JP4931596B2 - タバコ組成物 - Google Patents
タバコ組成物 Download PDFInfo
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- JP4931596B2 JP4931596B2 JP2006539648A JP2006539648A JP4931596B2 JP 4931596 B2 JP4931596 B2 JP 4931596B2 JP 2006539648 A JP2006539648 A JP 2006539648A JP 2006539648 A JP2006539648 A JP 2006539648A JP 4931596 B2 JP4931596 B2 JP 4931596B2
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- tobacco
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- flavor
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- 239000008121 dextrose Substances 0.000 description 1
- 238000007907 direct compression Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000007884 disintegrant Substances 0.000 description 1
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 description 1
- PYLIXCKOHOHGKQ-UHFFFAOYSA-L disodium;hydrogen phosphate;heptahydrate Chemical compound O.O.O.O.O.O.O.[Na+].[Na+].OP([O-])([O-])=O PYLIXCKOHOHGKQ-UHFFFAOYSA-L 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
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- 230000005593 dissociations Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
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- 229920001971 elastomer Polymers 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
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- 238000005538 encapsulation Methods 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 210000000416 exudates and transudate Anatomy 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000005243 fluidization Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000007903 gelatin capsule Substances 0.000 description 1
- 235000010492 gellan gum Nutrition 0.000 description 1
- 239000000216 gellan gum Substances 0.000 description 1
- 235000021312 gluten Nutrition 0.000 description 1
- 235000010417 guar gum Nutrition 0.000 description 1
- 239000000665 guar gum Substances 0.000 description 1
- 229960002154 guar gum Drugs 0.000 description 1
- 108091005708 gustatory receptors Proteins 0.000 description 1
- 239000011874 heated mixture Substances 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
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- 239000000416 hydrocolloid Substances 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000002198 insoluble material Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 229940029339 inulin Drugs 0.000 description 1
- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 description 1
- 235000010485 konjac Nutrition 0.000 description 1
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- 150000002632 lipids Chemical class 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 235000010420 locust bean gum Nutrition 0.000 description 1
- 239000000711 locust bean gum Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
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- 239000004292 methyl p-hydroxybenzoate Substances 0.000 description 1
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 description 1
- 229960002216 methylparaben Drugs 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
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- 235000019426 modified starch Nutrition 0.000 description 1
- 239000012778 molding material Substances 0.000 description 1
- 210000002200 mouth mucosa Anatomy 0.000 description 1
- 229920005615 natural polymer Polymers 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- JCXJVPUVTGWSNB-UHFFFAOYSA-N nitrogen dioxide Inorganic materials O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 description 1
- 239000004745 nonwoven fabric Substances 0.000 description 1
- 235000019645 odor Nutrition 0.000 description 1
- 238000000643 oven drying Methods 0.000 description 1
