JP2005510346A5 - - Google Patents
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- Publication number
- JP2005510346A5 JP2005510346A5 JP2003547049A JP2003547049A JP2005510346A5 JP 2005510346 A5 JP2005510346 A5 JP 2005510346A5 JP 2003547049 A JP2003547049 A JP 2003547049A JP 2003547049 A JP2003547049 A JP 2003547049A JP 2005510346 A5 JP2005510346 A5 JP 2005510346A5
- Authority
- JP
- Japan
- Prior art keywords
- nickel chloride
- method described
- alkyl
- bidentate
- reducing metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 claims description 23
- 229910021586 Nickel(II) chloride Inorganic materials 0.000 claims description 21
- QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 claims description 21
- 239000002184 metal Substances 0.000 claims description 9
- 229910052751 metal Inorganic materials 0.000 claims description 9
- 239000003054 catalyst Substances 0.000 claims description 7
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 4
- 238000005669 hydrocyanation reaction Methods 0.000 claims description 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 3
- 239000003446 ligand Substances 0.000 claims description 3
- 229910052698 phosphorus Inorganic materials 0.000 claims description 3
- 239000011574 phosphorus Substances 0.000 claims description 3
- 229910052759 nickel Inorganic materials 0.000 claims description 2
- 150000002825 nitriles Chemical class 0.000 claims description 2
- 150000003003 phosphines Chemical class 0.000 claims description 2
- 125000005538 phosphinite group Chemical group 0.000 claims description 2
- AQSJGOWTSHOLKH-UHFFFAOYSA-N phosphite(3-) Chemical class [O-]P([O-])[O-] AQSJGOWTSHOLKH-UHFFFAOYSA-N 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 description 13
- 229910052739 hydrogen Inorganic materials 0.000 description 12
- 229910052799 carbon Inorganic materials 0.000 description 10
- 125000004642 (C1-C12) alkoxy group Chemical group 0.000 description 9
- 238000001694 spray drying Methods 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 2
- 229910002091 carbon monoxide Inorganic materials 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- 125000004400 (C1-C12) alkyl group Chemical group 0.000 description 1
- 125000004178 (C1-C4) alkyl group Chemical group 0.000 description 1
- 125000003545 alkoxy group Chemical group 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 150000004683 dihydrates Chemical class 0.000 description 1
- 229910052733 gallium Inorganic materials 0.000 description 1
- 229910052738 indium Inorganic materials 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 125000001624 naphthyl group Chemical group 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 229910052712 strontium Inorganic materials 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 229910052720 vanadium Inorganic materials 0.000 description 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/994,102 US6893996B2 (en) | 2001-11-26 | 2001-11-26 | Process for the preparation of a nickel/phosphorous ligand catalyst for olefin hydrocyanation |
