JP2010510048A5 - - Google Patents
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- JP2010510048A5 JP2010510048A5 JP2009537275A JP2009537275A JP2010510048A5 JP 2010510048 A5 JP2010510048 A5 JP 2010510048A5 JP 2009537275 A JP2009537275 A JP 2009537275A JP 2009537275 A JP2009537275 A JP 2009537275A JP 2010510048 A5 JP2010510048 A5 JP 2010510048A5
- Authority
- JP
- Japan
- Prior art keywords
- composition
- gold
- allyl
- support
- catalyst
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000010931 gold Substances 0.000 claims 21
- 239000000203 mixture Substances 0.000 claims 19
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims 7
- 229910052737 gold Inorganic materials 0.000 claims 7
- 239000003446 ligand Substances 0.000 claims 5
- 150000001336 alkenes Chemical class 0.000 claims 4
- 239000003054 catalyst Substances 0.000 claims 4
- 239000012018 catalyst precursor Substances 0.000 claims 4
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims 4
- 238000000034 method Methods 0.000 claims 3
- 239000002105 nanoparticle Substances 0.000 claims 3
- 239000002245 particle Substances 0.000 claims 3
- MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 claims 2
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 claims 2
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims 2
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 claims 2
- 230000015572 biosynthetic process Effects 0.000 claims 2
- ZSWFCLXCOIISFI-UHFFFAOYSA-N cyclopentadiene Chemical compound C1C=CC=C1 ZSWFCLXCOIISFI-UHFFFAOYSA-N 0.000 claims 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims 2
- 229910052709 silver Inorganic materials 0.000 claims 2
- 239000004332 silver Substances 0.000 claims 2
- 239000010936 titanium Substances 0.000 claims 2
- LWJHSQQHGRQCKO-UHFFFAOYSA-N 1-prop-2-enoxypropane Chemical compound CCCOCC=C LWJHSQQHGRQCKO-UHFFFAOYSA-N 0.000 claims 1
- HECLRDQVFMWTQS-RGOKHQFPSA-N 1755-01-7 Chemical compound C1[C@H]2[C@@H]3CC=C[C@@H]3[C@@H]1C=C2 HECLRDQVFMWTQS-RGOKHQFPSA-N 0.000 claims 1
- ATVJXMYDOSMEPO-UHFFFAOYSA-N 3-prop-2-enoxyprop-1-ene Chemical compound C=CCOCC=C ATVJXMYDOSMEPO-UHFFFAOYSA-N 0.000 claims 1
- RMZIOVJHUJAAEY-UHFFFAOYSA-N Allyl butyrate Chemical compound CCCC(=O)OCC=C RMZIOVJHUJAAEY-UHFFFAOYSA-N 0.000 claims 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 claims 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 1
- XYLMUPLGERFSHI-UHFFFAOYSA-N alpha-Methylstyrene Chemical compound CC(=C)C1=CC=CC=C1 XYLMUPLGERFSHI-UHFFFAOYSA-N 0.000 claims 1
- 150000001408 amides Chemical class 0.000 claims 1
- 150000001412 amines Chemical class 0.000 claims 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 1
- 239000011230 binding agent Substances 0.000 claims 1
- VASBMTKQLWDLDL-UHFFFAOYSA-N but-3-enoxybenzene Chemical compound C=CCCOC1=CC=CC=C1 VASBMTKQLWDLDL-UHFFFAOYSA-N 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 229910002091 carbon monoxide Inorganic materials 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 claims 1
- 239000013078 crystal Substances 0.000 claims 1
- 150000001993 dienes Chemical class 0.000 claims 1