- 239000012785 packaging film Substances 0.000 description 1
- 229920006280 packaging film Polymers 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 229960000292 pectin Drugs 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 239000000244 polyoxyethylene sorbitan monooleate Substances 0.000 description 1
- 229940068968 polysorbate 80 Drugs 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 235000007686 potassium Nutrition 0.000 description 1
- 229960003975 potassium Drugs 0.000 description 1
- 229910001414 potassium ion Inorganic materials 0.000 description 1
- 239000004302 potassium sorbate Substances 0.000 description 1
- 235000010241 potassium sorbate Nutrition 0.000 description 1
- 229940069338 potassium sorbate Drugs 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 235000010409 propane-1,2-diol alginate Nutrition 0.000 description 1
- 239000000770 propane-1,2-diol alginate Substances 0.000 description 1
- 108020003175 receptors Proteins 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000004208 shellac Substances 0.000 description 1
- 229940113147 shellac Drugs 0.000 description 1
- 235000013874 shellac Nutrition 0.000 description 1
- ZLGIYFNHBLSMPS-ATJNOEHPSA-N shellac Chemical compound OCCCCCC(O)C(O)CCCCCCCC(O)=O.C1C23[C@H](C(O)=O)CCC2[C@](C)(CO)[C@@H]1C(C(O)=O)=C[C@@H]3O ZLGIYFNHBLSMPS-ATJNOEHPSA-N 0.000 description 1
- 239000001488 sodium phosphate Substances 0.000 description 1
- 229910000162 sodium phosphate Inorganic materials 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000012453 solvate Substances 0.000 description 1
- 229940001941 soy protein Drugs 0.000 description 1
- 150000003432 sterols Chemical class 0.000 description 1
- 235000003702 sterols Nutrition 0.000 description 1
- 229920001059 synthetic polymer Polymers 0.000 description 1
- 235000010491 tara gum Nutrition 0.000 description 1
- 239000000213 tara gum Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
- 239000011800 void material Substances 0.000 description 1
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- 230000037303 wrinkles Effects 0.000 description 1
- 239000005019 zein Substances 0.000 description 1
- 229940093612 zein Drugs 0.000 description 1
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical class [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B13/00—Tobacco for pipes, for cigars, e.g. cigar inserts, or for cigarettes; Chewing tobacco; Snuff
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/70—Fixation, conservation, or encapsulation of flavouring agents
- A23L27/79—Fixation, conservation, or encapsulation of flavouring agents in the form of films
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/81—Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
Landscapes
- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Pharmacology & Pharmacy (AREA)
- Alternative & Traditional Medicine (AREA)
- Microbiology (AREA)
- Medicinal Chemistry (AREA)
- Medical Informatics (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Mycology (AREA)
- Nutrition Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Formation And Processing Of Food Products (AREA)
- Medicinal Preparation (AREA)
Description
本発明はタバコ製品の分野に関する。
本発明はタバコ組成物ならびにその使用および製造の方法を特徴とする。本発明の組成物はさまざまな技術に基づくことができる。技術としては、フィルム、錠剤(tab)、成形部、ゲル、消耗単位、不溶性マトリックスおよび中空形状が挙げられる。タバコに加えて、組成物はまた、フレーバー、色および本明細書に記述されるようなその他の添加物を含んでもよい。組成物はまた、経口的に崩壊可能であってもよい。典型的な組成物およびその製造の方法が本明細書に記述される。
本発明は、典型的にはタバコ満足感のためのタバコ組成物を特徴とする。
