明のある実施形態において、軟化性、耐候性、化学的耐久性、及び/又は機械的強度を向上させることに役立つことができる0.5〜5モル%の間のSiO2;
9)発明のある実施形態において、メルトフローの向上及び/又は濡れ性の低下に役立つことができる0.5〜4モル%の間のCsCO3。
結合剤の一例は、エンパワーマテリアルズ社(Empower Materials Inc)から市販される材料(商品名QPAC 40)である。上記のように、図13において、このような実施形態2及び実施形態3のTGA分析によれば、結合剤材料の燃焼が約250〜275℃であると示された。
Claims (11)
- 真空断熱ガラス(VIG)ユニットを製造する方法であって、
第1ガラス基板及び/又は第2ガラス基板に直接又は間接的に、少なくともフリット材料及び結合剤溶液を含むシール材料を提供する、ステップと、
実質的に平行で互いに離隔された前記第1及び第2ガラス基板を提供するステップであり、前記シール材料が前記ガラス基板の少なくとも1つの上に提供されて前記第1ガラス基板と前記第2ガラス基板との間に空隙を定め、前記シール材料の少なくとも一部は前記第1ガラス基板と前記第2ガラス基板との間に位置する、ステップと、
400℃未満のガラス軟化温度を有する前記フリット材料を溶融するように前記フリット材料にエネルギを印加するステップと、
を含み、
前記エネルギの印加によって、実質的に前記シール材料の結合剤溶液が燃焼し、前記エネルギ印加後に前記第1及び第2ガラス基板が直接又は間接的に互いに封止され、
前記フリット材料は次の成分、すなわち、
酸化バナジウムの成分を正規化されたモル%で45%〜50%、
酸化バリウムの成分を正規化されたモル%で20%〜23%、及び
酸化亜鉛の成分を正規化されたモル%で19%〜22%、
MoO3の成分を正規化されたモル%で1〜6%、
TeO2の成分を正規化されたモル%で1〜10%、
Ta2O5の成分を正規化されたモル%で0.5〜5%、
Nb2O5の成分を正規化されたモル%で0.5〜6%、
を含む組成物から形成される、
真空断熱ガラス(VIG)ユニットの製造方法。 - 前記フリット材料に前記エネルギを印加するステップは、
前記フリット材料の温度を第1期間中に第1温度で保持するステップと、
前記フリット材料の温度を第2期間中に前記ガラス軟化温度まで上昇させるステップと、
を含む請求項1に記載の方法。 - 前記第1期間は、前記第2期間より長い、
請求項2に記載の方法。 - 前記第1期間は、2分から15分の間である、
請求項2又は請求項3に記載の方法。 - 前記第1期間は、5分から10分の間である、
請求項2〜請求項4のいずれか一項に記載の方法。 - 前記第2期間は、5分未満である、
請求項2〜請求項5のいずれか一項に記載の方法。 - 前記第2期間は、3分未満である、
請求項2〜請求項6のいずれか一項に記載の方法。 - 前記第1温度は、300℃未満である、
請求項2〜請求項7のいずれか一項に記載の方法。 - 前記エネルギを印加するステップの前に、前記フリット材料と前記結合剤溶液との比率を5:1とする、
請求項1〜請求項8のいずれか一項に記載の方法。 - 前記結合剤溶液は、ポリプロピレンカーボネイト又はポリエチレンカーボネイトを含む、
請求項1〜請求項9のいずれか一項に記載の方法。 - 少なくとも前記フリット材料によってシールを形成した後、前記第1ガラス基板と前記第2ガラス基板との間の空隙を大気圧未満の圧力まで真空処理するステップをさらに含む、
請求項1に記載の方法。
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PCT/US2012/071324 WO2013101748A1 (en) | 2011-12-29 | 2012-12-21 | Vanadium-based frit materials, sealing material and methods of making the same and using the same for sealing vacuum insulating glass |
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Families Citing this family (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8802203B2 (en) | 2011-02-22 | 2014-08-12 | Guardian Industries Corp. | Vanadium-based frit materials, and/or methods of making the same |
US9309146B2 (en) | 2011-02-22 | 2016-04-12 | Guardian Industries Corp. | Vanadium-based frit materials, binders, and/or solvents and methods of making the same |
US9359247B2 (en) | 2011-02-22 | 2016-06-07 | Guardian Industries Corp. | Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same |
US9290408B2 (en) | 2011-02-22 | 2016-03-22 | Guardian Industries Corp. | Vanadium-based frit materials, and/or methods of making the same |
US9458052B2 (en) * | 2011-02-22 | 2016-10-04 | Guardian Industries Corp. | Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same |
EP3925937B1 (en) * | 2012-01-20 | 2022-12-07 | Guardian Glass, LLC | Process of using a coefficient of thermal expansion filler for frit materials |
