JP2007277510A - 粘着型光学フィルム、積層光学フィルムおよび画像表示装置 - Google Patents
粘着型光学フィルム、積層光学フィルムおよび画像表示装置 Download PDFInfo
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- JP2007277510A JP2007277510A JP2006217151A JP2006217151A JP2007277510A JP 2007277510 A JP2007277510 A JP 2007277510A JP 2006217151 A JP2006217151 A JP 2006217151A JP 2006217151 A JP2006217151 A JP 2006217151A JP 2007277510 A JP2007277510 A JP 2007277510A
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- optical film
- pressure
- sensitive adhesive
- film
- meth
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Abstract
【解決手段】 光学フィルムの少なくとも片面に粘着剤層を有する粘着型光学フィルムにおいて、前記粘着剤層は、モノマー成分として、複素環含有アクリルモノマー3〜10重量%、カルボキシル基含有モノマー0.5〜5重量%、ヒドロキシル基含有モノマー0.05〜2重量%、およびアルキル(メタ)アクリレート83〜96.45重量%、を含有してなり、かつ重量平均分子量が150万〜280万の(メタ)アクリル系ポリマー、ならびに架橋剤を含有してなる粘着剤により形成されている。
【選択図】 図1
Description
前記粘着剤層は、
モノマー成分として、
複素環含有アクリルモノマー3〜10重量%、
カルボキシル基含有モノマー0.5〜5重量%、
ヒドロキシル基含有モノマー0.05〜2重量%、および
アルキル(メタ)アクリレート83〜96.45重量%、を含有してなり、かつ重量平均分子量が150万〜280万の(メタ)アクリル系ポリマー、
ならびに架橋剤を含有してなる粘着剤により形成されていることを特徴とする粘着型光学フィルム、に関する。
実施例等における評価項目は下記のようにして測定を行った。
得られた(メタ)アクリル系ポリマーの重量平均分子量は、GPC(ゲル・パーミエー
ション・クロマトグラフィー)により測定した。
・分析装置:東ソー社製、HLC−8120GPC
・データ処理装置:東ソー社製、GPC−8020
・カラム:東ソー社製、G7000HXL−H+GMHXL+GMHXL
・カラムサイズ;各7.8mmφ×30cm(計90cm)
・流量:0.8ml/min
・注入試料濃度:約0.1重量%
・注入量:100μl
・カラム温度:40℃
・溶離液:テトラヒドロフラン
・検出器:示差屈折計(RI)
なお、分子量はポリスチレン換算により算出した。また、分子量10万以下の重量分率(Area%)は、GPC測定結果から上記データ処理装置で算出した。このときモノマー成分は含めなかった。
<(メタ)アクリル系ポリマーの調製>
攪拌羽根、温度計、窒素ガス導入管、冷却器を備えた4つ口フラスコに、ブチルアクリレート91部、N−アクリロイルモルホリン6部、アクリル酸2.7部、2−ヒドロキシブチルアクリレート0.3部、重合開始剤として2,2’−アゾビスイソブチロニトリル0.1重量部、酢酸エチル200重量部を仕込み、緩やかに攪拌しながら窒素ガスを導入して窒素置換した後、フラスコ内の液温を55℃付近に保って8時間重合反応を行い、アクリル系ポリマー溶液を調製した。上記アクリル系ポリマーの重量平均分子量は220万であった。
製造例1において、モノマー成分の種類および使用量、ならびに重合開始剤の使用量のいずれか少なくも一つを、表1に示すように変えたこと以外は、実施例1と同様にして、アクリル系ポリマー溶液を調製した。各例で得られたアクリル系ポリマーの重量平均分子量を表1に示す
(粘着剤層付偏光板の作製)
製造例1で得られたアクリル系ポリマー溶液の固形分100部に対して、架橋剤としてトリレンジイソシアネートのトリメチロールプロパン付加物からなるポリイソシアネート系架橋剤(日本ポリウレタン工業社製、コロネートL)0.2部を配合したアクリル系粘着剤溶液を調製した。
実施例1において、アクリル系粘着剤溶液の調製に用いたアクリル系ポリマー溶液の種類、架橋剤の配合量、乾燥後の粘着剤層の厚さを表2に示すように変えたこと以外は、実施例1と同様にして、粘着剤層付偏光板(A1)を作製した。
