JP2006507337A - 結晶形態のフェノール系抗酸化剤 - Google Patents

結晶形態のフェノール系抗酸化剤 Download PDF

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Publication number
JP2006507337A
JP2006507337A JP2004554535A JP2004554535A JP2006507337A JP 2006507337 A JP2006507337 A JP 2006507337A JP 2004554535 A JP2004554535 A JP 2004554535A JP 2004554535 A JP2004554535 A JP 2004554535A JP 2006507337 A JP2006507337 A JP 2006507337A
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JP
Japan
Prior art keywords
strength
medium
butyl
tert
low strength
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Pending
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JP2004554535A
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Japanese (ja)
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JP2006507337A5 (https=
Inventor
レーム，ダニエル
スカフター，ヨハネス
デル スカッフ，ポール エイドリアン バン
グッケル，クリスチャン
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BASF Schweiz AG
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Ciba Spezialitaetenchemie Holding AG
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Publication date
Application filed by Ciba Spezialitaetenchemie Holding AG filed Critical Ciba Spezialitaetenchemie Holding AG
Publication of JP2006507337A publication Critical patent/JP2006507337A/ja
Publication of JP2006507337A5 publication Critical patent/JP2006507337A5/ja
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/22—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/22—Separation; Purification; Stabilisation; Use of additives
    • C07C231/24—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/66—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety
    • C07C69/73—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of unsaturated acids
    • C07C69/732—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of unsaturated acids of unsaturated hydroxy carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/13—Phenols; Phenolates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/16—Nitrogen-containing compounds
    • C08K5/20—Carboxylic acid amides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/002—Physical properties
    • C08K2201/005—Additives being defined by their particle size in general

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Anti-Oxidant Or Stabilizer Compositions (AREA)
JP2004554535A 2002-11-26 2003-11-17 結晶形態のフェノール系抗酸化剤 Pending JP2006507337A (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP02406023 2002-11-26
PCT/EP2003/050838 WO2004048312A1 (en) 2002-11-26 2003-11-17 Phenolic antioxidants in crystalline form

Publications (2)

Publication Number Publication Date
JP2006507337A true JP2006507337A (ja) 2006-03-02
JP2006507337A5 JP2006507337A5 (https=) 2007-01-11

Family

ID=32338231

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2004554535A Pending JP2006507337A (ja) 2002-11-26 2003-11-17 結晶形態のフェノール系抗酸化剤

Country Status (11)

Country Link
US (1) US7262319B2 (https=)
EP (1) EP1575895A1 (https=)
JP (1) JP2006507337A (https=)
KR (1) KR20050085019A (https=)
CN (1) CN100448838C (https=)
AU (1) AU2003300566B2 (https=)
BR (1) BR0316567A (https=)
MY (1) MY136146A (https=)
RU (1) RU2362764C2 (https=)
TW (1) TWI308145B (https=)
WO (1) WO2004048312A1 (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010285380A (ja) * 2009-06-12 2010-12-24 Sumitomo Chemical Co Ltd 粒状物質の製造方法