WO2015087718A1 (ja) * | 2013-12-11 | 2015-06-18 | 日立化成株式会社 | 断熱部材及び低融点ガラス組成物、並びに封止材料ペースト |
US9988302B2 (en) | 2014-02-04 | 2018-06-05 | Guardian Glass, LLC | Frits for use in vacuum insulating glass (VIG) units, and/or associated methods |
US9593527B2 (en) | 2014-02-04 | 2017-03-14 | Guardian Industries Corp. | Vacuum insulating glass (VIG) unit with lead-free dual-frit edge seals and/or methods of making the same |
US10279565B2 (en) | 2016-02-11 | 2019-05-07 | Guardian Glass, LLC | Vacuum insulating glass window unit including edge seal and/or method of making the same |
JP6865391B2 (ja) * | 2016-09-30 | 2021-04-28 | パナソニックIpマネジメント株式会社 | ガラスパネルユニット、ガラス窓およびガラスパネルユニットの製造方法 |
CN108002717A (zh) * | 2016-10-31 | 2018-05-08 | 张跃 | 一种真空玻璃 |
US12065872B2 (en) * | 2017-02-17 | 2024-08-20 | Vkr Holding A/S | Top frit heat treatment |
CN109133648B (zh) * | 2018-09-30 | 2021-10-01 | 中国建筑材料科学研究总院有限公司 | 一种低软化点无铅玻璃组合物及包含该玻璃组合物的低温无铅封接材料和低温无铅焊接料浆 |
WO2020125880A1 (en) * | 2018-12-21 | 2020-06-25 | Vkr Holding A/S | Vacuum insulated glazing unit with dense side seal material |
US20200399949A1 (en) | 2019-06-18 | 2020-12-24 | Guardian Glass, LLC | Flanged tube for vacuum insulated glass (vig) unit evacuation and hermetic sealing, vig unit including flanged tube, and associated methods |
EP3999708A1 (en) * | 2019-07-15 | 2022-05-25 | VKR Holding A/S | Manufacturing of vacuum insulated glazing unit |
Family Cites Families (141)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2727301A (en) | 1952-02-04 | 1955-12-20 | Continental Can Co | Method of soldering a lap side seam in a can body |
US3222153A (en) | 1955-01-10 | 1965-12-07 | Libbey Owens Ford Glass Co | Method of producing multiple sheet glazing units |
US2936923A (en) | 1956-10-08 | 1960-05-17 | Owens Illinois Glass Co | Laminated joint for glass parts and method of sealing |
US2988852A (en) | 1957-12-11 | 1961-06-20 | Owens Illinois Glass Co | Method of thermally sealing hollow glass articles at minimal temperatures |
US3120433A (en) | 1960-02-05 | 1964-02-04 | Owens Illinois Glass Co | Method of joining glass components by radiant energy |
DE1229272B (de) | 1963-03-12 | 1966-11-24 | Libbey Owens Ges Fuer Maschine | Mehrscheiben-Isolierglas |
US3252811A (en) | 1963-12-11 | 1966-05-24 | Corning Glass Works | Glass-ceramic bodies and method of making them |
US3331659A (en) | 1964-03-31 | 1967-07-18 | Malloy Frank | Process for producing lead titanate powder |
US3981753A (en) | 1968-04-30 | 1976-09-21 | Kennecott Copper Corporation | Stop-weld composition and the method of using it |
US3650778A (en) | 1969-10-29 | 1972-03-21 | Fairchild Camera Instr Co | Low-expansion, low-melting zinc phosphovanadate glass compositions |
JPS526097B2 (ja) | 1972-03-14 | 1977-02-18 | ||
