JP6130503B2 - 3D成形のためのイオン交換可能なLi含有ガラス組成物 - Google Patents
3D成形のためのイオン交換可能なLi含有ガラス組成物 Download PDFInfo
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- JP6130503B2 JP6130503B2 JP2015523150A JP2015523150A JP6130503B2 JP 6130503 B2 JP6130503 B2 JP 6130503B2 JP 2015523150 A JP2015523150 A JP 2015523150A JP 2015523150 A JP2015523150 A JP 2015523150A JP 6130503 B2 JP6130503 B2 JP 6130503B2
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- 239000011521 glass Substances 0.000 title claims description 446
- 239000000203 mixture Substances 0.000 title description 374
- 238000000465 moulding Methods 0.000 title description 18
- 229910052796 boron Inorganic materials 0.000 claims description 78
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 77
- 229910018068 Li 2 O Inorganic materials 0.000 claims description 77
- 238000005342 ion exchange Methods 0.000 claims description 48
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 43
- 229910052708 sodium Inorganic materials 0.000 claims description 27
- 150000003839 salts Chemical class 0.000 claims description 18
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 16
- 239000011734 sodium Substances 0.000 description 65
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 63
- 238000000034 method Methods 0.000 description 20
- 230000000052 comparative effect Effects 0.000 description 15
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 14
- 230000008569 process Effects 0.000 description 13
- 239000003513 alkali Substances 0.000 description 11
- 230000004927 fusion Effects 0.000 description 10
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 8
- 150000002500 ions Chemical class 0.000 description 8
- 229910000272 alkali metal oxide Inorganic materials 0.000 description 7
- 238000007665 sagging Methods 0.000 description 7
- 238000012937 correction Methods 0.000 description 5
- 239000006059 cover glass Substances 0.000 description 5
- 239000006025 fining agent Substances 0.000 description 5
- 229910052760 oxygen Inorganic materials 0.000 description 5
- 238000005728 strengthening Methods 0.000 description 5
- 229910006404 SnO 2 Inorganic materials 0.000 description 4
- 238000000137 annealing Methods 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 230000003247 decreasing effect Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 238000002844 melting Methods 0.000 description 4
- 230000008018 melting Effects 0.000 description 4
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 230000006835 compression Effects 0.000 description 3
- 238000007906 compression Methods 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 230000009477 glass transition Effects 0.000 description 3
- 238000007654 immersion Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 229910052700 potassium Inorganic materials 0.000 description 3
- 239000011591 potassium Substances 0.000 description 3
- 229910001414 potassium ion Inorganic materials 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 229910001415 sodium ion Inorganic materials 0.000 description 3
- 238000006467 substitution reaction Methods 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 239000005388 borosilicate glass Substances 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000003280 down draw process Methods 0.000 description 2
- 230000003993 interaction Effects 0.000 description 2
- 230000000670 limiting effect Effects 0.000 description 2
- 229910052744 lithium Inorganic materials 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000003607 modifier Substances 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000011253 protective coating Substances 0.000 description 2
- 230000002787 reinforcement Effects 0.000 description 2
- 238000007679 ring-on-ring test Methods 0.000 description 2
- 229910052845 zircon Inorganic materials 0.000 description 2
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 description 2
- -1 (Al) OH 3 Inorganic materials 0.000 description 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- 238000006124 Pilkington process Methods 0.000 description 1
- NPYPAHLBTDXSSS-UHFFFAOYSA-N Potassium ion Chemical compound [K+] NPYPAHLBTDXSSS-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 239000005354 aluminosilicate glass Substances 0.000 description 1
- 229910001423 beryllium ion Inorganic materials 0.000 description 1
- 229910052810 boron oxide Inorganic materials 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000004031 devitrification Methods 0.000 description 1
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 238000003286 fusion draw glass process Methods 0.000 description 1
- 238000007496 glass forming Methods 0.000 description 1
- 239000000156 glass melt Substances 0.000 description 1
- 239000005400 gorilla glass Substances 0.000 description 1
- 238000003475 lamination Methods 0.000 description 1
- 230000031700 light absorption Effects 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 230000036961 partial effect Effects 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 230000002829 reductive effect Effects 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 238000002798 spectrophotometry method Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 238000007655 standard test method Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/097—Glass compositions containing silica with 40% to 90% silica, by weight containing phosphorus, niobium or tantalum
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/083—Glass compositions containing silica with 40% to 90% silica, by weight containing aluminium oxide or an iron compound
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C21/00—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface
- C03C21/001—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface in liquid phase, e.g. molten salts, solutions
- C03C21/002—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface in liquid phase, e.g. molten salts, solutions to perform ion-exchange between alkali ions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/083—Glass compositions containing silica with 40% to 90% silica, by weight containing aluminium oxide or an iron compound
- C03C3/085—Glass compositions containing silica with 40% to 90% silica, by weight containing aluminium oxide or an iron compound containing an oxide of a divalent metal
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/083—Glass compositions containing silica with 40% to 90% silica, by weight containing aluminium oxide or an iron compound
- C03C3/085—Glass compositions containing silica with 40% to 90% silica, by weight containing aluminium oxide or an iron compound containing an oxide of a divalent metal
- C03C3/087—Glass compositions containing silica with 40% to 90% silica, by weight containing aluminium oxide or an iron compound containing an oxide of a divalent metal containing calcium oxide, e.g. common sheet or container glass
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/089—Glass compositions containing silica with 40% to 90% silica, by weight containing boron
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/089—Glass compositions containing silica with 40% to 90% silica, by weight containing boron
- C03C3/091—Glass compositions containing silica with 40% to 90% silica, by weight containing boron containing aluminium
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/089—Glass compositions containing silica with 40% to 90% silica, by weight containing boron
- C03C3/091—Glass compositions containing silica with 40% to 90% silica, by weight containing boron containing aluminium
- C03C3/093—Glass compositions containing silica with 40% to 90% silica, by weight containing boron containing aluminium containing zinc or zirconium
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C4/00—Compositions for glass with special properties
- C03C4/18—Compositions for glass with special properties for ion-sensitive glass
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31—Surface property or characteristic of web, sheet or block
- Y10T428/315—Surface modified glass [e.g., tempered, strengthened, etc.]
