JP6259617B2 - 固体電解質の製造方法 - Google Patents

固体電解質の製造方法 Download PDF

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Publication number
JP6259617B2
JP6259617B2 JP2013191083A JP2013191083A JP6259617B2 JP 6259617 B2 JP6259617 B2 JP 6259617B2 JP 2013191083 A JP2013191083 A JP 2013191083A JP 2013191083 A JP2013191083 A JP 2013191083A JP 6259617 B2 JP6259617 B2 JP 6259617B2
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Japan
Prior art keywords
solid electrolyte
sulfide
solvent
manufacturing
electrolyte according
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JP2013191083A
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English (en)
Japanese (ja)
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JP2014225425A5 (enExample
JP2014225425A (ja
Inventor
美勝 清野
美勝 清野
孝宜 菅原
孝宜 菅原
千賀　実
実 千賀
亮 油谷
亮 油谷
直憲 順毛
直憲 順毛
正克 木村
正克 木村
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Idemitsu Kosan Co Ltd
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Idemitsu Kosan Co Ltd
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Priority to JP2013191083A priority Critical patent/JP6259617B2/ja
Priority to US14/786,808 priority patent/US9793574B2/en
Priority to PCT/JP2014/002238 priority patent/WO2014174829A1/ja
Publication of JP2014225425A publication Critical patent/JP2014225425A/ja
Publication of JP2014225425A5 publication Critical patent/JP2014225425A5/ja
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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0561—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of inorganic materials only
    • H01M10/0562—Solid materials
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/22—Alkali metal sulfides or polysulfides
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
    • H01B1/06—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances
    • H01B1/10—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances sulfides
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/14—Pore volume
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2220/00—Batteries for particular applications
    • H01M2220/20—Batteries in motive systems, e.g. vehicle, ship, plane
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2220/00—Batteries for particular applications
    • H01M2220/30—Batteries in portable systems, e.g. mobile phone, laptop
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2300/00—Electrolytes
    • H01M2300/0017—Non-aqueous electrolytes
    • H01M2300/0065—Solid electrolytes
    • H01M2300/0068—Solid electrolytes inorganic
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Manufacturing & Machinery (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Materials Engineering (AREA)
  • Secondary Cells (AREA)
  • Conductive Materials (AREA)
  • Glass Compositions (AREA)
JP2013191083A 2013-04-24 2013-09-13 固体電解質の製造方法 Active JP6259617B2 (ja)

Priority Applications (3)

Application Number Priority Date Filing Date Title
JP2013191083A JP6259617B2 (ja) 2013-04-24 2013-09-13 固体電解質の製造方法
US14/786,808 US9793574B2 (en) 2013-04-24 2014-04-21 Method for producing solid electrolyte
PCT/JP2014/002238 WO2014174829A1 (ja) 2013-04-24 2014-04-21 固体電解質の製造方法

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2013091032 2013-04-24
JP2013091032 2013-04-24
JP2013191083A JP6259617B2 (ja) 2013-04-24 2013-09-13 固体電解質の製造方法

Publications (3)

Publication Number Publication Date
JP2014225425A JP2014225425A (ja) 2014-12-04
JP2014225425A5 JP2014225425A5 (enExample) 2016-10-27
JP6259617B2 true JP6259617B2 (ja) 2018-01-10

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US (1) US9793574B2 (enExample)
JP (1) JP6259617B2 (enExample)
WO (1) WO2014174829A1 (enExample)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2021163758A (ja) * 2020-03-31 2021-10-11 出光興産株式会社 固体電解質の製造方法
US11799126B2 (en) 2019-05-31 2023-10-24 Samsung Electronics Co., Ltd. Method of preparing solid electrolyte and all-solid battery including solid electrolyte prepared by the method