US3837866A (en) | 1972-04-24 | 1974-09-24 | Corning Glass Works | Low melting vanadate glasses |
US3862830A (en) | 1973-07-18 | 1975-01-28 | Rca Corp | Method of forming vitreous enclosures for liquid crystal cells |
US3947260A (en) | 1975-01-02 | 1976-03-30 | Owens-Illinois, Inc. | Method of sealing and spacing glass substrates of gaseous discharge display panels used at high altitudes |
US4045200A (en) | 1975-01-02 | 1977-08-30 | Owens-Illinois, Inc. | Method of forming glass substrates with pre-attached sealing media |
GB1566558A (en) | 1976-09-03 | 1980-05-08 | Standard Telephones Cables Ltd | Large liquid crystal cells |
CH622358A5 (ja) | 1977-09-06 | 1981-03-31 | Bbc Brown Boveri & Cie | |
JPS5446215A (en) | 1977-09-21 | 1979-04-12 | Hitachi Ltd | Sealing glass |
US4186023A (en) | 1978-05-01 | 1980-01-29 | Technology Glass Corporation | Sealing glass composition |
JPS54150150A (en) | 1978-05-17 | 1979-11-26 | Hitachi Ltd | Production of liquid crystal display element |
US4221604A (en) | 1978-05-22 | 1980-09-09 | Corning Glass Works | Hermetic seals |
FR2446263A1 (fr) | 1979-01-12 | 1980-08-08 | Corning Glass Works | Verre de scellement presentant un coefficient d'absorption eleve pour les rayons infra-rouges |
SU852811A1 (ru) | 1979-12-18 | 1981-08-07 | Грузинский Ордена Ленина И Орденатрудового Красного Знамени Политехническийинститут Им. B.И.Ленина | Черна глазурь |
US4314031A (en) | 1980-06-17 | 1982-02-02 | Corning Glass Works | Tin-phosphorus oxyfluoride glasses |
DE3126996A1 (de) | 1981-03-21 | 1982-09-30 | Karl 7531 Neuhausen Lenhardt | Verfahren zum herstellen des festen verbundes von isolierglasscheiben |
US4450441A (en) | 1981-08-27 | 1984-05-22 | Person Herman R | Dot matrix plasma display and method for driving same |
US4482579A (en) | 1983-01-17 | 1984-11-13 | Sony Corporation | Apparatus for supplying viscous material |
US4801488A (en) | 1984-09-19 | 1989-01-31 | Olin Corporation | Sealing glass composite |
JPH062584B2 (ja) | 1984-12-28 | 1994-01-12 | ソニー株式会社 | チタン酸鉛微結晶及びその製造方法 |
SU1276639A1 (ru) | 1985-06-11 | 1986-12-15 | Днепропетровский химико-технологический институт им.Ф.Э.Дзержинского | Припой из стекла |
US4683154A (en) | 1985-08-19 | 1987-07-28 | The United States Of America As Represented By The United States Department Of Energy | Laser sealed vacuum insulation window |
US4743302A (en) | 1986-06-06 | 1988-05-10 | Vlsi Packaging Materials, Inc. | Low melting glass composition |
US4788471A (en) | 1986-11-21 | 1988-11-29 | Zenith Electronics Corporation | Sealing for CRT components |
SU1578093A1 (ru) | 1987-08-26 | 1990-07-15 | Организация П/Я А-1695 | Глазурный шликер дл керамических конденсаторов |
US4820365A (en) | 1987-09-30 | 1989-04-11 | Dimension Industries, Inc. | Glass edge sealant curing system |