- 150000004820 halides Chemical class 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 150000003949 imides Chemical class 0.000 claims 1
- 150000002466 imines Chemical class 0.000 claims 1
- 229910052741 iridium Inorganic materials 0.000 claims 1
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- JFZUABNDWZQLIJ-UHFFFAOYSA-N methyl 2-[(2-chloroacetyl)amino]benzoate Chemical compound COC(=O)C1=CC=CC=C1NC(=O)CCl JFZUABNDWZQLIJ-UHFFFAOYSA-N 0.000 claims 1
- 150000005673 monoalkenes Chemical class 0.000 claims 1
- 229910000510 noble metal Inorganic materials 0.000 claims 1
- 150000002903 organophosphorus compounds Chemical class 0.000 claims 1
- 229910052762 osmium Inorganic materials 0.000 claims 1
- SYQBFIAQOQZEGI-UHFFFAOYSA-N osmium atom Chemical compound [Os] SYQBFIAQOQZEGI-UHFFFAOYSA-N 0.000 claims 1
- 238000007254 oxidation reaction Methods 0.000 claims 1
- 229910052760 oxygen Inorganic materials 0.000 claims 1
- 239000001301 oxygen Substances 0.000 claims 1
- 229910052763 palladium Inorganic materials 0.000 claims 1
- HVAMZGADVCBITI-UHFFFAOYSA-M pent-4-enoate Chemical compound [O-]C(=O)CCC=C HVAMZGADVCBITI-UHFFFAOYSA-M 0.000 claims 1
- 229930015698 phenylpropene Natural products 0.000 claims 1
- 229910052697 platinum Inorganic materials 0.000 claims 1
- 239000011148 porous material Substances 0.000 claims 1
- POSICDHOUBKJKP-UHFFFAOYSA-N prop-2-enoxybenzene Chemical compound C=CCOC1=CC=CC=C1 POSICDHOUBKJKP-UHFFFAOYSA-N 0.000 claims 1
- HJWLCRVIBGQPNF-UHFFFAOYSA-N prop-2-enylbenzene Chemical compound C=CCC1=CC=CC=C1 HJWLCRVIBGQPNF-UHFFFAOYSA-N 0.000 claims 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims 1
- 229910052703 rhodium Inorganic materials 0.000 claims 1
- 239000010948 rhodium Substances 0.000 claims 1
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 claims 1
- 229910052707 ruthenium Inorganic materials 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- 150000007944 thiolates Chemical class 0.000 claims 1
- 150000003573 thiols Chemical class 0.000 claims 1
- 229910052719 titanium Inorganic materials 0.000 claims 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US85973806P | 2006-11-17 | 2006-11-17 | |
| PCT/US2007/083859 WO2008063880A1 (en) | 2006-11-17 | 2007-11-07 | Hydro-oxidation process using a catalyst prepared from a gold cluster complex |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2010510048A JP2010510048A (ja) | 2010-04-02 |
| JP2010510048A5 true JP2010510048A5 (enExample) | 2010-11-11 |
Family
ID=39168720
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009537275A Pending JP2010510048A (ja) | 2006-11-17 | 2007-11-07 | 金クラスター錯体から製造された触媒を用いるヒドロ酸化法 |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US8288311B2 (enExample) |
| EP (1) | EP2086674B1 (enExample) |
| JP (1) | JP2010510048A (enExample) |
| KR (1) | KR20090083906A (enExample) |
| CN (2) | CN101534941B (enExample) |
| AT (1) | ATE527057T1 (enExample) |
| BR (1) | BRPI0716682A2 (enExample) |
| ES (1) | ES2372548T3 (enExample) |
| MX (1) | MX2009005173A (enExample) |
| MY (1) | MY145792A (enExample) |