| PCT/US2002/036468 WO2003045555A2 (en) | 2001-11-26 | 2002-11-14 | Process for the preparation of a nickel/phosphorus ligand catalyst for olefin hydrocyanation |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008284604A Division JP2009035482A (ja) | 2001-11-26 | 2008-11-05 | オレフィンヒドロシアン化用のニッケル／リン配位子触媒の調製方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2005510346A JP2005510346A (ja) | 2005-04-21 |
| JP2005510346A5 true JP2005510346A5 (enExample) | 2006-01-05 |
Family
ID=25540279
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2003547049A Pending JP2005510346A (ja) | 2001-11-26 | 2002-11-14 | オレフィンヒドロシアン化用のニッケル／リン配位子触媒の調製方法 |
| JP2008284604A Pending JP2009035482A (ja) | 2001-11-26 | 2008-11-05 | オレフィンヒドロシアン化用のニッケル／リン配位子触媒の調製方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008284604A Pending JP2009035482A (ja) | 2001-11-26 | 2008-11-05 | オレフィンヒドロシアン化用のニッケル／リン配位子触媒の調製方法 |
Country Status (17)
| Country | Link |
|---|---|
| US (1) | US6893996B2 (enExample) |
| EP (2) | EP1604954A1 (enExample) |
| JP (2) | JP2005510346A (enExample) |
| KR (2) | KR100912331B1 (enExample) |
| CN (2) | CN100445210C (enExample) |
| AT (1) | ATE307669T1 (enExample) |
| AU (1) | AU2002356942A1 (enExample) |
| BR (1) | BR0214260B1 (enExample) |
| CA (1) | CA2468293A1 (enExample) |
| DE (1) | DE60206958T2 (enExample) |
| ES (1) | ES2250748T3 (enExample) |
| MX (1) | MXPA04004942A (enExample) |
| MY (1) | MY129876A (enExample) |
| PL (1) | PL371463A1 (enExample) |
| RU (1) | RU2301704C2 (enExample) |
| TW (1) | TW592817B (enExample) |
| WO (1) | WO2003045555A2 (enExample) |
Families Citing this family (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20030100803A1 (en) * | 2001-11-26 | 2003-05-29 | Lu Helen S.M. | 3-Alkylated-5,5',6,6',7,7,'8,8'-octahydro-2,2'-binaphthols and 3,3'-dialkylated-5,5',6,6',7,7',8,8'-octahydro-2,2'-binaphthols and processes for making them |
| FR2849027B1 (fr) * | 2002-12-23 | 2005-01-21 | Rhodia Polyamide Intermediates | Procede de synthese de composes comprenant des fonctions nitriles a partir de composes a insaturations ethyleniques |
| US6897329B2 (en) * | 2003-01-14 | 2005-05-24 | Invista North America S.A.R.L. | Process for the preparation of nickel/phosphorous ligand catalyst for olefin hydrocyanation |
| FR2850966B1 (fr) | 2003-02-10 | 2005-03-18 | Rhodia Polyamide Intermediates | Procede de fabrication de composes dinitriles |
| FR2854892B1 (fr) * | 2003-05-12 | 2005-06-24 | Rhodia Polyamide Intermediates | Procede de fabrication de dinitriles |
| FR2854891B1 (fr) | 2003-05-12 | 2006-07-07 | Rhodia Polyamide Intermediates | Procede de preparation de dinitriles |
| DE10351000A1 (de) * | 2003-10-30 | 2005-06-09 | Basf Ag | Verfahren zur Herstellung von Nickel(O)-Phosphorligand-Komplexen |
| DE10351003A1 (de) * | 2003-10-30 | 2005-05-25 | Basf Ag | Verfahren zur Herstellung von Nickel-Phosphorligand-Komplexen |
| DE10351002A1 (de) * | 2003-10-30 | 2005-05-25 | Basf Ag | Einsatz von azeotrop-getrockneten Nickel(II)-halogeniden |
| DE102004004718A1 (de) * | 2004-01-29 | 2005-08-18 | Basf Ag | Verfahren zur Hydrocyanierung |
| EP1825914A1 (de) * | 2006-02-22 | 2007-08-29 | Basf Aktiengesellschaft | Verbessertes Verfahren zur Herstellung von Nickel(0)-Phophorligand-Komplexen |
| WO2007109005A2 (en) * | 2006-03-17 | 2007-09-27 | Invista Technologies S.A R.L. | Method for the purification of triorganophosphites by treatment with a basic additive |