SU1590472A1 (ru) | 1987-11-16 | 1990-09-07 | Киевский Политехнический Институт Им.50-Летия Великой Октябрьской Социалистической Революции | Нефриттованна глазурь |
JP2767276B2 (ja) | 1989-04-06 | 1998-06-18 | 株式会社日立製作所 | 封着材料 |
JPH0764588B2 (ja) | 1989-04-28 | 1995-07-12 | 日本電気硝子株式会社 | 被覆用ガラス組成物 |
US5657607A (en) | 1989-08-23 | 1997-08-19 | University Of Sydney | Thermally insulating glass panel and method of construction |
US5013360A (en) | 1989-09-15 | 1991-05-07 | Vlsi Packaging Materials, Inc. | Sealing glass compositions |
SU1694561A1 (ru) | 1990-01-08 | 1991-11-30 | Государственный научно-исследовательский институт строительной керамики | Глазурь |
US5089446A (en) | 1990-10-09 | 1992-02-18 | Corning Incorporated | Sealing materials and glasses |
SU1791433A1 (ru) | 1991-04-11 | 1993-01-30 | Gnii Stroitelnoj Keramiki | Глaзуpь |
WO1993002980A1 (en) * | 1991-08-07 | 1993-02-18 | Vlsi Packaging Materials, Inc. | Low temperature lead vanadium sealing glass compositions |
US5188990A (en) | 1991-11-21 | 1993-02-23 | Vlsi Packaging Materials | Low temperature sealing glass compositions |
ATE194205T1 (de) | 1992-01-31 | 2000-07-15 | Univ Sydney | Verbesserungen für thermisch isolierende glasscheiben |
US5424605A (en) | 1992-04-10 | 1995-06-13 | Silicon Video Corporation | Self supporting flat video display |
US5355051A (en) | 1992-12-21 | 1994-10-11 | Zenith Electronics Corporation | CRT bulb having a front panel with a higher CTE than its funnel |
JP3339647B2 (ja) | 1993-03-03 | 2002-10-28 | 旭テクノグラス株式会社 | 無鉛系低融点ガラス及び封着用ガラス組成物 |
JP3554325B2 (ja) | 1993-06-30 | 2004-08-18 | ザ・ユニバーシティ・オブ・シドニー | 断熱ガラスパネルおよびその製造方法 |
US5336644A (en) | 1993-07-09 | 1994-08-09 | Johnson Matthey Inc. | Sealing glass compositions |
DE69429699T2 (de) | 1993-09-27 | 2002-08-14 | Saint-Gobain Glass France, Courbevoie | Isolierverglasung und Vakuumerzeugungsverfahren dafür |
US5516733A (en) | 1994-03-31 | 1996-05-14 | Corning Incorporated | Fusion seal and sealing mixtures |
US5489321A (en) | 1994-07-14 | 1996-02-06 | Midwest Research Institute | Welding/sealing glass-enclosed space in a vacuum |
DE4430710C1 (de) | 1994-08-30 | 1996-05-02 | Jenaer Glaswerk Gmbh | Borsäurearmes Borosilikatglas und seine Verwendung |
AUPM888994A0 (en) | 1994-10-19 | 1994-11-10 | University Of Sydney, The | Design improvement to vacuum glazing |
US5643840A (en) | 1994-12-29 | 1997-07-01 | Nippon Electric Glass Co., Ltd. | Low temperature sealing composition with reduced SiO2 content but |
GB9500798D0 (en) | 1995-01-16 | 1995-03-08 | Cookson Group Plc | Sealing glass paste |
US5766053A (en) | 1995-02-10 | 1998-06-16 | Micron Technology, Inc. | Internal plate flat-panel field emission display |
US5534469A (en) | 1995-09-12 | 1996-07-09 | Nippon Electric Glass Co., Ltd. | Low temperature non-crystallizing sealing glass |