| RU (1) | RU2445159C2 (enExample) |
| WO (1) | WO2008063880A1 (enExample) |
Families Citing this family (44)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20090250353A1 (en) * | 2006-05-26 | 2009-10-08 | Aicheng Chen | Nanoporous Material |
| JP2010222333A (ja) * | 2009-03-25 | 2010-10-07 | Hokkaido Univ | Ａｕ１３クラスタ及び金クラスタの製造方法 |
| US9441072B2 (en) * | 2009-11-06 | 2016-09-13 | The Regents Of The University Of California | Metal colloids with accessible metal surfaces |
| KR101268280B1 (ko) | 2010-12-28 | 2013-05-28 | 연세대학교 산학협력단 | 광촉매 활성을 갖는 금 클러스터 이산화티타늄 나노 복합체, 그 제조방법 및 이를 이용한 유기염료 분해방법 |
| US8617502B2 (en) | 2011-02-07 | 2013-12-31 | Cristal Usa Inc. | Ce containing, V-free mobile denox catalyst |
| EP2682206A4 (en) * | 2011-03-04 | 2014-09-17 | Toyota Motor Co Ltd | METAL PARTS, CATALYST FOR THE PURIFICATION OF PURIFICATION AND MANUFACTURING METHOD THEREFOR |
| ES2396896B1 (es) * | 2011-05-19 | 2014-01-16 | Sumitomo Chemical Company, Limited | Proceso para producir óxido de olefina. |
| HK1198960A1 (en) * | 2011-06-10 | 2015-06-19 | 因温斯特技术公司 | Improvement in metal-ligand catalyst formation |
| GB201111819D0 (en) * | 2011-07-11 | 2011-08-24 | Johnson Matthey Plc | Catalyst and method for its preparation |
| CN103781548B (zh) | 2011-08-23 | 2016-05-04 | 丰田自动车株式会社 | 排气用净化催化剂及其制造方法 |
| EP2794089A4 (en) * | 2011-12-22 | 2015-09-09 | 3M Innovative Properties Co | ETHYLENE DISTANCE MEDIUM |
| JP5943280B2 (ja) * | 2012-06-12 | 2016-07-05 | 公立大学法人首都大学東京 | 金クラスター触媒及びその製造方法 |
| US20140081040A1 (en) * | 2012-09-20 | 2014-03-20 | Lyondell Chemical Technology, L.P. | Process for pre-treatment of a catalyst support and catalyst prepared therefrom |
| US9931623B2 (en) * | 2012-11-30 | 2018-04-03 | Hiroshima University | Method for producing metal nanoparticle complex, and metal nanoparticle complex produced by said method |
| CN102962029A (zh) * | 2012-12-11 | 2013-03-13 | 常州大学 | 一种造纸废水的处理剂 |
| US20170014805A1 (en) * | 2014-04-22 | 2017-01-19 | Sabic Global Technologies B.V. | Method for the synthesis of supported gold (au) nanoparticles for epoxidation reactions |
| NL2013836B1 (en) * | 2014-11-20 | 2016-10-10 | Univ Delft Tech | Production of nanostructured materials. |
| JP6461663B2 (ja) * | 2015-03-20 | 2019-01-30 | 高知県公立大学法人 | 酸化チタン触媒およびその製造方法 |
| CN113603658A (zh) * | 2015-08-28 | 2021-11-05 | 利安德化学技术有限公司 | 环氧化工艺及其使用的催化剂 |
| US9849445B2 (en) * | 2015-09-28 | 2017-12-26 | Uchicago Argonne, Llc | Subnanometer to nanometer transition metal CO oxidation catalysts |
| AU2016363675A1 (en) * | 2015-11-30 | 2018-07-19 | Adelaide Research And Innovation | Photocatalytic conversion of carbon dioxide and water into substituted or unsubstituted hydrocarbon(s) |
| CN105344383B (zh) * | 2015-12-11 | 2018-07-20 | 中国科学院上海高等研究院 | 一种载体TiO2及其制备方法与应用 |
| CN111569936B (zh) * | 2015-12-28 | 2023-12-05 | 丰田自动车株式会社 | 簇载持催化剂及其制造方法 |
| CN106040303B (zh) * | 2016-06-30 | 2018-07-20 | 苏州大学张家港工业技术研究院 | β–二亚胺基二价稀土硼氢配合物在催化酮与硼烷硼氢化反应中的应用 |
| CN108164555B (zh) * | 2016-06-30 | 2020-05-22 | 苏州大学 | 一种硼酸酯的合成方法 |
| WO2019004318A1 (ja) * | 2017-06-27 | 2019-01-03 | トヨタ自動車株式会社 | クラスター担持多孔質担体及びその製造方法 |