実施例1において、偏光板の代わりに、位相差板(JSR社製,ノルボルネン系フィルム、製品名アートン)を用いたこと以外は、実施例1と同様にして粘着剤層付位相差板(A3)を作製した。得られた粘着剤層付位相差板(A3)の位相差板側に、実施例1で得られた粘着剤層付偏光板(A1)を貼り合せて、偏光板/粘着剤層/位相差板/粘着剤層の構成の粘着剤層付きの積層光学フィルムを作製した。
実施例1において、アクリル系粘着剤溶液の調製に用いたアクリル系ポリマー溶液の種類、架橋剤の配合量を表2に示すように変えたこと、偏光板の代わりに、位相差板(JSR社製,ノルボルネン系フィルム、製品名アートン)を用いたこと以外は、実施例1と同様にして粘着剤層付位相差板(A3)を作製した。得られた粘着剤層付位相差板(A3)の位相差板側に、実施例1で得られた粘着剤層付偏光板(A1)を貼り合せて、偏光板/粘着剤層/位相差板/粘着剤層の構成の粘着剤層付きの積層光学フィルムを作製した。
(サンプルの作製)
攪拌羽根、温度計、窒素ガス導入管、冷却器を備えた4つ口フラスコに、ブチルアクリレート100部、アクリル酸5部、2−ヒドロキシブチルアクリレート0.1部、重合開始剤として2,2’−アゾビスイソブチロニトリル0.1重量部、酢酸エチル200重量部を仕込み、緩やかに攪拌しながら窒素ガスを導入して窒素置換した後、フラスコ内の液温を55℃付近に保って8時間重合反応を行い、アクリル系ポリマー溶液を調製した。上記アクリル系ポリマーの重量平均分子量は192万であった。得られたアクリル系ポリマー溶液の固形分100部に対して、架橋剤としてトリレンジイソシアネートのトリメチロールプロパン付加物からなるポリイソシアネート系架橋剤(日本ポリウレタン工業社製、コロネートL)0.6重量部を配合したアクリル系粘着剤溶液を調製した。これを、アクリル系粘着剤溶液Aとする。
上記サンプル1、2を5インチサイズに裁断し、0.5mmの無アクリルガラス(コーニング社製、1737)に貼り付けた後、50℃、0.5Mpaのオートクレーブにて15分間処理した後、次いで90℃の雰囲気下で500時間保存してから、室温(約25℃)に戻した。
上記サンプル1、2を5インチサイズに裁断し、0.5mmの無アクリルガラス(コーニング社製、1737)に貼り付けた後、50℃、0.5Mpaのオートクレーブにて15分間処理した後、次いで60℃、95%RHの雰囲気下で500時間保存してから、室温(約25℃)に戻した。
○:剥がれや浮き、発泡なし。
×:剥がれや浮き、発泡あり。
上記実施例および比較例で得られた、粘着剤層付偏光板(A1)または粘着剤層付きの積層光学フィルムを、位相差板(JSR社製,ノルボルネン系フィルム、製品名アートン)に貼り合せた後、25mm×150mmに裁断し、引張り試験機にて、剥離角度90°、剥離速度300mm/minで粘着力を測定した。
耐久性の評価にあたり、粘着剤層付偏光板(A1)または粘着剤層付きの積層光学フィルムを、粘着剤層付位相差板(A2)に貼り合せたときの状態を目視により、下記基準で行った。
○:かみこみ気泡等が発生せず、きちんと貼り合せができた場合。
×:気泡等がかみこんで、貼り合せが困難な場合。
厚さ48μmのノルボルネン系フィルム(JSR社製,製品名アートン)を、150℃で1.71倍に横延伸した。得られた位相差板1は、厚さ28μm、面内位相差140nm、Nz係数1.55であった。
厚さ60μmのノルボルネン系フィルム(日本ゼオン社製,製品名ゼオノア)を、140℃で1.28倍に一軸延伸した。得られた位相差板2は、厚さ35μm、面内位相差130nm、Nz係数1.0であった。
下記化1:
(粘着剤層付偏光板の作製)
製造例1で得られたアクリル系ポリマー溶液の固形分100部に対して、架橋剤としてトリレンジイソシアネートのトリメチロールプロパン付加物からなるポリイソシアネート系架橋剤(日本ポリウレタン工業社製、コロネートL)0.5部を配合したアクリル系粘着剤溶液を調製した。
次いで、上記耐久性の評価で調製した、アクリル系粘着剤溶液Aを、シリコーン処理を施したポリエチレンテレフタレート(PET)フィルム(三菱化学ポリエステルフィルム社製、厚さ:38μm)の片面に、乾燥後の粘着剤層の厚さが25μmになるように塗布し、130℃で3分間乾燥を行い、粘着剤層を形成した。当該粘着剤層を位相差板1に転写し、粘着剤層付位相差板(A3-1)を作製した。得られた粘着剤層付位相差板(A3-1)の位相差板1の側に、上記粘着剤層付偏光板(A1-1)を貼り合せて、偏光板/粘着剤層/位相差板1/粘着剤層の構成の粘着剤層付きの積層光学フィルム(構成2‐1)を作製した。
実施例18において、位相差板1の代わりに、位相差板3を用いたこと以外は、実施例18と同様にして、偏光板/粘着剤層/位相差板3/粘着剤層の構成の粘着剤層付きの積層光学フィルム(構成2‐2)を作製した。なお、位相差板3の液晶層側にアクリル系粘着剤溶液Aにより厚さ25μmの粘着剤層を形成した。