DE19545422C2 (de) | 1995-12-06 | 1998-11-19 | Inst Physikalische Hochtech Ev | Verfahren zum anodischen Bonden von Siliziumkomponenten mit Glaskomponenten |
GB9713831D0 (en) | 1997-06-30 | 1997-09-03 | Fry Metals Inc | Sealing glass paste for cathode ray tubes |
DE19733443A1 (de) | 1997-08-02 | 1999-02-04 | Hauni Maschinenbau Ag | Vorrichtung zum Fördern eines Stranges der tabakverarbeitenden Industrie |
CN1212993C (zh) * | 1998-03-17 | 2005-08-03 | 日本板硝子株式会社 | 双层玻璃 |
US6326685B1 (en) | 1998-05-04 | 2001-12-04 | Agere Systems Guardian Corp. | Low thermal expansion composite comprising bodies of negative CTE material disposed within a positive CTE matrix |
CA2332811A1 (en) | 1998-05-19 | 1999-12-16 | Corning Incorporated | Negative thermal expansion materials including method of preparation and uses therefor |
ID27093A (id) | 1999-03-05 | 2001-03-01 | Uni Charm Corp | Lembaran komposit dan metode pembuatannya |
US6336984B1 (en) | 1999-09-24 | 2002-01-08 | Guardian Industries Corporation | Vacuum IG window unit with peripheral seal at least partially diffused at temper |
US6365242B1 (en) | 1999-07-07 | 2002-04-02 | Guardian Industries Corp. | Peripheral seal for vacuum IG window unit |
US6399169B1 (en) | 1999-07-07 | 2002-06-04 | Guardian Industries Corp. | Vacuum IG window unit with dual peripheral seal |
US6946171B1 (en) | 1999-09-22 | 2005-09-20 | Guardian Industries Corp. | Vacuum IG pillar with lubricating and/or reflective coating |
US6478911B1 (en) | 2000-09-27 | 2002-11-12 | Guardian Industries Corp. | Vacuum IG window unit with edge seal formed via microwave curing, and corresponding method of making the same |
US6444281B1 (en) | 1999-10-13 | 2002-09-03 | Guardian Industries Corp. | Vacuum IG window unit with spacers between first and second edge seals |
US6383580B1 (en) | 1999-11-12 | 2002-05-07 | Guardian Industries Corp. | Vacuum IG window unit with edge mounted pump-out tube |
US6503583B2 (en) | 1999-11-16 | 2003-01-07 | Guardian Industries Corp. | Vacuum IG window unit with fiber inclusive edge seal |
US6300263B1 (en) | 1999-12-16 | 2001-10-09 | Corning Incorporated | Low-expansion cordierite glass ceramics |
US6391809B1 (en) | 1999-12-30 | 2002-05-21 | Corning Incorporated | Copper alumino-silicate glasses |
US6541083B1 (en) | 2000-01-11 | 2003-04-01 | Guardian Industries Corp. | Vacuum IG unit with alkali silicate edge seal and/or spacers |
US20050191515A1 (en) | 2000-07-20 | 2005-09-01 | Shipley Company, L.L.C. | Very low thermal expansion composite |
WO2002014640A1 (en) | 2000-08-11 | 2002-02-21 | Anthony John Cooper | Double glazing |