| US10753247B2 (en) * | 2018-02-22 | 2020-08-25 | GM Global Technology Operations LLC | Bi-metallic oxidation catalyst materials and appurtenant devices and systems |
| KR102134767B1 (ko) * | 2018-06-01 | 2020-08-26 | 한국과학기술연구원 | Au-Pt 합금을 포함하는 촉매, 이의 제조방법 및 이를 이용한 과산화수소 합성 방법 |
| CN109399659A (zh) * | 2018-11-16 | 2019-03-01 | 华东理工大学 | 一种小尺寸金纳米颗粒负载的钛硅沸石及其制备方法 |
| CN109647506A (zh) * | 2019-02-03 | 2019-04-19 | 华东理工大学 | 一种负载型金催化剂制备方法和用途 |
| CN110465327B (zh) * | 2019-08-24 | 2022-07-15 | 中海油天津化工研究设计院有限公司 | 一种高活性重芳烃轻质化催化剂及其制备方法 |
| EP3862080B1 (en) | 2019-09-30 | 2025-02-12 | LG Chem, Ltd. | Catalyst for ammoxidation of propylene, method for preparing same, and method for ammoxidation of propylene by using same |
| WO2021066409A1 (ko) * | 2019-09-30 | 2021-04-08 | 주식회사 엘지화학 | 프로필렌의 암모산화용 촉매, 이의 제조 방법, 이를 이용한 프로필렌의 암모산화 방법 |
| JP7161614B2 (ja) | 2019-09-30 | 2022-10-26 | エルジー・ケム・リミテッド | プロピレンのアンモ酸化用触媒、その製造方法、それを用いたプロピレンのアンモ酸化方法 |
| WO2021066411A1 (ko) * | 2019-09-30 | 2021-04-08 | 주식회사 엘지화학 | 프로필렌의 암모산화용 촉매, 이의 제조 방법, 및 이를 이용한 프로필렌의 암모산화 방법 |
| KR102519507B1 (ko) | 2019-09-30 | 2023-04-07 | 주식회사 엘지화학 | 프로필렌의 암모산화용 촉매, 이의 제조 방법, 및 이를 이용한 프로필렌의 암모산화 방법 |
| CN112973681B (zh) * | 2019-12-16 | 2022-11-08 | 中国科学院大连化学物理研究所 | 一种金属纳米团簇催化剂在醇一步法制备缩醛中的应用 |
| CN111393271B (zh) * | 2020-05-06 | 2023-05-02 | 复旦大学 | 一种用于催化烃类化合物与氧气反应的协同催化氧化方法 |
| CN113912569B (zh) * | 2020-07-10 | 2024-04-26 | 中国石油化工股份有限公司 | 可降低稀释气用量的丙烯直接环氧化的方法 |
| CN111939974A (zh) * | 2020-08-20 | 2020-11-17 | 江苏博霖环保科技有限公司 | 一种净化室内甲醛的钛硅分子筛复合材料的制备方法 |
| CN114618568B (zh) * | 2020-12-09 | 2023-08-15 | 中国石油化工股份有限公司 | Ti-β分子筛在制甲烷氧化偶联反应催化剂中的应用以及镱系催化剂及其制备方法和应用 |
| CN116037202B (zh) * | 2021-10-28 | 2024-08-06 | 中国石油化工股份有限公司 | 一种co催化氧化催化剂及其制备方法和应用 |
| CN114471700A (zh) * | 2022-02-28 | 2022-05-13 | 华东理工大学 | 用于丙烯氢氧环氧化的物理混合式催化剂及制备方法和应用 |
| CN115155653B (zh) * | 2022-08-12 | 2024-12-24 | 华东理工大学 | 一种硫助剂修饰的钛硅分子筛固载金催化剂及其制备方法与应用 |
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| DE4425672A1 (de) * | 1994-07-20 | 1996-01-25 | Basf Ag | Oxidationskatalysator, Verfahren zu seiner Herstellung und Oxidationsverfahren unter Verwendung des Oxidationskatalysators |
| JP2615432B2 (ja) | 1994-10-28 | 1997-05-28 | 工業技術院長 | 金−酸化チタン含有触媒による炭化水素の部分酸化方法 |
| DE19600708A1 (de) | 1996-01-11 | 1997-07-17 | Basf Ag | Oxidationskatalysator mit einem Gehalt an Lanthanoidmetallen, Verfahren zu seiner Herstellung und Oxidationsverfahren unter Verwendung des Oxidationskatalysators |
| DE19609301C2 (de) * | 1996-03-09 | 1998-12-10 | Veba Oel Ag | Clusterbeladene Träger |
| DE19623609A1 (de) | 1996-06-13 | 1997-12-18 | Basf Ag | Oxidationskatalysator und Verfahren zur Herstellung von Epoxiden aus Olefinen, Wasserstoff und Sauerstoff unter Verwendung des Oxidationskatalysators |
| DE69708880T2 (de) | 1996-07-01 | 2002-04-11 | The Dow Chemical Co., Midland | Verfahren zur direkten oxidation von olefinen zu olefinoxiden |
| US6323351B1 (en) | 1997-06-30 | 2001-11-27 | The Dow Chemical Company | Process for the direct oxidation of olefins to olefin oxides |