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Glass Compositions (AREA)
- Surface Treatment Of Glass (AREA)
Description
Claims (3)
- 65モル%から71モル%のSiO2、
7モル%から12モル%のAl2O3、
1モル%から3.5モル%のLi2O、
6モル%から16モル%のNa2O、
0モル%から5モル%のK2O、
0.8から10モル%の二価酸化物であって、MgOおよびZnOの少なくとも一方を含む二価酸化物、および
0モル%から0.5モル%未満のB2O3
を含み、
前記Al2O3の濃度(モル%)および前記二価酸化物の濃度(モル%)の合計が10モル%超であり、
810℃以下の軟化点;
27×10-6/℃以下の高温CTE;および
15時間以下に亘る390℃から450℃の温度範囲でのKNO3を含む塩浴中におけるイオン交換後の、600MPa以上の圧縮応力および25μm以上の層の深さ、
を有するガラス物品。 - 55モル%から68モル%のSiO2、
9モル%から15モル%のAl2O3、
4.5モル%から12モル%のB2O3、
1モル%から7モル%のLi2O、
3モル%から12モル%のNa2O、および
0モル%から3モル%のK2O、
を含み、
R2Oは、Li2Oの濃度、Na2Oの濃度、およびK2Oの濃度の合計であり、Al2O3の濃度に対するR2Oの比が、1.15以下であり、
810℃以下の軟化点;
27×10-6/℃以下の高温CTE;および
15時間以下に亘る390℃から450℃の温度範囲でのKNO3を含む塩浴中におけるイオン交換後の、600MPa以上の圧縮応力および25μm以上の層の深さ、
を有するガラス物品であって、
Lが0から5.0であり、a*が−2.0から2.0であり、b*が0から−5.0である、L、a*、b*色座標を有する、
ガラス物品。 - Al2O3の濃度に対するR2Oの比が1.02以上であり、前記ガラス物品がTiO2およびFe2O3をさらに含み、TiO2(モル%)に対するFe2O3(モル%)の比が、0.52以上かつ1.22以下である、請求項2記載のガラス物品。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201261672346P | 2012-07-17 | 2012-07-17 | |
US61/672,346 | 2012-07-17 | ||
PCT/US2013/050442 WO2014014798A1 (en) | 2012-07-17 | 2013-07-15 | Ion exchangeable li-containing glass compositions for 3-d forming |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2017079571A Division JP6491688B2 (ja) | 2012-07-17 | 2017-04-13 | 3D成形のためのイオン交換可能なLi含有ガラス組成物 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2015527970A JP2015527970A (ja) | 2015-09-24 |
JP6130503B2 true JP6130503B2 (ja) | 2017-05-17 |
Family
ID=48808561
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2015523150A Active JP6130503B2 (ja) | 2012-07-17 | 2013-07-15 | 3D成形のためのイオン交換可能なLi含有ガラス組成物 |
JP2017079571A Active JP6491688B2 (ja) | 2012-07-17 | 2017-04-13 | 3D成形のためのイオン交換可能なLi含有ガラス組成物 |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2017079571A Active JP6491688B2 (ja) | 2012-07-17 | 2017-04-13 | 3D成形のためのイオン交換可能なLi含有ガラス組成物 |
Country Status (8)
Country | Link |
---|---|
US (5) | US9139469B2 (ja) |
EP (2) | EP2874959B1 (ja) |
JP (2) | JP6130503B2 (ja) |
KR (2) | KR20190133802A (ja) |
CN (3) | CN108191229A (ja) |
DE (1) | DE202013012811U1 (ja) |
TW (1) | TWI624443B (ja) |
WO (1) | WO2014014798A1 (ja) |
Families Citing this family (84)
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US10183887B2 (en) | 2019-01-22 |
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KR20190133802A (ko) | 2019-12-03 |
JP2015527970A (ja) | 2015-09-24 |
EP2874959B1 (en) | 2022-08-17 |
CN108191229A (zh) | 2018-06-22 |
US11814316B2 (en) | 2023-11-14 |
US10150691B2 (en) | 2018-12-11 |
KR20150038177A (ko) | 2015-04-08 |
CN104703937A (zh) | 2015-06-10 |
EP2874959A1 (en) | 2015-05-27 |
US20140023865A1 (en) | 2014-01-23 |
KR102128490B1 (ko) | 2020-07-01 |
US20190092679A1 (en) | 2019-03-28 |
US20220002187A1 (en) | 2022-01-06 |
CN112851115A (zh) | 2021-05-28 |
EP3632861A1 (en) | 2020-04-08 |
US20180022638A1 (en) | 2018-01-25 |
WO2014014798A1 (en) | 2014-01-23 |
US20150344351A1 (en) | 2015-12-03 |
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JP2017149644A (ja) | 2017-08-31 |
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