US6701749B2 (en) | 2000-09-27 | 2004-03-09 | Guardian Industries Corp. | Vacuum IG window unit with edge seal at least partially diffused at temper and completed via microwave curing, and corresponding method of making the same |
BR0114285A (pt) | 2000-10-02 | 2003-07-29 | Corning Inc | Cerâmica de aluminosilicato de lìtio |
JP2002137939A (ja) | 2000-10-30 | 2002-05-14 | Matsushita Electric Ind Co Ltd | 表示パネルの製造方法およびその製造装置 |
JP4203235B2 (ja) | 2001-07-05 | 2008-12-24 | 日本板硝子株式会社 | ガラスパネル |
US6692600B2 (en) | 2001-09-14 | 2004-02-17 | Guardian Industries Corp. | VIG evacuation with plasma excitation |
JP2003192378A (ja) * | 2001-12-25 | 2003-07-09 | Yamato Denshi Kk | 封着加工用無鉛低融点ガラス |
US7105235B2 (en) | 2002-05-17 | 2006-09-12 | Her Majesty The Queen In Right Of Canada As Represented By The Minister Of Natural Resources | Isotropic zero CTE reinforced composite materials |
US6992030B2 (en) | 2002-08-29 | 2006-01-31 | Corning Incorporated | Low-density glass for flat panel display substrates |
JP2004182567A (ja) | 2002-12-05 | 2004-07-02 | Nippon Sheet Glass Co Ltd | 真空ガラスパネルの製造方法、及び該製造方法により製造された真空ガラスパネル |
JP4299021B2 (ja) * | 2003-02-19 | 2009-07-22 | ヤマト電子株式会社 | 封着加工材及び封着加工用ペースト |
US6998776B2 (en) * | 2003-04-16 | 2006-02-14 | Corning Incorporated | Glass package that is hermetically sealed with a frit and method of fabrication |
US7344901B2 (en) | 2003-04-16 | 2008-03-18 | Corning Incorporated | Hermetically sealed package and method of fabricating of a hermetically sealed package |
WO2005000755A1 (ja) | 2003-06-27 | 2005-01-06 | Yamato Electronic Co., Ltd. | 封着加工用無鉛ガラス材とこれを用いた封着加工物及び封着加工方法 |
JP4682556B2 (ja) | 2003-09-19 | 2011-05-11 | 日本電気硝子株式会社 | 低融点封着組成物、低融点ガラスペースト及び低融点ガラスタブレット |
US20050110168A1 (en) | 2003-11-20 | 2005-05-26 | Texas Instruments Incorporated | Low coefficient of thermal expansion (CTE) semiconductor packaging materials |
JP4393308B2 (ja) | 2004-08-24 | 2010-01-06 | キヤノン株式会社 | 画像表示装置の製造方法 |
US7435695B2 (en) | 2004-12-09 | 2008-10-14 | B.G. Negev Technologies And Applications Ltd. | Lead-free phosphate glasses |
JP5041323B2 (ja) | 2005-05-09 | 2012-10-03 | 日本電気硝子株式会社 | 粉末材料及びペースト材料 |
JP5011481B2 (ja) | 2006-01-06 | 2012-08-29 | 株式会社日立製作所 | 接合用ガラスおよびこの接合用ガラスを用いた平板型ディスプレイ装置 |
US8022000B2 (en) | 2006-01-06 | 2011-09-20 | Hitachi Displays Ltd. | Display device and production method thereof |
JP4837471B2 (ja) | 2006-02-20 | 2011-12-14 | 三星モバイルディスプレイ株式會社 | 有機電界発光表示装置及びその製造方法 |
JPWO2007129629A1 (ja) | 2006-05-02 | 2009-09-17 | 日本板硝子株式会社 | ガラス組成物およびこれを用いたガラススペーサ |
JP4800850B2 (ja) | 2006-06-02 | 2011-10-26 | 株式会社日立製作所 | 導電部材とその製造方法、画像表示装置及びガラススペーサ |
JP5083706B2 (ja) | 2006-11-21 | 2012-11-28 | 日本電気硝子株式会社 | ビスマス系ガラス組成物およびビスマス系封着材料 |
DE102007025465B3 (de) | 2007-05-30 | 2008-09-25 | Schott Ag | Niedrig aufschmelzendes bleifreies Lotglas und dessen Verwendung |
KR101457362B1 (ko) * | 2007-09-10 | 2014-11-03 | 주식회사 동진쎄미켐 | 유리 프릿 및 이를 이용한 전기소자의 밀봉방법 |