| US6562986B2 (en) | 1997-06-30 | 2003-05-13 | Dow Global Technologies, Inc. | Process for the direct oxidation of olefins to olefin oxides |
| JP4016121B2 (ja) * | 1997-09-05 | 2007-12-05 | 独立行政法人産業技術総合研究所 | 炭化水素部分酸化用触媒及び含酸素有機化合物の製造方法 |
| AU3387099A (en) * | 1998-04-15 | 1999-11-01 | Dow Chemical Company, The | Process for the direct oxidation of olefins to olefin oxides |
| ES2190280T3 (es) | 1998-12-16 | 2003-07-16 | Dow Global Technologies Inc | Procedimiento para la oxidacion directa de olefinas a oxidos de olefina. |
| JP4646409B2 (ja) * | 1999-04-08 | 2011-03-09 | ダウ グローバル テクノロジーズ インコーポレイティド | 酸化された金触媒を使用してオレフィンをオレフィンオキシドにハイドロ酸化するための方法 |
| US6821923B1 (en) * | 1999-04-08 | 2004-11-23 | Dow Global Technologies Inc. | Method of preparing a catalyst containing gold and titanium |
| JP2001026422A (ja) * | 1999-05-10 | 2001-01-30 | Nippon Shokubai Co Ltd | 金含有複合体の製造方法 |
| BR0108536A (pt) * | 2000-02-22 | 2003-04-22 | Arco Chemical Techinology L P | Processo de epoxidação direta empregando composição de catalisador melhorado |
| BR0211796A (pt) * | 2001-08-01 | 2004-08-03 | Dow Global Technologies Inc | Método para aumentar a vida útil de um catalisador de hidro-oxidação |
| AU2003209327A1 (en) | 2002-01-23 | 2003-09-02 | Huntsman International Llc | Gas-phase process and catalyst for the preparation of propylene oxide |
| US7081433B2 (en) * | 2003-03-12 | 2006-07-25 | The United States Of America As Represented By The Secretary Of The Navy | Catalytic three dimensional aerogels having mesoporous nanoarchitecture |
| RU2359754C2 (ru) | 2003-09-26 | 2009-06-27 | Зм Инновейтив Пропертиз Компани | Наномерные золотые катализаторы, активаторы, твердые носители и соответствующие методики, применяемые для изготовления таких каталитических систем, особенно при осаждении золота на твердый носитель с использованием конденсации из паровой фазы |
| EP1776187A1 (en) | 2004-07-06 | 2007-04-25 | University College Cardiff Consultants, Ltd. | Supported gold catalysts |
| US7432384B2 (en) * | 2005-10-25 | 2008-10-07 | Lyondell Chemical Technology, L.P. | Direct epoxidation process |
-
2007
- 2007-11-07 MX MX2009005173A patent/MX2009005173A/es active IP Right Grant
- 2007-11-07 BR BRPI0716682-6A2A patent/BRPI0716682A2/pt not_active IP Right Cessation
- 2007-11-07 EP EP07844932A patent/EP2086674B1/en not_active Not-in-force
- 2007-11-07 CN CN200780042532XA patent/CN101534941B/zh not_active Expired - Fee Related
- 2007-11-07 ES ES07844932T patent/ES2372548T3/es active Active
- 2007-11-07 JP JP2009537275A patent/JP2010510048A/ja active Pending
- 2007-11-07 AT AT07844932T patent/ATE527057T1/de not_active IP Right Cessation
- 2007-11-07 CN CN2011101880310A patent/CN102309987A/zh active Pending
- 2007-11-07 WO PCT/US2007/083859 patent/WO2008063880A1/en not_active Ceased
- 2007-11-07 KR KR1020097010091A patent/KR20090083906A/ko not_active Ceased
- 2007-11-07 RU RU2009122732/04A patent/RU2445159C2/ru not_active IP Right Cessation
- 2007-11-07 US US12/445,547 patent/US8288311B2/en not_active Expired - Fee Related
- 2007-11-07 MY MYPI20092020A patent/MY145792A/en unknown
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