JP6029898B2 - リチウム二次電池用正極の作製方法 - Google Patents
リチウム二次電池用正極の作製方法 Download PDFInfo
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- JP6029898B2 JP6029898B2 JP2012192846A JP2012192846A JP6029898B2 JP 6029898 B2 JP6029898 B2 JP 6029898B2 JP 2012192846 A JP2012192846 A JP 2012192846A JP 2012192846 A JP2012192846 A JP 2012192846A JP 6029898 B2 JP6029898 B2 JP 6029898B2
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- positive electrode
- lithium
- secondary battery
- graphene oxide
- lithium secondary
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/30—Alkali metal phosphates
- C01B25/305—Preparation from phosphorus-containing compounds by alkaline treatment
- C01B25/306—Preparation from phosphorus-containing compounds by alkaline treatment from phosphates
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/362—Composites
- H01M4/366—Composites as layered products
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- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/362—Composites
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/45—Phosphates containing plural metal, or metal and ammonium
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/20—Graphite
- C01B32/21—After-treatment
- C01B32/23—Oxidation
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- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
- C30B29/14—Phosphates
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- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
- C30B7/10—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
- H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
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- H01M4/00—Electrodes
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- H01M4/04—Processes of manufacture in general
- H01M4/0402—Methods of deposition of the material
- H01M4/0404—Methods of deposition of the material by coating on electrode collectors
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
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- H01M4/0435—Rolling or calendering
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- H—ELECTRICITY
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- H01M4/04—Processes of manufacture in general
- H01M4/0471—Processes of manufacture in general involving thermal treatment, e.g. firing, sintering, backing particulate active material, thermal decomposition, pyrolysis
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- H01M4/1397—Processes of manufacture of electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
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- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
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- H—ELECTRICITY
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- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/583—Carbonaceous material, e.g. graphite-intercalation compounds or CFx
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- H01—ELECTRIC ELEMENTS
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- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/583—Carbonaceous material, e.g. graphite-intercalation compounds or CFx
- H01M4/587—Carbonaceous material, e.g. graphite-intercalation compounds or CFx for inserting or intercalating light metals
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
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- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
- H01M2004/028—Positive electrodes
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Composite Materials (AREA)
- Metallurgy (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
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- Battery Electrode And Active Subsutance (AREA)
- Secondary Cells (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2012192846A JP6029898B2 (ja) | 2011-09-09 | 2012-09-03 | リチウム二次電池用正極の作製方法 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2011197021 | 2011-09-09 | ||
| JP2011197021 | 2011-09-09 | ||
| JP2012192846A JP6029898B2 (ja) | 2011-09-09 | 2012-09-03 | リチウム二次電池用正極の作製方法 |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2016205017A Division JP2017010947A (ja) | 2011-09-09 | 2016-10-19 | リチウム二次電池用正極 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2013069677A JP2013069677A (ja) | 2013-04-18 |
| JP2013069677A5 JP2013069677A5 (OSRAM) | 2015-10-15 |
| JP6029898B2 true JP6029898B2 (ja) | 2016-11-24 |
Family
ID=47830113
Family Applications (5)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012192846A Expired - Fee Related JP6029898B2 (ja) | 2011-09-09 | 2012-09-03 | リチウム二次電池用正極の作製方法 |
| JP2016205017A Withdrawn JP2017010947A (ja) | 2011-09-09 | 2016-10-19 | リチウム二次電池用正極 |
| JP2018146492A Withdrawn JP2018166129A (ja) | 2011-09-09 | 2018-08-03 | リチウム二次電池用正極の作製方法 |
| JP2020212466A Withdrawn JP2021044269A (ja) | 2011-09-09 | 2020-12-22 | 表示装置 |