本明細書に記述されている組成物に有用なタバコは、任意の未加工または加工形状、例えば、粉末、顆粒または断片を含む。タバコは口腔内で崩壊する(例えば、溶解する)ように一定の大きさに作られるかまたは作製されて、可溶性であるという知覚を与える(例えば、タバコが口腔内で触覚を発生させない)か、または容易に嚥下されることが好ましい。あるいは、タバコは口腔内で触覚をもたらすように一定の大きさに作られるかまたは作製されてもよい。典型的な平均サイズは1から1000 μmの範囲内、例えば、およそ800、500、250、100、80、75、50、25、20、15、10、8、6、5、3、2もしくは1 μmまたはそれ以下、好ましくは80 μmまたはそれ以下である。タバコはまた、スラリーまたは流動性を有するゲルの形状であってもよい。流動性を有するゲルは水に溶解させたフォーマットの混合物であり、これをタバコと混合し、その後、フォーマットの完全な溶解を阻止する混和性(miscible)溶媒と混合する。そのような混合によってフォーマットの膨潤を引き起こし、偽塑性であって僅かな圧力で容器(例えば、管)から容易に分配される粘性ペーストを形成させる。典型的なタバコは無煙タバコである。さらなるタバコは米国特許公開第2003/0094182号および第2003/0070687号、米国特許出願第60/603,887号、ならびに2004年11月5日付で出願された「Nicotiana Compositions」という表題の米国特許出願第______号に記述されており、これらの開示は参照により本明細書に組み入れられる。組成物に利用されるタバコはまた、米国特許公開第2004/0112394号の方法にしたがって調製されてもよく、その開示は参照により本明細書に組み入れられる。その他の適当なタバコは当技術分野において公知である。
一般に、本発明の組成物は経口使用または経口消費を対象とする。タバコを含有する組成物は、いずれかの適当な経口的に適合するフォーマットを用いて製造されてもよい。タバコはフォーマットと直接的に混合されてもよく、または別の方法でフォーマットにより支持されてもよい。例えば、組成物はフォーマットに堆積(deposit)されるか、フォーマットに混合されるか、フォーマットに囲まれるか、または別の方法でフォーマットと混合されるかしたタバコを、例えば、乾燥粒子、断片、顆粒、粉末またはスラリーとして含んでもよい。組成物中のタバコは可溶性であってもなくてもよく、または可溶性であると知覚されてもされなくてもよい。1つの態様では、組成物は唾のでないタバコ組成物である。組成物はまた、タバコの形態または種類の混合物を含んでもよい。組成物は発泡状または高密度状とされてもよい。発泡状の組成物は剛性または可塑性であってもよく、水溶性、不水溶性または熱可塑性のフォーマットに基づいてもよい。典型的な組成物が本明細書に記述される。1つの態様では、本発明の組成物は不燃性である。
フィルム
本発明の組成物は、経口的に崩壊可能でありうるフィルムとして成形されてもよい。そのようなフィルムは単層または多層を含んでもよい。単層フィルムはタバコ、フォーマットおよびその他の成分を、例えば、均一混合物の中に含むことができよう。多層フィルムはいくつかのタバコ含有層を、例えば、同じまたは異なる種類または大きさのタバコ、例えば、可溶性であると知覚されるタバコとともに含むことができる。多層はともに積層されてもよい。さらに、多層フィルムは本明細書に記述されるように、タバコを1つまたは複数の層および付加的な成分を含んだその他の層の中に含んでもよい。例えば、個々の層はフレーバー、甘味、色、崩壊速度または安定性(例えば、取り扱いの間または消費の間の)を目的に付加されてもよい。タバコはまた、2つまたはそれ以上の層の間に交互重ね配置で配置されてもよい。交互重ね配置中の1つまたは複数の層はまた、タバコを含んでもよい。多層を有するフィルムでは、それらの層は同じまたは異なる速度で崩壊してもよく、あるいは層は経口的に崩壊しなくてもよい。崩壊速度が異なる場合、組成物は層が崩壊するのに基づいて、異なる時間でタバコを供与してもよい。単層フィルムまたは多層フィルム内の個々の層はさらに、所望の物理的特性または所望の溶解もしくは解離速度を与えるように発泡または曝気されてもよい。
十分に撹拌された脱イオン水であって、予め180°Fまで加熱しておいたもの450グラムを含んだビーカーに、Dow ChemicalのK-3 (60%)、K-100 (35%)およびK4M (5%)グレードのヒドロキシプロピルメチルセルロース(HPMC) 50グラムの混合物を添加する。混合しながら、微粉砕タバコ40グラムをHPMC溶液に、微結晶性セルロース(FMC) 15グラム、澱粉(Grain Processing Corp.のB-700) 17グラム、グリセリン16グラム、ポリソルベート80 (Unichema) 0.8グラムおよびモノステアリン酸プロピレングリコール(DaniscoのPGMS) 4グラムとともに添加する。温度が100°F未満に下がったら、シナモンフレーバー10グラムおよびスクラロース(人工甘味料)2グラムを溶液に添加する。炭酸ナトリウム2グラムを添加して、pHを約7.5に調整する。全ての成分を添加して均一に分散させたら、混合物を湯浴の中に入れて、30分間続けて混合し、65°Fまでの温度に下げる。65°Fの温度で5,000センチポアズのBrookfield粘度を得るために必要に応じて、さらなる水を添加する。
実施例Bと同じ手順を用いて、溶液をタバコの添加なくして調製する。溶液がまだ熱いうちに、Sensient Colorsから提供される二酸化チタン分散液(50%二酸化チタン水溶液) 32グラムおよびFD&C Red No. 40レーキ(lake) (Sensient Colors) 0.01グラムを撹拌しながら添加する。溶液を65°Fまで冷却し、実施例Bに記述されているとおり、ガラスプレートに広げ、乾燥させてガラスプレートから取り去る。十分な強度と1.5ミル(0.015インチ)の乾燥フィルム厚の不透明な、淡い赤色のフィルムが製造される。
実施例Bの溶液の一部を、15ミル(0.015インチ)の一定の間隙を有するドローダウンナイフによってガラスプレートに広げる。このガラスプレートを恒温乾燥機の中に置き、フィルムを実施例Bと同じように乾燥させる。ガラスプレートを乾燥機から取り出し、室温まで冷却するが、しかしフィルムはガラスプレートから取り除かない。
実施例Cの溶液の一部を、5ミルの一定の間隙を有するドローダウンナイフによってガラスプレートに広げ、すでに述べたように恒温乾燥機の中で乾燥させる。実施例Bの溶液の一部を、15ミルの一定の間隙を有するドローダウンナイフによって実施例Cの乾燥フィルム全体に広げ、すでに述べたように恒温乾燥機の中で乾燥させる。実施例Cの溶液の一部を、5ミルの一定の間隙を有するドローダウンナイフによってガラスプレートに広げ、すでに述べたように恒温乾燥機の中で乾燥させる。得られるフィルムは厚さが3ミル(0.003インチ)であり、両側に不透明な、赤色の、フレーバー付きフィルムの層とタバコ含有フィルムの中心層とを有する3層からなる。1.0インチ×1.25インチのフィルム片は、通常、1分に満たないうちに口腔内で崩壊するであろう。
実施例Bのタバコ含有溶液100グラム量に、激しく混合しながらラウリル硫酸ナトリウム(界面活性剤) 0.5グラムを添加する。次いで、この溶液をSilverson Laboratory Homogenizer, Model L4RT-Wなどの高剪断ミキサーで混合して、均一な気泡構造を作り出す。次いで、この高度に泡だった溶液を、4ミル(0.040インチ)の一定の間隙を有するドローダウンナイフによってガラスプレートに広げ、恒温乾燥機の中で乾燥させる。乾燥した発泡フィルムは、ガラスプレートから取り去ると、4ミル(0.004インチ)の厚さを有する。1.0インチ×1.25インチ×厚さ4ミル(0.004インチ)のこの発泡フィルム片の重量は、実施例Bで調製の未発泡フィルムの同一片よりも35%低い。口腔内での発泡フィルムの溶解速度は、通常、実施例Bで調製の同一の未発泡フィルムと比べて速い。
30分間激しく混合しながら、脱イオン水60グラムに噴霧乾燥アラビアゴム(TIC Gums, Inc.) 40グラムおよびモノステアリン酸プロピレングリコール(PGMS) 0.4グラムを添加することにより、溶液をビーカーの中で調製する。この溶液10グラムに、激しく撹拌しながらFD&C Red No. 40レーキ0.01グラムを添加して、色の均一な分散を確実とする。この溶液を24時間覆って傍らに置き、混入した気泡全てを放散させる。次いで、この溶液の一部を、5ミル(0.005インチ)の一定の間隙を有するドローダウンナイフによってガラスプレートに広げる。フィルムが完全に乾くまで、ガラスプレートを170°Fに事前設定された恒温乾燥機の中に20分間置く。フィルムをガラスプレートから取り去ると、フィルムは粉々に砕けて高光沢の、色鮮やかな、赤色の薄片になる。この工程をその他のFD&Cレークで繰り返して、多くの色違いの薄片を製造する。フレーバーおよび人工甘味料を薄片に添加することもできる。