実施例18において、アクリル系粘着剤溶液の調製に用いたアクリル系ポリマー溶液の種類、偏光板に積層した乾燥後の粘着剤層の厚さ、積層光学フィルムの構成を表3に示すように変えたこと以外は、実施例18と同様にして、粘着剤層付きの積層光学フィルムを作製した。
上記粘着剤層付きの積層光学フィルムを40mm×30mmに裁断し、0.5mmの無アクリルガラス(コーニング社製、1737)に貼り付けた後、サンプル中央部の位相差(測定波長550nm)を測定した。位相差の測定は、大塚電子社製のRETS‐1200VAにて測定した。前記ガラスに貼り合わせたサンプルを90℃で500時間保存してから、室温(約25℃)に戻した後、再度位相差を測定した。位相差変化が、初期値と比べて、2nm以下であれば「○」、2nmを超えれば「×」とした。
1 光学フィルム
11 偏光板
12、13 位相差板
2(21、22、23) 粘着剤層
G ガラス基板
Claims (11)
- 光学フィルムの少なくとも片面に粘着剤層を有する粘着型光学フィルムにおいて、
前記粘着剤層は、
モノマー成分として、
複素環含有アクリルモノマー3〜10重量%、
カルボキシル基含有モノマー0.5〜5重量%、
ヒドロキシル基含有モノマー0.05〜2重量%、および
アルキル(メタ)アクリレート83〜96.45重量%、を含有してなり、かつ重量平均分子量が150万〜280万の(メタ)アクリル系ポリマー、
ならびに架橋剤を含有してなる粘着剤により形成されていることを特徴とする粘着型光学フィルム。 - 複素環含有アクリルモノマーが、複素環として、モルホリン環、ピペリジン環またはピロリジン環を有することを特徴とする請求項1記載の粘着型光学フィルム。
- カルボキシル基含有モノマーが、アクリル酸であることを特徴とする請求項1または2記載の粘着型光学フィルム。
- ヒドロキシ基含有モノマーが、ヒドロキシアルキル(メタ)アクリレートであることを特徴とする請求項1〜3のいずれかに記載の粘着型光学フィルム。
- 架橋剤が、イソシアネート系架橋剤であることを特徴とする請求項1〜4のいずれかに記載の粘着型光学フィルム。
- 架橋剤の使用量が、(メタ)アクリル系ポリマー100重量部に対して、0.02〜2重量部であることを請求項1〜5のいずれかに記載の粘着型光学フィルム。
- 粘着剤層の厚さが1〜15μmであることを特徴とする請求項1〜6のいずれかに記載の粘着型光学フィルム。
- 光学フィルムが偏光板または位相差板であることを特徴とする請求項1〜7のいずれかに記載の粘着型光学フィルム。
- 請求項1〜8のいずれかに記載の粘着型光学フィルムが、当該粘着型光学フィルムの粘着剤層を介して、他の光学フィルムに積層されていることを特徴とする積層光学フィルム。
- 請求項1〜8のいずれかに記載の粘着型光学フィルムが粘着型偏光板であり、他の光学フィルムが位相差板であることを特徴とする請求項9記載の積層光学フィルム。
- 請求項1〜8のいずれかに記載の粘着型光学フィルムまたは請求項9もしくは10記載の積層光学フィルムを少なくとも1枚用いた画像表示装置。
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- 2007-03-13 CN CN2007800079844A patent/CN101395508B/zh active Active
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US20090087650A1 (en) | 2009-04-02 |
EP2006715A9 (en) | 2009-07-22 |
EP2006715A2 (en) | 2008-12-24 |
EP2006715B1 (en) | 2014-09-10 |
CN101395508A (zh) | 2009-03-25 |
TW200801603A (en) | 2008-01-01 |
EP2006715A4 (en) | 2013-04-17 |
KR101010889B1 (ko) | 2011-01-25 |
KR20080091256A (ko) | 2008-10-09 |
CN101395508B (zh) | 2010-07-21 |
JP4140736B2 (ja) | 2008-08-27 |
WO2007108363A1 (ja) | 2007-09-27 |
TWI349118B (ja) | 2011-09-21 |
US8932710B2 (en) | 2015-01-13 |
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