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008507613A (ja) * 2004-07-23 2008-03-13 ポルノクス コーポレーション 抗酸化マクロモノマーおよび抗酸化ポリマー、ならびにその作製方法および使用方法
US7498457B2 (en) * 2004-07-27 2009-03-03 Ciba Specialty Chemicals Corp. Process for preparing solid particles of phenolic antioxidants
WO2006060800A1 (en) 2004-12-03 2006-06-08 Polnox Corporation Synthesis of aniline and phenol-based antioxidant macromonomers and corresponding polymers
EP1861484A2 (en) 2005-02-22 2007-12-05 Polnox Corporation Nitrogen and hindered phenol containing dual functional macromolecular antioxidants: synthesis , performances and applications
CA2606303A1 (en) 2005-03-25 2006-10-05 Polnox Corporation Alkylated and polymeric macromolecular antioxidants and methods of making and using the same
WO2007050985A2 (en) 2005-10-27 2007-05-03 Polnox Corporation Macromolecular antioxidants based on stξrically hindered phenolic phosphites
EP1966293A1 (en) 2005-10-27 2008-09-10 Polnox Corporation Stabilized polyolefin compositions
US20070161522A1 (en) 2005-12-02 2007-07-12 Cholli Ashok L Lubricant oil compositions
WO2008005358A2 (en) 2006-07-06 2008-01-10 Polnox Corporation Novel macromolecular antioxidants comprising differing antioxidant moieties: structures, methods of making and using the same
US7767853B2 (en) 2006-10-20 2010-08-03 Polnox Corporation Antioxidants and methods of making and using the same
WO2008055832A2 (en) * 2006-11-09 2008-05-15 Ciba Holding Inc. Process using liquid phenolic antioxidants
KR101211231B1 (ko) * 2008-08-21 2012-12-11 주식회사 엘지화학 산화방지제 유성 분산액과 이의 제조방법 및 이로부터 제조된 염화비닐계 수지 중합체
WO2012125686A1 (en) * 2011-03-14 2012-09-20 Dow Global Technologies Llc Ethylene-based compositions
JP5542289B2 (ja) * 2012-01-23 2014-07-09 トヨタ自動車株式会社 オイル添加物およびオイルフィルター
WO2015077635A2 (en) 2013-11-22 2015-05-28 Polnox Corporation Macromolecular antioxidants based on dual type moiety per molecule: structures methods of making and using the same
US20180251695A1 (en) 2017-03-01 2018-09-06 Polnox Corporation Macromolecular Corrosion (McIn) Inhibitors: Structures, Methods Of Making And Using The Same
WO2018189016A1 (en) 2017-04-10 2018-10-18 Basf Se Low volatile organic anti-oxidation stabilisers for polymeric systems, their production and use
CN107417528A (zh) * 2017-05-02 2017-12-01 沈阳化工大学 一种抗氧剂1076在甲醇溶剂中得到针状晶形结晶的方法
CN111495312B (zh) * 2020-05-22 2023-07-28 河南心连心化学工业集团股份有限公司 一种草酰胺合成装置以及合成方法
KR102771644B1 (ko) * 2022-06-21 2025-02-26 금호석유화학 주식회사 산화방지제의 제조방법