実施例Gで調製した溶液10グラムに、微粉砕タバコ粉末4グラムを添加する。フィルムをガラスプレート上で調製し、実施例Gにあるのと同じ方法で乾燥し、冷却し、取り去る。得られる薄片は50%タバコおよび50%アラビアゴムからなり、深茶色である。フレーバーを、必要に応じて、薄片に添加することができる。炭酸ナトリウムなどの材料を薄片に添加して、pHを調整することもできる。
フィルムを実施例Bと同じように調製する。フィルムがガラスプレート上でまだ湿っているうちに、計測された量の薄片を調製し、湿ったフィルムの全体に均一に広げる。次いで、ガラスプレートを恒温乾燥機の中で乾燥させる; フィルムを室温まで冷却し、その後、ガラスプレートから取り去る。通常、実施例Bの乾燥フィルムは1グラム(タバコを25%または0.25グラム含有する)の乾燥重量を有する。このフィルムを20等分のフィルム(1.0インチ×1.25インチ×2ミル)に分割する場合、各分割片は50ミリグラム(タバコを25%または12.5ミリグラム含有する)の重さになるはずである。タバコ薄片(これはタバコの50重量%である) 1グラムをフィルム全体に均一に広げる場合、完全なフィルム部片は2グラム(タバコを計0.75グラム含有する)の乾燥重量を有するはずである。20等分に分割する場合、各分割片は100ミリグラムの重さになるはずであり、タバコを37.5ミリグラム含むはずである。1.0インチ×1.25インチの大きさに切断されたフィルム片は、通常、1分に満たないうちに口腔内で崩壊するであろう。
装飾薄片(例えば、タバコを少しも含まない着色薄片)を用いてまたは着色薄片とタバコ含有薄片との混合物を使って、実施例Iに概説した手順を繰り返すことができる。得られるフィルムは色鮮やかな外観を有する。
MIX1
HM3PA2910(Wolff Cellulosics) 30.98 g
HM100PA2208(Wolff Cellulosics) 15.51 g
HM4000PA2910(Wolff Cellulosics) 2.60 g
B700(Grain Processing Corporation) 16.36 g
タバコ粉末(平均粒径 < 80 μm) 32.72 g
MIX2
Na2CO3 1.96 g
モノステアリン酸プロピレングリコール 0.65 g
ラウリル硫酸ナトリウム 0.65 g
MIX3
グリセリン 5.89 g
プロピレングリコール 5.22 g
ポリエチレングリコール400 6.54 g
シナモンフレーバー 6.54 g
タバコ香喫味改良剤(Hagelin) 2.62 g
スクラロース溶液25%(Tate & Lyle) 2.62 g
MIX1
HM3PA2910(Wolff Cellulosics) 30.98 g
HM100PA2208(Wolff Cellulosics) 15.51 g
HM4000PA2910(Wolff Cellulosics) 2.60 g
B700(Grain Processing Corporation) 16.36 g
タバコ粉末(平均粒径 < 80 μm) 32.72 g
MIX2
Na2CO3 1.96 g
モノステアリン酸プロピレングリコール 0.65 g
ラウリル硫酸ナトリウム 0.65 g
MIX3
グリセリン 4.58 g
プロピレングリコール 5.22 g
ポリエチレングリコール400 4.58 g
ミントフレーバー 9.81 g
タバコ香喫味改良剤(Hagelin) 2.62 g
スクラロース溶液25%(Tate & Lyle) 2.62 g
MIX1
HM3PA2910(Wolff Cellulosics) 30.98 g
HM100PA2208(Wolff Cellulosics) 15.51 g
HM4000PA2910(Wolff Cellulosics) 2.60 g
B700(Grain Processing Corporation) 16.36 g
タバコ粉末(平均粒径 < 80 μm) 32.72 g
MIX2
Na2CO3 1.96 g
モノステアリン酸プロピレングリコール 0.65 g
ラウリル硫酸ナトリウム 0.65 g
MIX3
グリセリン 1.31 g
プロピレングリコール 1.31 g
ポリエチレングリコール400 1.31 g
ピーチピューレ 100.0 g
ピーチフレーバー 3.27 g
タバコ香喫味改良剤(Hagelin) 2.62 g
スクラロース溶液25%(Tate & Lyle) 2.62 g
MIX1
HM3PA2910(Wolff Cellulosics) 38.48 g
HM100PA2208(Wolff Cellulosics) 19.27 g
HM4000PA2910(Wolff Cellulosics) 3.24 g
B700(Grain Processing Corporation) 20.32 g
タバコ粉末(平均粒径 < 80 μm) 14.39 g
MIX2
Na2CO3 2.16 g
モノステアリン酸プロピレングリコール 0.72 g
ラウリル硫酸ナトリウム 0.72 g
MIX3
グリセリン 7.19 g
プロピレングリコール 7.19 g
ポリエチレングリコール400 7.19 g
トリアセチン 6.47 g
シナモンフレーバー 10.80 g
タバコ香喫味改良剤(Hagelin) 2.88 g
スクラロース溶液25%(Tate & Lyle) 2.88 g
MIX1
HM3PA2910(Wolff Cellulosics) 38.48 g
HM100PA2208(Wolff Cellulosics) 19.27 g
HM4000PA2910(Wolff Cellulosics) 3.24 g
B700(Grain Processing Corporation) 20.32 g
Fibersol-2(Matsutani) 14.39 g
FD&C Red 40 Alum Lake 35〜42% (Sensient Colors) 0.29 g
MIX2
Na2CO3 2.16 g
モノステアリン酸プロピレングリコール 0.58 g
ラウリル硫酸ナトリウム 0.58 g
MIX3
グリセリン 7.19 g
プロピレングリコール 7.19 g
ポリエチレングリコール400 7.19 g
トリアセチン 6.47 g
シナモンフレーバー 10.79 g
タバコ香喫味改良剤(Hagelin) 2.88 g
スクラロース溶液25%(Tate & Lyle) 2.88 g
MIX1
HM3PA2910(Wolff Cellulosics) 38.48 g
HM100PA2208(Wolff Cellulosics) 19.27 g
HM4000PA2910(Wolff Cellulosics) 3.24 g
B700(Grain Processing Corporation) 20.32 g
タバコ粉末(平均粒径 < 80 μm) 14.39 g
MIX2
Na2CO3 2.16 g
モノステアリン酸プロピレングリコール 0.72 g
ラウリル硫酸ナトリウム 0.72 g
MIX3
グリセリン 7.19 g
プロピレングリコール 7.19 g
ポリエチレングリコール400 7.19 g
トリアセチン 6.47 g
ピーチピューレ 100.0 g
ピーチフレーバー 3.60 g
タバコ香喫味改良剤(Hagelin) 2.88 g
スクラロース溶液25%(Tate & Lyle) 2.88 g
MIX1
HM3PA2910(Wolff Cellulosics) 38.48 g
HM100PA2208(Wolff Cellulosics) 19.27 g
HM4000PA2910(Wolff Cellulosics) 3.24 g
B700(Grain Processing Corporation) 20.32 g
Fibersol-2(Matsutani) 14.39 g
MIX2
Na2CO3 1.44 g
モノステアリン酸プロピレングリコール 0.72 g
ラウリル硫酸ナトリウム 0.72 g
MIX3
グリセリン 3.60 g
プロピレングリコール 3.60 g
ポリエチレングリコール400 3.60 g
トリアセチン 3.60 g
TiO2懸濁液50%(Sensient Colors) 28.04 g
タバコ香喫味改良剤(Hagelin) 1.44 g
スクラロース溶液25%(Tate & Lyle) 1.44 g
Klucel LF (Hercules/Aqualon) 3448.0 g
Na2CO3 181.0 g
スクラロース(Tate & Lyle) 45.0 g