| US7709673B2 (en) * | 2006-07-14 | 2010-05-04 | Invista North America S.A R.L. | Process for making 3-pentenenitrile by hydrocyanation of butadiene |
| US7709674B2 (en) * | 2006-07-14 | 2010-05-04 | Invista North America S.A R.L | Hydrocyanation process with reduced yield losses |
| US7659422B2 (en) * | 2006-07-14 | 2010-02-09 | Invista North America S.A.R.L. | Hydrocyanation process with reduced yield losses |
| US7880028B2 (en) * | 2006-07-14 | 2011-02-01 | Invista North America S.A R.L. | Process for making 3-pentenenitrile by hydrocyanation of butadiene |
| US7919646B2 (en) | 2006-07-14 | 2011-04-05 | Invista North America S.A R.L. | Hydrocyanation of 2-pentenenitrile |
| JP5295512B2 (ja) * | 2007-03-29 | 2013-09-18 | 三井化学株式会社 | ゼロ価ニッケルの有機ホスフィン錯体の製造方法 |
| EP2229354B1 (en) * | 2008-01-15 | 2013-03-20 | Invista Technologies S.à.r.l. | Process for making and refining 3-pentenenitrile, and for refining 2-methyl-3-butenenitrile |
| EP2229353B1 (en) * | 2008-01-15 | 2018-01-03 | INVISTA Textiles (U.K.) Limited | Hydrocyanation of pentenenitriles |
| WO2011075496A1 (en) | 2009-12-18 | 2011-06-23 | Invista Technologies S.A.R.L. | Nickel compositions for preparing nickel metal and nickel complexes |
| ES2542430T3 (es) | 2010-07-07 | 2015-08-05 | Invista Technologies S.À.R.L. | Proceso para hacer nitrilos |
| CN103080119B (zh) | 2010-09-07 | 2015-04-08 | 因温斯特技术公司 | 用于制备镍金属的镍组合物和镍配合物 |
| HK1198960A1 (en) * | 2011-06-10 | 2015-06-19 | 因温斯特技术公司 | Improvement in metal-ligand catalyst formation |
| JP2014530221A (ja) | 2011-10-07 | 2014-11-17 | インヴィスタテクノロジーズ エスアエルエル | ニトリルの作製方法 |
| US10759741B2 (en) | 2013-07-17 | 2020-09-01 | Invista North America S.A R.L. | Separating a solvent from a nickel catalyst by distillation |
| KR102048134B1 (ko) | 2016-01-21 | 2019-11-22 | 제이엑스금속주식회사 | 무수 염화 니켈 및 그 제조 방법 |
| CN114212836A (zh) * | 2021-12-31 | 2022-03-22 | 金川集团镍盐有限公司 | 一种无水氯化镍粉体材料的制备方法 |
| CN114835176A (zh) * | 2022-05-30 | 2022-08-02 | 金川集团镍盐有限公司 | 一种球形无水氯化镍产品的制备方法 |
| JP2024097610A (ja) * | 2023-01-06 | 2024-07-19 | レアメタルリサイクル環境合同会社 | 無水塩化ニッケル粉末の製造方法 |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3631191A (en) | 1970-04-08 | 1971-12-28 | Du Pont | Synthesis of zero valent nickel-tetrakis triaryl phosphite complexes |
| US3846461A (en) | 1972-10-25 | 1974-11-05 | Du Pont | Process of preparing a zerovalent nickel complex with organic phosphorus compounds |
| US3847959A (en) | 1972-10-25 | 1974-11-12 | Du Pont | Process of preparing a zerovalent nickel complex with organic phosphorus compounds |
| SU1096223A1 (ru) | 1981-11-16 | 1984-06-07 | Ленинградский Ордена Октябрьской Революции И Ордена Трудового Красного Знамени Технологический Институт Им.Ленсовета | Способ получени безводного хлорида никел |
| US5061669A (en) | 1988-11-30 | 1991-10-29 | Eastman Kodak Company | Preparation of biaryl compounds |
| DE4109743C2 (de) * | 1991-03-25 | 1995-03-23 | Escher Wyss Gmbh | Verfahren zur thermischen Behandlung von feuchten Hydraten |
| US5175335A (en) | 1991-11-12 | 1992-12-29 | E. I. Du Pont De Nemours And Company | Enantioselective hydrocyanation of aromatic vinyl compounds |
| CN1045301C (zh) * | 1993-10-12 | 1999-09-29 | 纳幕尔杜邦公司 | 一种改进的镍膦和镍的亚磷酸酯催化剂的合成方法 |