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JPS5974182A (ja) * 1982-10-20 1984-04-26 Sumitomo Chem Co Ltd 複合酸化防止剤の球状製品の製造法
JPS6013017B2 (ja) * 1980-01-14 1985-04-04 三井化学株式会社 テトラキス〔３−（３，５−ジ−ｔ−ブチル−４−ヒドロキシフエニル）プロピオニルオキシメチル〕メタンの製造方法
JPS6013018B2 (ja) * 1980-04-01 1985-04-04 三井化学株式会社 新規な結晶構造を有するテトラキス〔３−（３，５−ジ−ｔ−ブチル−４−ヒドロキシフエニル）プロピオニルオキシメチル〕メタン
JPS6063274A (ja) * 1983-09-16 1985-04-11 Mitsui Toatsu Chem Inc 酸化防止剤分散液
JPS60186547A (ja) * 1984-03-07 1985-09-24 Mitsui Toatsu Chem Inc 酸化防止剤分散液
JPS61261333A (ja) * 1985-05-02 1986-11-19 チバ−ガイギ−　アクチエンゲゼルシヤフト 球状に重合されたポリオレフィンの安定化方法
JPS6222745A (ja) * 1985-07-19 1987-01-30 チバ−ガイギ−　アクチエンゲゼルシヤフト ペンタエリトリトールテトラキス―〔３―（３，５―ジー第三ブチル―４―ヒドロキシフェニル）プロピオネート〕の完全無溶媒結晶化方法
JPS62258343A (ja) * 1986-04-30 1987-11-10 Musashino Geigy Kk 独立粒子状β晶テトラキス〔３−（３，５−ジ−ｔ−ブチル−４−ヒドロキシフエニル）プロピオニルオキシメチル〕メタンおよびその製造方法
JPS63159315A (ja) * 1986-12-22 1988-07-02 Yuutoku Yakuhin Kogyo Kk パツプ剤
WO1989009202A1 (fr) * 1988-03-31 1989-10-05 Yoshitomi Pharmaceutical Industries, Ltd. PROCEDE DE CRISTALLISATION ET DE PURIFICATION PERMETTANT D'OBTENIR DES beta CRISTAUX STABLES DE TETRAKIS[3-(3,5-DI-BUTYLE TERTIAIRE-4-HYDROXYPHENYL)PROPIONYLOXYMETHYL]METHANE A L'ECHELLE INDUSTRIELLE
JPH0249752A (ja) * 1988-03-31 1990-02-20 Yoshitomi Pharmaceut Ind Ltd テトラキス〔３―（３，５―ジ第３級ブチル―４―ヒドロキシフェニル）プロピオニルオキシメチル〕メタンのβ晶の晶出精製方法
JPH0311038A (ja) * 1989-06-08 1991-01-18 Yoshitomi Pharmaceut Ind Ltd 粉体特性の優れたα晶テトラキス〔３―（３，５―ジ―ｔ―ブチル―４―ヒドロキシフェニル）プロピオニルオキシメチル〕メタンの製造法
JPH0311037A (ja) * 1989-06-08 1991-01-18 Yoshitomi Pharmaceut Ind Ltd 流動性の優れたα晶テトラキス〔３―（３，５―ジ―ｔ―ブチル―４―ヒドロキシフェニル）プロピオニルオキシメチル〕メタンおよびその製造方法
JPH0381390A (ja) * 1989-08-25 1991-04-05 Adeka Argus Chem Co Ltd ラテックス用酸化防止剤分散液
JPH03146563A (ja) * 1989-11-01 1991-06-21 Adeka Argus Chem Co Ltd ラテックス用酸化防止剤分散液
JPH04506979A (ja) * 1989-08-11 1992-12-03 イーストマン ケミカル カンパニー 水系媒体中に分散可能な固形添加剤系、その製造方法及びポリマー粒子へのその適用
JPH05271516A (ja) * 1992-03-26 1993-10-19 Polyplastics Co ポリオキシメチレン組成物
JPH0625430A (ja) * 1992-07-09 1994-02-01 Yoshitomi Pharmaceut Ind Ltd 有機材料の安定化処理法
JPH0641348A (ja) * 1992-03-31 1994-02-15 Union Carbide Chem & Plast Technol Corp 脂肪酸エステル中のポリマー添加剤の分散体
JPH06128195A (ja) * 1992-10-15 1994-05-10 Asahi Denka Kogyo Kk テトラキス〔３−（３，５−ジ第三ブチル−４−ヒドロキシフェニル）プロピオニルオキシメチル〕メタンの製造方法
JPH07173369A (ja) * 1991-02-04 1995-07-11 Polyplastics Co ポリアセタール樹脂着色組成物
JPH0931464A (ja) * 1995-06-26 1997-02-04 Hoechst Ag 自己発火温度の高い分散性粉末
JP2001504758A (ja) * 1996-11-26 2001-04-10 ゼネカ リミテッド 結晶化方法
JP2001526711A (ja) * 1997-04-15 2001-12-18 チバ スペシャルティ ケミカルズ ホールディング インコーポレーテッド 低粉塵性安定剤の製造方法