プロピレングリコール 363.0 g
タバコ粉末(平均粒径 < 80 μm) 1451.0 g
水 2344.0 g
MIX1
HM3PA2910(Wolff Cellulosics) 13.84 g
HM100PA2208(Wolff Cellulosics) 7.24 g
HM4000PA2910(Wolff Cellulosics) 1.21 g
B700(Grain Processing Corporation) 7.63 g
ゼラチン 0.61 g
タバコ粉末(平均粒径 < 80 μm) 15.27 g
MIX2
Na2CO3 0.91 g
モノステアリン酸プロピレングリコール 0.30 g
ラウリル硫酸ナトリウム 0.30 g
MIX3
グリセリン 2.14 g
プロピレングリコール 2.44 g
ポリエチレングリコール400 2.14 g
ミントフレーバー 4.58 g
タバコ香喫味改良剤(Hagelin) 1.22 g
スクラロース溶液25%(Tate & Lyle) 1.22 g
MIX1
HM3PA2910(Wolff Cellulosics) 11.40 g
HM100PA2208(Wolff Cellulosics) 7.24 g
HM4000PA2910(Wolff Cellulosics) 1.21 g
B700(Grain Processing Corporation) 7.63 g
ゼラチン 3.05 g
タバコ粉末(平均粒径 < 80 μm) 15.27 g
MIX2
Na2CO3 0.91 g
モノステアリン酸プロピレングリコール 0.30 g
ラウリル硫酸ナトリウム 0.30 g
MIX3
グリセリン 2.14 g
プロピレングリコール 2.44 g
ポリエチレングリコール400 2.14 g
ミントフレーバー 4.58 g
タバコ香喫味改良剤(Hagelin) 1.22 g
スクラロース溶液25%(Tate & Lyle) 1.22 g
MIX1
HM3PA2910(Wolff Cellulosics) 8.35 g
HM100PA2208(Wolff Cellulosics) 7.24 g
HM4000PA2910(Wolff Cellulosics) 1.21 g
B700(Grain Processing Corporation) 7.63 g
ゼラチン 6.11 g
タバコ粉末(平均粒径 < 80 μm) 15.27 g
MIX2
Na2CO3 0.91 g
モノステアリン酸プロピレングリコール 0.30 g
ラウリル硫酸ナトリウム 0.30 g
MIX3
グリセリン 2.14 g
プロピレングリコール 2.44 g
ポリエチレングリコール400 2.14 g
ミントフレーバー 4.58 g
タバコ香喫味改良剤(Hagelin) 1.22 g
スクラロース溶液25%(Tate & Lyle) 1.22 g
チュアブル錠は以下の成分を用いて形成することができる: 圧縮性糖類 (40%); タバコ (20%); デキストロース (25%); マルトデキストリン (13%); 着色剤 (0.05%);フレーバー (1.35%); およびステアリン酸マグネシウム (0.60%)。
熱可塑性錠は以下の成分(部として)を用いて形成することができる: ヒドロキシプロピルセルロース(HPC) 54; タバコ 27; 微結晶性セルロース 10; プロピレングリコール 4; 人工甘味料 2; フレーバー 2; および安定剤 0.2。これらの成分を乾燥混合し、HPCを溶かすのに必要なバレル温度(通常、340〜370°F)を用いて押出成形機に送り込む。直径およそ1/2インチの棒を押出して、錠剤を形成するのに十分な大きさに切断する。
表AB2に記載の成分量を別の容器の中に量り分けた。水和済みアラビアゴム(Gum Arabic Pre-hydrated) (乳化剤)を水にゆっくり添加し、ステンレス製容器中にて高剪断撹拌下で混合した。完全な溶解後、M 585マルトデキストリン (Grain Processing Corporation)を水にゆっくり添加した。M585が完全に溶解したら、スクラロース甘味料(Tate & Lyle)をゆっくり添加し、確実に完全溶解させるために徹底的に混合した。
表AB1に記載のとおり、マンニトール(甘味料)およびタバコ粉末(絶乾ベース)の配合量を一緒に混合し、製造器の中に入れた。
結合溶液を乾燥成分の混合物に塗布して最終造粒体を形成させるため、Vector Multiflo-15流動層塗布機を使用した。そのコントロールパネルコンピュータで、手動プロセスを選択した。表AB3にある機器運転パラメータをプログラムに読み込んだ:
(表AB3)Vector Multiflo-15 Fluid Bedパラメータ設定
乾燥成分が流動層室内で流動化されて40〜45℃の温度に達したら、造粒体を形成させるため、結合溶液を乾燥成分にゆっくり噴霧した。ノズル圧を22 psiにおよび気流を200 CFMに設定した。十分な製造物の移動または流動層室内での流動化を確実とするため、気流を増大させた。全ての結合溶液が塗布されたら、気流を200 CFMまで低下させた。製造物の温度が約43℃に達したら、この工程を停止させた。
次いで、造粒化された材料を12メッシュのふるいに通して寸法で分類した。ステアリン酸マグネシウム(滑沢剤)を40メッシュのふるいに通して寸法で分類した。表AB4に記載のステアリン酸マグネシウムの配合量を造粒化された材料と、プラスチック袋の中で混合し、2分間手で振った。
(表AB4)錠剤を形成するための成分の配合
造粒化された材料に加えて滑沢剤を圧縮ホッパの中に添加した。表AB5に記載の以下のパラメータをVanguard VSP 8 Mini Rotary Pressに設定した:
(表AB5)タバコ錠用のパラメータ
既に記述したとおり、造粒化された材料およびステアリン酸マグネシウムを適切なふるいに通して寸法で分類した。ステアリン酸マグネシウムの配合量(高速性崩壊錠の場合には0.75%または緩徐性崩壊錠の場合には1.00%)を造粒化された材料と、プラスチック袋の中で混合し、2分間手で振った。
造粒化された材料およびステアリン酸マグネシウムをそれぞれ、12メッシュおよび40メッシュのふるいに通して寸法で分類した。ステアリン酸マグネシウムの配合量(高速性崩壊錠の場合には0.50%または緩徐性崩壊錠の場合には1.00%)を造粒化された材料と、プラスチック袋の中で混合し、2分間手で振った。
ウィンターグリーンフレーバーをシナモンフレーバーの代わりに使用したことを除いて、実施例ADのタバコ錠を作製するため同じ手順にしたがった。
次いで、製品原材料を12メッシュのふるいに通して寸法で分類した。ステアリン酸マグネシウムを40メッシュのふるいに通して寸法で分類した。ステアリン酸マグネシウムの配合量(高速性崩壊錠の場合には0.50%または緩徐性崩壊錠の場合には0.75%)を造粒化された材料と、プラスチック袋の中で混合し、2分間手で振った。
結合溶液の調製について既に記述した手順にしたがった。表AF1に記載されている配合量のリンゴフレーバー、天然苦味抑制物質(Comax)、およびNa2CO3を結合溶液に添加した。結合溶液の調製のための残る手順、乾燥成分(ラクトース増量剤に加えてタバコ粉末)の調製、Vector Multiflo-15 Fluid Bed Chamber(流動層室)の準備、および造粒化工程にしたがった。
次いで、製品原材料を12メッシュのふるいに通して寸法で分類した。ステアリン酸マグネシウムを40メッシュのふるいに通して寸法で分類した。ステアリン酸マグネシウムの配合量(緩徐性崩壊錠の場合には0.75%)を造粒化された材料と、プラスチック袋の中で混合し、2分間手で振った。
20% Opadry II水溶液を製造業者による指示のとおり調製し、被覆の前に45分混合させた。
錠剤(5.5〜6.5 KG)をVector/Freund Hi-Coaterパンコーティング機のコーティングパンの中に入れて、排気温度が45℃に達するまで加温した。これは錠剤の磨耗を最小限に抑えるため、パンを5 RPM未満で稼動させながら行った。75℃および100 CFMの空気を-0.5"水のパン圧でパン全体に通した。
以下の成分を個別の容器の中に量り分けた:
Klucel EF (Hercules) 60 g
タバコ粉末 75 g
タバコ香喫味改良剤 6 g
コーンシロップ (65%) 45 g
スクロース 45 g
B700 (Grain Processing Corp.) 51 g