| JP2022208036A Active JP7748932B2 (ja) | 2011-09-09 | 2022-12-26 | リチウム二次電池用正極及びリチウム二次電池 |
Family Applications After (4)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2016205017A Withdrawn JP2017010947A (ja) | 2011-09-09 | 2016-10-19 | リチウム二次電池用正極 |
| JP2018146492A Withdrawn JP2018166129A (ja) | 2011-09-09 | 2018-08-03 | リチウム二次電池用正極の作製方法 |
| JP2020212466A Withdrawn JP2021044269A (ja) | 2011-09-09 | 2020-12-22 | 表示装置 |
| JP2022208036A Active JP7748932B2 (ja) | 2011-09-09 | 2022-12-26 | リチウム二次電池用正極及びリチウム二次電池 |
Country Status (4)
| Country | Link |
|---|---|
| US (3) | US9252419B2 (OSRAM) |
| JP (5) | JP6029898B2 (OSRAM) |
| CN (2) | CN103000862B (OSRAM) |
| TW (3) | TWI583042B (OSRAM) |
Families Citing this family (58)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6029898B2 (ja) * | 2011-09-09 | 2016-11-24 | 株式会社半導体エネルギー研究所 | リチウム二次電池用正極の作製方法 |
| KR101561377B1 (ko) | 2013-01-10 | 2015-10-20 | 주식회사 엘지화학 | 리튬 인산철 나노분말 제조방법 |
| KR101561373B1 (ko) | 2013-01-10 | 2015-10-19 | 주식회사 엘지화학 | 리튬 인산철 나노분말 제조방법 |
| KR101561378B1 (ko) | 2013-01-10 | 2015-10-20 | 주식회사 엘지화학 | 탄소 코팅 리튬 인산철 나노분말 제조방법 |
| GB2516932B (en) * | 2013-08-07 | 2018-12-26 | Nokia Technologies Oy | An apparatus and associated methods for water detection |
| JP2016013958A (ja) | 2013-12-02 | 2016-01-28 | 株式会社半導体エネルギー研究所 | 素子、膜の作製方法 |
| KR102306495B1 (ko) * | 2013-12-04 | 2021-09-28 | 가부시키가이샤 한도오따이 에네루기 켄큐쇼 | 축전체 및 전자 기기 |
| CN104752693A (zh) * | 2013-12-30 | 2015-07-01 | 北京有色金属研究总院 | 锂离子电池正极材料磷酸铁锂/石墨烯复合物的制备方法 |
| KR102573541B1 (ko) | 2014-08-27 | 2023-09-01 | 가부시키가이샤 한도오따이 에네루기 켄큐쇼 | 축전지의 전극, 그 제조 방법, 축전지, 전자 장치, 및 그래핀 |
| JP6666107B2 (ja) | 2014-10-24 | 2020-03-13 | 株式会社半導体エネルギー研究所 | 蓄電池用電極の製造方法、及び蓄電池用電極 |
| JP2016143553A (ja) * | 2015-02-02 | 2016-08-08 | Jsr株式会社 | 蓄電デバイス電極用スラリー、蓄電デバイス電極及び蓄電デバイス |
| WO2016160703A1 (en) | 2015-03-27 | 2016-10-06 | Harrup Mason K | All-inorganic solvents for electrolytes |
| CN104852046B (zh) * | 2015-04-08 | 2017-01-18 | 浙江大学 | 纳米片状磷酸锰铁锂材料及其制备方法和应用 |
| WO2016178117A1 (en) | 2015-05-06 | 2016-11-10 | Semiconductor Energy Laboratory Co., Ltd. | Secondary battery and electronic device |
| JP2016222526A (ja) | 2015-05-29 | 2016-12-28 | 株式会社半導体エネルギー研究所 | 膜の作製方法および素子 |
| JP6269597B2 (ja) * | 2015-06-29 | 2018-01-31 | トヨタ自動車株式会社 | 正極活物質層、全固体リチウム電池および正極活物質層の製造方法 |
| US10686207B2 (en) * | 2015-07-03 | 2020-06-16 | Semiconductor Energy Laboratory Co., Ltd. | Lithium-ion storage battery and electronic device |
| JP2017045726A (ja) | 2015-08-27 | 2017-03-02 | 株式会社半導体エネルギー研究所 | 電極、及びその製造方法、蓄電池、並びに電子機器 |
| CN105575678A (zh) * | 2015-12-17 | 2016-05-11 | 中国电子科技集团公司第十八研究所 | 一种锂离子电容器用电极膜的制备方法 |
| DE102016203240A1 (de) * | 2016-02-29 | 2017-08-31 | Robert Bosch Gmbh | Verfahren zur Herstellung einer Elektrode, Elektrode und Batteriezelle |
| CN109075320B (zh) | 2016-04-25 | 2021-11-05 | 日本碍子株式会社 | 正极 |
| EP3352256B1 (en) | 2016-04-25 | 2020-01-01 | NGK Insulators, Ltd. | Positive electrode |
| US10680242B2 (en) * | 2016-05-18 | 2020-06-09 | Semiconductor Energy Laboratory Co., Ltd. | Method for manufacturing positive electrode active material, and lithium ion battery |
| CN105977465A (zh) * | 2016-06-29 | 2016-09-28 | 上海应用技术学院 | 一种石墨烯/磷酸铁锂复合正极材料的制备方法 |
| DE202017007594U1 (de) | 2016-07-05 | 2023-09-11 | Semiconductor Energy Laboratory Co., Ltd. | Positivelektrodenaktivmaterial und Sekundärbatterie |
| US20180013151A1 (en) * | 2016-07-08 | 2018-01-11 | Semiconductor Energy Laboratory Co., Ltd. | Positive electrode active material, power storage device, electronic device, and method for manufacturing positive electrode active material |
| US12308421B2 (en) | 2016-09-12 | 2025-05-20 | Semiconductor Energy Laboratory Co., Ltd. | Electrode and power storage device comprising graphene compound |
| US10707531B1 (en) | 2016-09-27 | 2020-07-07 | New Dominion Enterprises Inc. | All-inorganic solvents for electrolytes |
| KR102697171B1 (ko) | 2016-10-12 | 2024-08-22 | 가부시키가이샤 한도오따이 에네루기 켄큐쇼 | 양극 활물질 입자 및 양극 활물질 입자의 제작 방법 |
| CN106711426B (zh) * | 2017-01-22 | 2018-05-15 | 深圳市沃特玛电池有限公司 | 一种磷酸铁锂正极材料的制备方法 |
| CN112259720A (zh) | 2017-05-12 | 2021-01-22 | 株式会社半导体能源研究所 | 正极活性物质粒子 |
| CN117038957A (zh) | 2017-05-19 | 2023-11-10 | 株式会社半导体能源研究所 | 锂离子二次电池 |
| KR20250086799A (ko) | 2017-06-26 | 2025-06-13 | 가부시키가이샤 한도오따이 에네루기 켄큐쇼 | 양극 활물질의 제작 방법 및 이차 전지 |
| US10601033B2 (en) | 2017-09-29 | 2020-03-24 | International Business Machines Corporation | High-performance rechargeable batteries having a spalled and textured cathode layer |
| US10622636B2 (en) * | 2017-09-29 | 2020-04-14 | International Business Machines Corporation | High-capacity rechargeable battery stacks containing a spalled cathode material |
| CN109935781B (zh) * | 2017-12-19 | 2023-11-28 | 成都大超科技有限公司 | 正极结构及其制备方法、锂电池 |
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| TW201324936A (zh) | 2013-06-16 |
| JP2021044269A (ja) | 2021-03-18 |
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