| DK0730574T3 (da) | 1993-11-23 | 1999-05-25 | Du Pont | Fremgangsmåder og katalysatorsammensætninger til hydrocyanering af monoolefiner |
| DE4344159A1 (de) | 1993-12-23 | 1995-06-29 | Bayer Ag | Verfahren zur Herstellung von Dimethylcarbonat |
| US5512695A (en) | 1994-04-14 | 1996-04-30 | E. I. Du Pont De Nemours And Company | Bidentate phosphite and nickel catalyst compositions for hydrocyanation of monoolefins |
| EP0755302B1 (en) * | 1994-04-14 | 2000-10-04 | E.I. Du Pont De Nemours And Company | Bidentate phosphite and nickel catalyst compositions for hydrocyanation of monoolefins |
| US5512696A (en) | 1995-07-21 | 1996-04-30 | E. I. Du Pont De Nemours And Company | Hydrocyanation process and multidentate phosphite and nickel catalyst composition therefor |
| TW315370B (enExample) | 1994-10-07 | 1997-09-11 | Du Pont | |
| US5523453A (en) | 1995-03-22 | 1996-06-04 | E. I. Du Pont De Nemours And Company | Process for hydrocyanation |
| FR2739378B1 (fr) * | 1995-09-29 | 1997-10-31 | Rhone Poulenc Fibres | Procede d'hydrocyanation de composes organiques a insaturation ethylenique |
| US5693843A (en) | 1995-12-22 | 1997-12-02 | E. I. Du Pont De Nemours And Company | Process for hydrocyanation of diolefins and isomerization of nonconjugated 2 alkyl-3-monoalkenenitriles |
| JPH1088205A (ja) * | 1996-09-10 | 1998-04-07 | Sumitomo Metal Mining Co Ltd | 金属ニッケル粉末の製造方法 |
| JPH11263625A (ja) | 1998-03-19 | 1999-09-28 | Sumitomo Metal Mining Co Ltd | 無水塩化ニッケルの製造方法 |
| JP4918194B2 (ja) * | 2001-03-22 | 2012-04-18 | Ｊｆｅミネラル株式会社 | 無水塩化ニッケルの製造方法 |
-
2001
- 2001-11-26 US US09/994,102 patent/US6893996B2/en not_active Expired - Fee Related
-
2002
- 2002-08-29 TW TW091119674A patent/TW592817B/zh not_active IP Right Cessation
- 2002-11-14 CN CNB2006101054979A patent/CN100445210C/zh not_active Expired - Lifetime
- 2002-11-14 EP EP05075636A patent/EP1604954A1/en not_active Withdrawn
- 2002-11-14 WO PCT/US2002/036468 patent/WO2003045555A2/en not_active Ceased
- 2002-11-14 AT AT02803976T patent/ATE307669T1/de not_active IP Right Cessation
- 2002-11-14 BR BRPI0214260-0A patent/BR0214260B1/pt not_active IP Right Cessation
- 2002-11-14 MX MXPA04004942A patent/MXPA04004942A/es active IP Right Grant
- 2002-11-14 RU RU2004116079/04A patent/RU2301704C2/ru not_active IP Right Cessation
- 2002-11-14 AU AU2002356942A patent/AU2002356942A1/en not_active Abandoned
- 2002-11-14 PL PL02371463A patent/PL371463A1/xx not_active Application Discontinuation
- 2002-11-14 KR KR1020047007924A patent/KR100912331B1/ko not_active Expired - Fee Related
- 2002-11-14 ES ES02803976T patent/ES2250748T3/es not_active Expired - Lifetime
- 2002-11-14 CN CNB028235339A patent/CN1293944C/zh not_active Expired - Lifetime
- 2002-11-14 EP EP02803976A patent/EP1450949B1/en not_active Expired - Lifetime
- 2002-11-14 JP JP2003547049A patent/JP2005510346A/ja active Pending
- 2002-11-14 KR KR1020097006558A patent/KR20090048517A/ko not_active Ceased
- 2002-11-14 CA CA002468293A patent/CA2468293A1/en not_active Abandoned
- 2002-11-14 DE DE60206958T patent/DE60206958T2/de not_active Expired - Lifetime
- 2002-11-26 MY MYPI20024421A patent/MY129876A/en unknown
-
2008
- 2008-11-05 JP JP2008284604A patent/JP2009035482A/ja active Pending
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