スクラロース溶液25%(Tate & Lyle) 3 g
プロピレングリコール 3 g
炭酸ナトリウム 1.5 g
水 6 g
ペパーミント油 4.5 g
水 ポーション1 (熱) 120 g
水 ポーション2 (冷) 120 g
以下の成分を個別の容器の中に量り分けた:
HPMC 2910 HM E5/6 Bv (Celanese) 60 g
タバコ粉末 75 g
タバコ香喫味改良剤 6 g
コーンシロップ (65%) 45 g
スクロース 45 g
B700 (Grain Processing Corp.) 39 g
スクラロース溶液25%(Tate & Lyle) 3 g
プロピレングリコール 15 g
炭酸ナトリウム 1.5 g
水 6 g
ペパーミント油 4.5 g
水 ポーション1 (熱) 120 g
水 ポーション2 (室温) 120 g
市販の圧縮装置を使って、2つまたはそれ以上の異なる層を有する錠剤を調製することができる。これらの層の組成は、組成が同じものまたは異なるものとすることができる。個々の層を色、フレーバー、タバコ類、タバコ含有量、溶解速度、およびその他類似の特徴により差別化することができる。例えば、ある層は素早く崩壊して、フレーバーまたはフレーバーマスキング成分を放出することができよう。タバコ粉末を含有する別の層はもっとゆっくり崩壊し、それによって徐々にタバコを露出させることができよう。
タバコ組成物はまた、容易に取り扱われるように十分に硬い製品に成形されてもよい。これらの成形品は物理的特性が異なってもよく、高可塑性から高剛性の部分品まで多岐にわたってもよい。そのような製品は任意の形状に成形されてもよく、高密度状または発泡状とされてもよい。これらの組成物は通常、完成した部分品の重量の2〜50%、好ましくは5〜10%の水分含有量を有する。典型的な形状としては、管状、爪楊枝状、スティック状、ねじれ状、または中実棒状が挙げられる。通常、成形部はしゃぶられるかまたは咀嚼されて、長時間、タバコ官能特性成分を口腔内に放出できよう。成形部は経口的に崩壊してもまたは崩壊しなくてもよい。崩壊する部分は1〜60分、好ましくは1〜10分かけて崩壊してもよい。
(表AK2)
タバコ棒はタバコ(54部); フレーバー(2); 不溶性繊維(28); CMC(10); 人工甘味料(0.2); および微結晶性セルロース(30)から作製する。粘性ペーストを形成させるのに十分な水(例えば、140部)を添加する。そうすれば、このペーストは押出し機を通じた加工処理に適する。適当な押出し機は、パスタ押出し機とダイとが付いたキッチンエイド(Kitchen Aid)ミキサーであろう。次いで、パスタダイを通じた押出しから調製された棒をらせん巻き機用の成形マンドレルとして使用することができ、タバコ含有フィルムを使って、タバコ芯の周囲に巻き付けを施すことができる。
MIX1
HM100PA2208(Wolff Cellulosics) 11.16 g
B700(Grain Processing Corporation) 55.77 g
シナモン粉末 24.54 g
Fibersol-2(Matsutani) 44.61 g
Na2CO3 6.69 g
スクラロース(Tate & Lyle) 2.22 g
タバコ粉末(平均粒径 < 80 μm) 55.77 g
MIX2
グリセリン 11.16 g
シナモンフレーバー 11.16 g
MIX1
HM100PA2208(Wolff Cellulosics) 11.16 g
B700(Grain Processing Corporation) 55.77 g
スクロース 22.29 g
Fibersol-2(Matsutani) 44.61 g
Na2CO3 6.69 g
スクラロース(Tate & Lyle) 1.11 g
リンゴ酸 2.22 g
タバコ粉末(平均粒径 < 80 μm) 55.77 g
MIX2
グリセリン 11.16 g
リンゴフレーバー 12.27 g
B700(Grain Processing Corporation) 3327.1 g
B825(Grain Processing Corporation) 120.0 g
Na2CO3 181.4 g
スクラロース(Tate & Lyle) 45.4 g
グリセリン 362.9 g
タバコ粉末(平均粒径 < 80 μm) 1451.5 g
水 3473.0 g
本発明の組成物はさらに、ゲルまたはゲルビーズとして作製されてもよい。この組成物はタバコを含有する可溶性または不溶性ゲルを含むことができる。ゲルは他の原料を封入するために使われてもよく、または他の原料がゲルを封入してもよい。ゲルは70%もの水を含有する水和化したフォーマットで消費されてもよい。ゲルはまた、1%から70%の水を含有する部分をもたらすように乾燥されてもよい。ゲルの中に保持される水の量は、最終製品において望まれる特性に依る。幅広い官能特性を与えるタバコ含有ゲルを調製することが可能である。
実施例AR ゲルビーズ
CMC-7MFの4%溶液100 gおよびタバコ20 gを混合する。液滴を水溶性で、食用の三価塩(例えば、AlCl3またはAl2(SO4)3)の5%溶液の中に堆積させる。次いで、液滴の表面を風乾または穏やかなオーブン乾燥で乾燥させる。
ゼラチン10 gおよび水90 gを混合し、140°Fまで加熱してゼラチンを溶解させる。タバコ20 gを添加し、鋳型の中に注ぎ込む。ゲルの強度はゼラチン6gおよび寒天4 gを代わりに用い、190°Fまで加熱して溶解させることによって増大させることができる。
以下の表および記述は本発明の不溶性ゲル、すなわち、経口的に崩壊しないゲルを製造するのに典型的な成分を示す。
(表AT1)カラギナンゲル
KClを添加した後、組成物を180°Fで鋳造し、徹底的に混合する。
水性3.9%カッパカラギナン416グラムおよびタバコ51.0グラムを混合した。この溶液を撹拌しながら180°F〜190°Fまで加熱し、次いで溶液を所望の形状の鋳型の中に堆積させた。冷却させた後、得られた固形物を鋳型から取り出し、所望のタバコ濃度およびゲル粘稠度に乾燥させた。
実施例AV 可溶性ゲル
水性20%ゼラチン100グラムおよびタバコ33グラムを混合した。この溶液を撹拌しながら140°F〜150°Fまで加熱し、次いで溶液を所望の形状の鋳型の中に堆積させた。所望の硬度に応じて数分から数日間の冷却の後、得られた固形物を鋳型から取り出し、所望のタバコ濃度およびゲル粘稠度に乾燥させた。
(表AV1)ゼラチンゲル
沸騰するまで加熱した水288 gにアルギン酸ナトリウム12 gを添加し、続いて30分間またはその溶液が均一になるまでホットプレート上で水を撹拌および連続加熱することにより、4%アルギン酸ナトリウム(Keltone LV, International Specialty Products)の溶液を調製した(原液A)。リン酸水素二ナトリウム七水和物33.5 gを水200 mlに、その塩が溶解するまで得られた混合物を加温および撹拌しながら溶解させ、続いてこの溶液を水で250 mlに調整することにより、0.50 Mリン酸水素二ナトリウムの第二溶液を調製した。0.50 Mリン酸ナトリウム水溶液100 gにタバコ20グラムを添加し、得られた溶液を5分間撹拌した(原液B)。得られたタバコスラリー(原液B) 50 gに4%アルギン酸ナトリウム水溶液(原液A) 50 mlを添加し、得られた混合物を5分間撹拌した。フレーバーを添えるため、粉末スクラロース0.20 gおよびペパーミント油0.80 g (精留済, Blend SX 0910001, Essex Labs)を得られたタバコ/アルギン酸ナトリウムスラリーに添加し(溶液C)、この混合物を2分間撹拌した。