CN101816045A (zh) | 2007-10-18 | 2010-08-25 | E.I.内穆尔杜邦公司 | 无铅导电组合物以及用于制造半导体装置的方法:含镁添加剂 |
KR101464321B1 (ko) | 2007-11-26 | 2014-11-24 | 주식회사 동진쎄미켐 | 저융점 프릿 페이스트 조성물 및 이를 이용한 전기소자의밀봉방법 |
US8500933B2 (en) | 2007-12-14 | 2013-08-06 | Guardian Industries Corp. | Localized heating of edge seals for a vacuum insulating glass unit, and/or unitized oven for accomplishing the same |
US8506738B2 (en) | 2007-12-17 | 2013-08-13 | Guardian Industries Corp. | Localized heating via an infrared heat source array of edge seals for a vacuum insulating glass unit, and/or unitized oven with infrared heat source array for accomplishing the same |
US7736546B2 (en) | 2008-01-30 | 2010-06-15 | Basf Se | Glass frits |
JP5190672B2 (ja) * | 2008-03-17 | 2013-04-24 | 日本電気硝子株式会社 | バナジウム系ガラス組成物およびバナジウム系材料 |
JP5574518B2 (ja) | 2008-03-17 | 2014-08-20 | 日本電気硝子株式会社 | 封着材料 |
US7992411B2 (en) | 2008-05-30 | 2011-08-09 | Corning Incorporated | Method for sintering a frit to a glass plate |
JP5354444B2 (ja) | 2008-06-17 | 2013-11-27 | 日本電気硝子株式会社 | 封着材料 |
KR20100004572A (ko) | 2008-07-04 | 2010-01-13 | 주식회사 에프피 | 평판 패널의 진공 봉착용 글라스 프릿과 평판 패널의 진공 봉착용 글라스 프릿 페이스트 조성물 |
KR101520316B1 (ko) | 2008-08-06 | 2015-05-14 | 니폰 덴키 가라스 가부시키가이샤 | 밀봉 유리 |
JP5085490B2 (ja) | 2008-09-29 | 2012-11-28 | 株式会社東芝 | 映像記録再生装置および映像記録再生方法 |
EP2187444A1 (en) | 2008-11-13 | 2010-05-19 | Gigastorage Corporation | Electroconductive paste composition, electrode and solar cell device comprising same |
JP5414409B2 (ja) | 2009-01-16 | 2014-02-12 | 日立粉末冶金株式会社 | 低融点ガラス組成物、それを用いた低温封着材料及び電子部品 |
US8227055B2 (en) | 2009-05-01 | 2012-07-24 | Guardian Industries Corp. | Vacuum insulating glass unit including infrared meltable glass frit, and/or method of making the same |
US8668798B2 (en) | 2009-06-30 | 2014-03-11 | Guardian Industries Corp. | Non-toxic water-based frit slurry paste, and assembly incorporating the same |
JP5476850B2 (ja) | 2009-08-14 | 2014-04-23 | 日本電気硝子株式会社 | タブレットおよびタブレット一体型排気管 |
JP2011084437A (ja) * | 2009-10-16 | 2011-04-28 | Nippon Electric Glass Co Ltd | 封着材料 |
US20110130264A1 (en) | 2009-11-30 | 2011-06-02 | George Halsey Beall | Negative-cte glass-ceramics free of microcracks |
WO2011108115A1 (ja) * | 2010-03-05 | 2011-09-09 | ヤマト電子株式会社 | 有機el封着用無鉛ガラス材とこれを用いた有機elディスプレイ及び該ディスプレイの製造方法 |
US9359247B2 (en) | 2011-02-22 | 2016-06-07 | Guardian Industries Corp. | Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same |
US9458052B2 (en) | 2011-02-22 | 2016-10-04 | Guardian Industries Corp. | Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same |
US8802203B2 (en) | 2011-02-22 | 2014-08-12 | Guardian Industries Corp. | Vanadium-based frit materials, and/or methods of making the same |