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JP6425426B2 (ja) * 2014-06-10 2018-11-21 三星電子株式会社Ｓａｍｓｕｎｇ Ｅｌｅｃｔｒｏｎｉｃｓ Ｃｏ．，Ｌｔｄ． 硫化物固体電解質、および硫化物固体電解質の製造方法
US20150093652A1 (en) * 2013-10-02 2015-04-02 Samsung Electronics Co., Ltd. Sulfide solid electrolyte, method of preparing the same, and solid state battery including the same
JP6761928B2 (ja) * 2014-12-05 2020-09-30 国立大学法人豊橋技術科学大学 固体電解質ガラス及びその製造方法、固体電解質ガラス用前駆体、サスペンジョン、リチウムイオン電池用電極並びにリチウムイオン電池
JP6320983B2 (ja) * 2015-12-01 2018-05-09 出光興産株式会社 硫化物ガラスセラミックスの製造方法
EP3432320B1 (en) * 2016-03-14 2023-05-31 Idemitsu Kosan Co.,Ltd. Solid electrolyte and method for producing solid electrolyte
KR20180055086A (ko) * 2016-11-16 2018-05-25 현대자동차주식회사 습식공정을 통한 황화물계 고체전해질의 제조방법
KR102417506B1 (ko) * 2016-11-16 2022-07-05 현대자동차주식회사 단일원소로부터 유래된 고체전해질 및 이의 제조방법
WO2018110647A1 (ja) * 2016-12-14 2018-06-21 出光興産株式会社 硫化物固体電解質の製造方法
JP6763808B2 (ja) * 2017-03-14 2020-09-30 出光興産株式会社 固体電解質の製造方法
KR102359583B1 (ko) * 2017-05-08 2022-02-07 현대자동차주식회사 고체전해질 및 이를 포함하는 전고체 전지의 제조방법
WO2019098009A1 (ja) * 2017-11-17 2019-05-23 富士フイルム株式会社 固体電解質組成物、全固体二次電池用シート、全固体二次電池用電極シート及び全固体二次電池、並びに、全固体二次電池用シート及び全固体二次電池の製造方法
JP6819559B2 (ja) * 2017-12-08 2021-01-27 トヨタ自動車株式会社 硫化物固体電解質材料の製造方法
KR102552153B1 (ko) * 2018-04-18 2023-07-05 현대자동차주식회사 전고체 전지용 황화물계 고체 전해질의 제조 방법
JP7032230B2 (ja) * 2018-05-14 2022-03-08 三星電子株式会社 硫化物系固体電解質の製造方法および全固体型二次電池の製造方法
JP7077766B2 (ja) * 2018-05-18 2022-05-31 トヨタ自動車株式会社 硫化物系固体電解質、当該硫化物系固体電解質の製造方法、及び、全固体電池の製造方法
JP7107087B2 (ja) * 2018-08-16 2022-07-27 三菱瓦斯化学株式会社 Ｌｇｐｓ系固体電解質の製造方法
KR102673003B1 (ko) * 2018-11-30 2024-06-05 현대자동차주식회사 용해석출법에 의한 고이온전도성 황화물계 고체전해질의 제조방법 및 이에 사용되는 황화물계 고체전해질 제조용 조성물
JP7107272B2 (ja) * 2019-04-11 2022-07-27 トヨタ自動車株式会社 硫化物固体電解質、硫化物固体電解質の製造方法、電極体および全固体電池
JP7324849B2 (ja) * 2019-08-09 2023-08-10 出光興産株式会社 電極合材及びその製造方法
CN110563013A (zh) * 2019-08-26 2019-12-13 浙江工业大学 一种硫化铝的球磨合成方法
US11702337B2 (en) 2019-09-27 2023-07-18 Samsung Sdi Co., Ltd. Solid ion conductor, solid electrolyte including the solid ion conductor, electrochemical cell including the solid ion conductor, and preparation method of the same
US12119441B2 (en) 2019-11-01 2024-10-15 Samsung Sdi Co., Ltd. Solid ion conductor compound, solid electrolyte including solid ion conductor compound, electrochemical cell including solid ion conductor compound, and method of preparing solid ion conductor compound
KR20230008725A (ko) * 2020-05-13 2023-01-16 이데미쓰 고산 가부시키가이샤 고체 전해질의 제조 방법
EP4152463A4 (en) * 2020-05-13 2024-06-19 Idemitsu Kosan Co., Ltd Solid electrolyte production method
JP7584354B2 (ja) * 2020-05-27 2024-11-15 出光興産株式会社 固体電解質の製造方法
JPWO2021261361A1 (enExample) * 2020-06-23 2021-12-30
WO2022186155A1 (ja) * 2021-03-05 2022-09-09 三井金属鉱業株式会社 固体電解質並びにそれを含む電極合剤及び電池
EP4303183A4 (en) * 2021-03-05 2024-10-02 Mitsui Mining & Smelting Co., Ltd. METHOD FOR PRODUCING A SULFIDE SOLID ELECTROLYTE
KR20240032052A (ko) 2021-07-07 2024-03-08 스페셜티 오퍼레이션스 프랑스 황화리튬 분말을 수득하는 방법, 및 lps 화합물을 제조하기 위한 이의 용도
JP2024047093A (ja) * 2022-09-26 2024-04-05 トヨタ自動車株式会社 全固体電池

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JP3528866B2 (ja) 1994-06-03 2004-05-24 出光石油化学株式会社 硫化リチウムの製造方法
JP3510420B2 (ja) 1996-04-16 2004-03-29 松下電器産業株式会社 リチウムイオン伝導性固体電解質およびその製造方法
WO2004093099A1 (ja) 2003-04-15 2004-10-28 Idemitsu Kosan Co., Ltd. リチウムイオン導電性固体電解質の製造方法及びそれを用いた全固体型二次電池
WO2005040039A1 (ja) 2003-10-23 2005-05-06 Idemitsu Kosan Co., Ltd. 硫化リチウムの精製方法
JP4813767B2 (ja) 2004-02-12 2011-11-09 出光興産株式会社 リチウムイオン伝導性硫化物系結晶化ガラス及びその製造方法
CN101821894B (zh) * 2007-10-11 2012-12-19 出光兴产株式会社 锂离子传导性固体电解质的制造方法
JP5460283B2 (ja) 2008-12-15 2014-04-02 出光興産株式会社 硫化リチウムの製造方法
JP5303428B2 (ja) 2009-10-16 2013-10-02 出光興産株式会社 硫化リチウム及びその製造方法
JP5629198B2 (ja) * 2009-12-04 2014-11-19 出光興産株式会社 アルカリ金属硫化物及びその製造方法
JP5349427B2 (ja) * 2010-08-26 2013-11-20 トヨタ自動車株式会社 硫化物固体電解質材料、正極体およびリチウム固体電池
JP5445527B2 (ja) * 2011-07-13 2014-03-19 トヨタ自動車株式会社 硫化物固体電解質材料の製造方法

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11799126B2 (en) 2019-05-31 2023-10-24 Samsung Electronics Co., Ltd. Method of preparing solid electrolyte and all-solid battery including solid electrolyte prepared by the method
JP2021163758A (ja) * 2020-03-31 2021-10-11 出光興産株式会社 固体電解質の製造方法
JP7575981B2 (ja) 2020-03-31 2024-10-30 出光興産株式会社 固体電解質の製造方法

Also Published As

Publication number Publication date
WO2014174829A1 (ja) 2014-10-30
US20160104916A1 (en) 2016-04-14
JP2014225425A (ja) 2014-12-04
US9793574B2 (en) 2017-10-17

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