本発明の組成物はまた、消耗単位として製造されてもよい。これらの単位は可食物または非可食物として包装されてもよい。1つの態様では、消耗単位としてはタバコ(例えば、無煙タバコ)またはタバコ組成物、例えば、薄片、錠剤、ビーズ、顆粒、もしくは本明細書に記載のその他のタバコ組成物、および包装、例えば、ポーチが挙げられる。包装は、1つの態様では、接着剤の機能を果たして組成物をまとめてもよい、例えば、複数の錠剤、ビーズ、薄片などをまとめてもよい。または、包装は組成物、例えば、粘着性のない錠剤、ビーズ、薄片などを封入してもよい。組成物はさらに、液体、例えば、タバコスラリーを含んでもよい。包装は経口的に崩壊可能であってもまたはなくてもよい。経口的に崩壊可能な包装を使用して、水性または非水性液体を封入してもよい。水性液体が水溶性包装とともに使われる場合、その液体は包装の溶解を阻止する作用物質を含む。典型的な作用物質としては、糖類、塩類、および水がもはや水溶性包装と相互作用しその包装を溶解することができないレベルにまで水分活性を低減させるのに十分に水を結合できるその他の親水剤が挙げられる。包装はまた、鋳造可能なタバコ組成物であって、口腔に適合するかまたは口腔内でその形状を維持する組成物を封入してもよい。1つの態様では、経口的に崩壊可能な包装は、可溶性と知覚される無煙タバコ、例えば、乾いた嗅ぎタバコまたはタバコ(例えば、粒径80 μm未満)を封入してもよい。経口的に崩壊可能な無煙タバコ組成物は、主題の技術にしたがって作製された可食フィルム(これはタバコを含んでもまたは含まなくてもよい)を用い、連続熱成形装置もしくは水平成形/充填/シール装置またはその他適当な包装装置で成形された消耗ポーションパックに導入されてもよい。消耗単位はまた、2つまたはそれ以上の、個別包装されたタバコ部分、例えば、全てがさらに大きな包装内に含まれるもの、1つがその他の部分を含むもの、または各部分のいずれもが他のものとともに含まれないものを含んでもよい。複数の部分が使用される場合、任意の2つが同じまたは異なるフレーバー、色、タバコの形態、または崩壊速度を有してもよい。
以下の記述は本発明の消耗単位を製造するのに典型的な成分を提供する。
本明細書に記述される組成物のいずれも、フィルムまたはカプセルで封入することができる。カプセルの材料は色、安定性(例えば、保存、取り扱いもしくは消費の間の)、または官能特性(例えば、フレーバー、甘味、香りもしくは口当たり)を提供してもよい。カプセルの材料はまた、タバコを含んでもよい。
無煙タバコ粒子または粉末、例えば、嗅ぎタバコは水崩壊性バッグの中に入れられてもよい。バッグは口腔内に入れられると、一定の時間後に崩壊する。バッグは一人分のタバコを含んでもよい。バッグはまた、本明細書に記載のさらなる添加物を含んでもよい。その包装が崩壊したら、タバコは成形可能なプラグ(moldable plug)としてそれ自体に付着してもよい。
無煙タバコ粒子または粉末は、水溶性包装フィルムに積層された目の粗いまたは高度に多孔質の包装材料、例えば、織布、紙またはプラスチック製フィルムから形成されるバッグの中に入れられてもよい。水溶性フィルム層はタバコ内容物に対する保護をもたらし、タバコが保存および取り扱いの間に不溶性材料の開口部を通じて移動するのを阻止する。バッグが口腔内に入れられると、水溶性フィルム層は溶解または崩壊する。
フィルムの実施例N、O、PおよびQの本明細書に記載のフィルムを使用して、タバコ含有ポーチを製造した。個々のユニットおよそ1インチ×11/4インチを、製造したフィルムの各シートから切断した。このユニットを長手方向に折り返し、Clamco Model 210-8Eインパルスシーラーによって熱融着させた。この形成ユニットの片端を同様に、同じ方法で密封した。この形成ポーチの内部にフレーバー付きタバコ造粒体を入れて、ポーチを密封するのに記述したようにして最後の密封を行った。このタバコ含有ポーチは20秒から1分の間に口腔内で崩壊し、ポーチの内容物を放出した。
タバコはまた、不溶性マトリックス上に被覆されてもよく、または不溶性マトリックス内に封入されてもよい。フィルムの形成時と同様に、フォーマットの水溶液中にタバコを分散させて、スラリーを形成させることができる; このスラリーを不溶性マトリックス上に被覆することができ、または多孔質の不溶性マトリックスを飽和させるのに使用することができる。その後、スラリーは可溶性または不溶性ゲルに変換されてもよく、あるいはそれは単に乾燥されて被覆を形成してもよい。この被覆/飽和した不溶性マトリックスの部分が口腔内に入れられると、官能特性成分の浸出が溶解、咀嚼またはその他の手段を通じて起こる。1つの態様では、フォーマット中のタバコを多孔性マトリックス、例えば、連続気泡ポリウレタンフォームまたは高ロフトポリエステル不織布に導入する。この不溶性マトリックスは口腔内に完全に入れられてもよく、あるいはそれはスティックまたはその他の柄であって、消費の間に部分的に口腔外のままとなるものに配置されてもよい。別の態様では、フォーマット中のタバコを非相溶性液体、例えば、カルナウバワックスの分散水と混合し、金型の中に堆積し、タバコスラリーがろう様構造内に配置されるような相分離を引き起こすように素早く冷却する。これらのマトリックスはまた、咀嚼可能であってもよい。
実施例BB ポリウレタンフォームA
本明細書に記載の微粉砕タバコを含むフィルム形成組成物を使用して、連続気泡ポリウレタンフォーム(Stephenson & Lawyer, Inc. Grand Rapids, MI)の断片(例えば、12インチ×12インチ×1インチ)を飽和させる。飽和したポリウレタンフォームを金皿に置いて、175°Fに事前設定された空気循環恒温乾燥機の中に1時間置く。このポリウレタンフォームを乾燥機から取り出すと、タバコ含有組成物が乾燥し、ポリウレタンフォームの隙間全てを均一に覆う被覆を形成していた。被覆されたポリウレタンフォームを口腔内に入れるのに適したサイズの断片(例えば、1インチ×1インチ×1インチ)に切断する。ポリウレタンフォームは、使用後に、口腔から取り出して捨てる。
本明細書に記載の微粉砕タバコを含む、アルギン酸ナトリウムおよびカルシウム塩のゲル組成物を使用して、連続気泡ポリウレタンフォーム(例えば、12インチ×12インチ×1インチ)を飽和させる。このアルギン酸塩のゲルを180°Fの温度に維持して、早過ぎるゲルの凝固を防ぐ。アルギン酸塩の熱いゲルをポリウレタンフォームに注ぎ、これを金皿に置いて、その後、40°Fの冷蔵庫の中で素早く冷却してゲルを凝固させる。このポリウレタンフォームを次に、175°Fに事前設定された恒温乾燥機の中に10分間置いて、ゲルを表面乾燥させ、水分含有量をゲルの乾燥重量に基づいて50%まで低下させる。部分的に乾燥させたゲルがポリウレタンフォーム中の孔隙を満たす。このポリウレタンフォームを刻んで、口腔内に入れる。不溶性マトリックス中のゲルのさらなる例は、ゲルをさらに低い水分含有量(例えば、ゲルの乾燥重量に基づいて10%)まで乾燥させることにより得られる。タバコ含有ゲルはフォームマトリックス内で堅固な、弾性のある集合組織を示し、口腔内に入れられて咀嚼されると、ゆっくり再水和する。ポリウレタンフォームは、使用後に、口腔から取り出して捨てる。
前述のように、材料の薄シートまたはフィルムを巻き付けるか、押出すか、ブロー成形するかまたは別の方法で成形して、管、ストローまたはその他の中空形状を形作ってもよい。典型的なフィルムまたはシート材料は、本明細書のフィルムの項に開示されている。そのような中空形状は単層または多層であってもよい。多層が使われる場合、タバコを含むものもあれば、色、フレーバー、甘味料、または本明細書に記載の他の化合物を含むものもあってよい。取り扱いの間の安定性のためまたは消費の間の崩壊を制御するため、異なる層が利用されてもよい。らせん状に巻き付けられた中空形状、例えば、管またはストローは解けないように接着剤(例えば、CMCまたはグアー)を必要としてもよい。多層中空形状の層は同じまたは異なる色またはフレーバーを含んでもよく、そのような層は同じまたは異なる速度で崩壊してもよい。フィルムと同様に、タバコは1つまたは複数の層のなかに配置されてもよく、あるいは層の間に交互重ね配置で配置されてもよい。中空形状はまた、崩壊を加速する崩壊剤を含んでもよい。
本明細書に記述される任意のタバコ組成物はさまざまな方法で修飾されてもよい。例えば、組成物は単層または多層に被覆されてもよい。そのような被覆は、例えば、取り扱い、崩壊速度、味および色彩のために利用される。典型的な被覆としてはHPMCが挙げられる。当技術分野において公知の工程、例えば、噴霧法、ブラッシング法、ロール塗布法、ドクターバー鋳造法、スロット塗布法、押出し塗布法、熱溶融物堆積法、粒子または薄片の堆積法、およびその他の典型的な方法を利用して、被覆または装飾模様がフィルムの表面に塗布されてもよい。被覆はつや消しまたはつや出しであってもよい。被覆は本明細書に記述されるとおり、色、フレーバー、甘味料またはフレーバーマスキング剤を含んでもよい。被覆中の色、フレーバー、甘味料またはフレーバーマスキング剤は、基礎をなす組成物と同じであってもまたは異なっていてもよい。さらに、複数の被覆が同じまたは異なる色、フレーバー、甘味料またはフレーバーマスキング剤を含んでもよい。被覆はまた、基礎をなす組成物と異なる速度で崩壊してもよい。例えば、被覆は基礎をなす組成物よりも速く崩壊して、フレーバーまたはその他の官能特性成分の噴出をもたらしてもよい。経口的に崩壊可能な被覆はさらに、経口的に崩壊しない組成物に載せられてもよい。経口的に崩壊しない被覆が経口的に崩壊する組成物に載せられてもよく、そのような被覆は、例えば、咀嚼によって除去されてもよい。被覆はさらに、組成物中の揮発性成分の蒸発を阻止するためにおよび使用前の組成物の力学的な染み込みを阻止するために利用されてもよい。被覆はまた、タバコを含んでもよい。