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JPS6013017B2 (ja) * 1980-01-14 1985-04-04 三井化学株式会社 テトラキス〔３−（３，５−ジ−ｔ−ブチル−４−ヒドロキシフエニル）プロピオニルオキシメチル〕メタンの製造方法
JPS6013018B2 (ja) * 1980-04-01 1985-04-04 三井化学株式会社 新規な結晶構造を有するテトラキス〔３−（３，５−ジ−ｔ−ブチル−４−ヒドロキシフエニル）プロピオニルオキシメチル〕メタン
JPS5974182A (ja) * 1982-10-20 1984-04-26 Sumitomo Chem Co Ltd 複合酸化防止剤の球状製品の製造法
JPS6063274A (ja) * 1983-09-16 1985-04-11 Mitsui Toatsu Chem Inc 酸化防止剤分散液
JPS60186547A (ja) * 1984-03-07 1985-09-24 Mitsui Toatsu Chem Inc 酸化防止剤分散液
JPS61261333A (ja) * 1985-05-02 1986-11-19 チバ−ガイギ−　アクチエンゲゼルシヤフト 球状に重合されたポリオレフィンの安定化方法
JPS6222745A (ja) * 1985-07-19 1987-01-30 チバ−ガイギ−　アクチエンゲゼルシヤフト ペンタエリトリトールテトラキス―〔３―（３，５―ジー第三ブチル―４―ヒドロキシフェニル）プロピオネート〕の完全無溶媒結晶化方法
JPH0867654A (ja) * 1985-07-19 1996-03-12 Ciba Geigy Ag ペンタエリトリトール テトラキス−〔３−（３，５−ジ−第三ブチル−４−ヒドロキシフェニル）プロピオネート〕の新規λ−変性結晶及びその製造方法
JPS62258343A (ja) * 1986-04-30 1987-11-10 Musashino Geigy Kk 独立粒子状β晶テトラキス〔３−（３，５−ジ−ｔ−ブチル−４−ヒドロキシフエニル）プロピオニルオキシメチル〕メタンおよびその製造方法
JPS63159315A (ja) * 1986-12-22 1988-07-02 Yuutoku Yakuhin Kogyo Kk パツプ剤
WO1989009202A1 (fr) * 1988-03-31 1989-10-05 Yoshitomi Pharmaceutical Industries, Ltd. PROCEDE DE CRISTALLISATION ET DE PURIFICATION PERMETTANT D'OBTENIR DES beta CRISTAUX STABLES DE TETRAKIS[3-(3,5-DI-BUTYLE TERTIAIRE-4-HYDROXYPHENYL)PROPIONYLOXYMETHYL]METHANE A L'ECHELLE INDUSTRIELLE
JPH0249752A (ja) * 1988-03-31 1990-02-20 Yoshitomi Pharmaceut Ind Ltd テトラキス〔３―（３，５―ジ第３級ブチル―４―ヒドロキシフェニル）プロピオニルオキシメチル〕メタンのβ晶の晶出精製方法
JPH0311037A (ja) * 1989-06-08 1991-01-18 Yoshitomi Pharmaceut Ind Ltd 流動性の優れたα晶テトラキス〔３―（３，５―ジ―ｔ―ブチル―４―ヒドロキシフェニル）プロピオニルオキシメチル〕メタンおよびその製造方法
JPH0311038A (ja) * 1989-06-08 1991-01-18 Yoshitomi Pharmaceut Ind Ltd 粉体特性の優れたα晶テトラキス〔３―（３，５―ジ―ｔ―ブチル―４―ヒドロキシフェニル）プロピオニルオキシメチル〕メタンの製造法
JPH04506979A (ja) * 1989-08-11 1992-12-03 イーストマン ケミカル カンパニー 水系媒体中に分散可能な固形添加剤系、その製造方法及びポリマー粒子へのその適用
JPH0381390A (ja) * 1989-08-25 1991-04-05 Adeka Argus Chem Co Ltd ラテックス用酸化防止剤分散液
JPH03146563A (ja) * 1989-11-01 1991-06-21 Adeka Argus Chem Co Ltd ラテックス用酸化防止剤分散液
JPH07173369A (ja) * 1991-02-04 1995-07-11 Polyplastics Co ポリアセタール樹脂着色組成物
JPH05271516A (ja) * 1992-03-26 1993-10-19 Polyplastics Co ポリオキシメチレン組成物
JPH0641348A (ja) * 1992-03-31 1994-02-15 Union Carbide Chem & Plast Technol Corp 脂肪酸エステル中のポリマー添加剤の分散体
JPH0625430A (ja) * 1992-07-09 1994-02-01 Yoshitomi Pharmaceut Ind Ltd 有機材料の安定化処理法
JPH06128195A (ja) * 1992-10-15 1994-05-10 Asahi Denka Kogyo Kk テトラキス〔３−（３，５−ジ第三ブチル−４−ヒドロキシフェニル）プロピオニルオキシメチル〕メタンの製造方法
JPH0931464A (ja) * 1995-06-26 1997-02-04 Hoechst Ag 自己発火温度の高い分散性粉末
JP2001504758A (ja) * 1996-11-26 2001-04-10 ゼネカ リミテッド 結晶化方法
JP2001526711A (ja) * 1997-04-15 2001-12-18 チバ スペシャルティ ケミカルズ ホールディング インコーポレーテッド 低粉塵性安定剤の製造方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010285380A (ja) * 2009-06-12 2010-12-24 Sumitomo Chemical Co Ltd 粒状物質の製造方法

Also Published As

Publication number Publication date
US20060189820A1 (en) 2006-08-24
RU2362764C2 (ru) 2009-07-27
TW200415234A (en) 2004-08-16
AU2003300566B2 (en) 2010-01-21
US7262319B2 (en) 2007-08-28
RU2005120164A (ru) 2006-04-27
AU2003300566A1 (en) 2004-06-18
EP1575895A1 (en) 2005-09-21
TWI308145B (en) 2009-04-01
CN1717385A (zh) 2006-01-04
CN100448838C (zh) 2009-01-07
KR20050085019A (ko) 2005-08-29
BR0316567A (pt) 2005-10-04
MY136146A (en) 2008-08-29
WO2004048312A1 (en) 2004-06-10

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