US8733128B2 (en) | 2011-02-22 | 2014-05-27 | Guardian Industries Corp. | Materials and/or method of making vacuum insulating glass units including the same |
US9290408B2 (en) * | 2011-02-22 | 2016-03-22 | Guardian Industries Corp. | Vanadium-based frit materials, and/or methods of making the same |
US9309146B2 (en) * | 2011-02-22 | 2016-04-12 | Guardian Industries Corp. | Vanadium-based frit materials, binders, and/or solvents and methods of making the same |
US9677323B2 (en) | 2011-05-31 | 2017-06-13 | Guardian Industries Corp. | Static plasma grid evacuation techniques for vacuum insulating glass (VIG) units |
US20130074445A1 (en) | 2011-09-28 | 2013-03-28 | Guardian Industries Corp. | Vacuum insulating glass (vig) unit pump-out tube protecting techniques, and/or vig units incorporating the same |
US8794033B2 (en) | 2011-12-15 | 2014-08-05 | Guardian Industries Corp. | Apparatuses for vacuum insulating glass (VIG) unit tip-off, and/or associated methods |
US8742287B2 (en) | 2011-12-15 | 2014-06-03 | Guardian Industries Corp. | Lighting solution for apparatuses for vacuum insulating glass (VIG) unit tip-off, and/or associated methods |
US9169155B2 (en) | 2012-05-03 | 2015-10-27 | Guardian Industries Corp. | Method and apparatus for making vacuum insulated glass (VIG) window unit including cleaning cavity thereof |
US9695628B2 (en) | 2012-05-08 | 2017-07-04 | Guardian Industries Corp. | Vacuum insulated glass (VIG) window unit including pump-out tube protection ring and/or cap and methods for making same |
US8833105B2 (en) | 2012-05-18 | 2014-09-16 | Guardian Industries Corp. | Method and apparatus for making vacuum insulated glass (VIG) window unit including pump-out tube sealing technique |
US10829984B2 (en) | 2012-05-18 | 2020-11-10 | Guardian Glass, LLC | Method and apparatus for making vacuum insulated glass (VIG) window unit including pump-out tube |
US9371683B2 (en) | 2012-05-18 | 2016-06-21 | Guardian Industries Corp. | Method and apparatus for making vacuum insulated glass (VIG) window unit including pump-out tube |
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PL2797847T3 (pl) | 2018-10-31 |
CN104520246B (zh) | 2017-12-19 |
US9309146B2 (en) | 2016-04-12 |
JP2015504840A (ja) | 2015-02-16 |
CN107827364B (zh) | 2021-06-15 |
US10107028B2 (en) | 2018-10-23 |
CN107827364A (zh) | 2018-03-23 |
KR102066456B1 (ko) | 2020-01-15 |
CN104520246A (zh) | 2015-04-15 |
TR201810797T4 (tr) | 2018-08-27 |
WO2013101748A1 (en) | 2013-07-04 |
KR20140116454A (ko) | 2014-10-02 |
US20160215557A1 (en) | 2016-07-28 |
DK2797847T3 (en) | 2018-06-18 |
EP2797847B1 (en) | 2018-05-02 |
EP2797847A1 (en) | 2014-11-05 |
ES2675109T3 (es) | 2018-07-06 |
US20190032394A1 (en) | 2019-01-31 |
US10858880B2 (en) | 2020-12-08 |
US20120213953A1 (en) | 2012-08-23 |
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