個々の組成物は組成物の内容に対し必要に応じて包装されよう。組成物は防水ケースの中に保存されて、40°Fから120°Fで安定であることが好ましい。典型的には、組成物は保存の間、乾燥性、可塑性および非付着性である。あるいは、中身がつかない仕切り、例えば、プラスチック製のフィルムまたは紙を1単位間に使い、組成物を包装してもよい。組成物はバルク状で提供してもよく、そこから個々の一回分量を分離する。
以下のタバコ溶液が本明細書に記載の任意の組成物の中に含まれてもよい。
冷水78.6グラムの中に30分間激しく混合しながらキサンタン(C. P. KelcoのKelzan) 0.2グラムを混合することによって、溶液を調製する。この溶液に、激しく混合し続けながら微粉砕タバコ20グラム、スクラロース0.2グラム、およびシナモンフレーバー2グラムを添加する。溶液粘度を水で50センチポアズの粘度に調整する。
冷水76.8グラムと30分間激しく混合しながらキサンタン(C. P. KelcoのKelzan) 1グラムを混合することによって、溶液を調製する。これに、激しく混合し続けながら微細タバコ20グラム、スクラロース0.2グラムおよびシナモンフレーバー2グラムを添加する。溶液粘度は1,500センチポアズである。
冷水35.8グラムとグリセリン40グラムの混合物に30分間激しく混合しながら中粘度のカルボキシメチルセルロース(Hercules, Inc.のCMC 7MF) 2グラムを添加することによって、ペーストを調製する。この混合物に、微細タバコ粉末20グラム、スクラロース0.2グラム、およびシナモンフレーバー2グラムを添加する。極めて剪断感応性である高粘度のペーストが調製される。このペーストは、管またはその他の圧搾可能な包装であって、圧搾による剪断力が粘度を低下させてペーストの流れを可能にするものに導入することができる。
本発明の具体的な態様の記述は、説明の目的で示されている。網羅的であることも本発明の範囲を本明細書に記述されている特定の形態に限定することも意図されない。本発明をいくつかの態様に関連して記述してきたが、特許請求の範囲に記載の本発明の範囲および趣旨から逸脱することなく、さまざまな変更をなすことができることを当業者は理解するであろう。本明細書において参照される全ての特許、特許出願および公報は、参照により本明細書に組み入れられる。
Claims (10)
- 管、爪楊枝、スティック、または棒の形状に押出すことにより形成される、タバコ属のいずれかの仲間のいずれかの粉砕部分を含むタバコ、およびフォーマットを含む不燃性の経口的に崩壊可能な無煙タバコ組成物であって、粉砕部分が250μm以下の平均粒径を有し、フォーマットが水溶性ポリマーである、前記タバコ組成物。
- 2〜50%の水分含有量を有する、請求項1記載の組成物。
- 1〜60分で崩壊する、請求項1記載の組成物。
- 口腔内に一部のみを割り当てるような大きさにされ、かつ6インチ未満もしくは2.5インチ未満の長さを有する、請求項1記載の組成物。
- 各部位がフレーバーまたは色を含む、1つまたは複数の不連続部位をさらに含むか、または各部位がストランドを含み、各ストランドがともにねじれて組成物を形成する、請求項1記載の組成物。
- 少なくとも1つの部位が異なるフレーバーまたは色を含む、請求項6記載の組成物。
- 各部位が異なるフレーバーまたは色を含む、少なくとも2つの部位を含む、請求項6記載の組成物。
- 射出成形、圧縮成形、オーバーモールド、押出し、またはスラリー工程により形成される、請求項1記載の組成物。
- 複数の前記管、爪楊枝、スティック、または棒が、ねじれ状に形成される、請求項1記載のタバコ組成物。
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- 2004-11-05 WO PCT/US2004/036793 patent/WO2005046363A2/en active Application Filing
- 2004-11-05 EP EP04800749A patent/EP1691631A4/en not_active Withdrawn
- 2004-11-05 CN CN201210162595.1A patent/CN102669810B/zh not_active Expired - Fee Related
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- 2004-11-05 US US10/982,248 patent/US8469036B2/en active Active
- 2004-11-08 TW TW093133982A patent/TWI428093B/zh not_active IP Right Cessation
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2007
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- 2008-12-29 US US12/345,063 patent/US10765140B2/en active Active
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2011
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2012
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2018
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CN102669810A (zh) | 2012-09-19 |
EP1691631A4 (en) | 2012-09-05 |
US20090133703A1 (en) | 2009-05-28 |
US20190029313A1 (en) | 2019-01-31 |
US20050244521A1 (en) | 2005-11-03 |
US8469036B2 (en) | 2013-06-25 |
CN102669810B (zh) | 2014-11-05 |
US20090133704A1 (en) | 2009-05-28 |
HK1175963A1 (en) | 2013-07-19 |
TW200529772A (en) | 2005-09-16 |
WO2005046363A3 (en) | 2006-11-16 |
WO2005046363A2 (en) | 2005-05-26 |
US20120199149A1 (en) | 2012-08-09 |
JP5455131B2 (ja) | 2014-03-26 |
US20200329755A1 (en) | 2020-10-22 |
JP2007515950A (ja) | 2007-06-21 |
CN104397869B (zh) | 2016-06-08 |
US8636011B2 (en) | 2014-01-28 |
JP2012085643A (ja) | 2012-05-10 |
US10098376B2 (en) | 2018-10-16 |
US10765140B2 (en) | 2020-09-08 |
AU2004289248B2 (en) | 2012-05-03 |
AU2004289248A1 (en) | 2005-05-26 |
BRPI0415741B1 (pt) | 2013-07-23 |
EP1691631A2 (en) | 2006-08-23 |
TWI428093B (zh) | 2014-03-01 |
CN104397869A (zh) | 2015-03-11 |
BRPI0415741A (pt) | 2006-12-19 |
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