BR0214260B1 - Processo para a preparação de um catalisador de hidrocianação - Google Patents

Processo para a preparação de um catalisador de hidrocianação Download PDF

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Publication number
BR0214260B1
BR0214260B1 BRPI0214260-0A BR0214260A BR0214260B1 BR 0214260 B1 BR0214260 B1 BR 0214260B1 BR 0214260 A BR0214260 A BR 0214260A BR 0214260 B1 BR0214260 B1 BR 0214260B1
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BR
Brazil
Prior art keywords
alkyl
alkoxy
process according
same
nickel chloride
Prior art date
Application number
BRPI0214260-0A
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English (en)
Portuguese (pt)
Other versions
BR0214260A (pt
Inventor
Luis A Chu
Norman Herron
Kenneth G Moloy
Lucy M Clarkson
Ronald J Mckinney
Zeru Tekie
Original Assignee
Invista Tech Sarl
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Invista Tech Sarl filed Critical Invista Tech Sarl
Publication of BR0214260A publication Critical patent/BR0214260A/pt
Publication of BR0214260B1 publication Critical patent/BR0214260B1/pt

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/26Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
    • B01J31/28Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24 of the platinum group metals, iron group metals or copper
    • B01J31/30Halides
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/18Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/06Halogens; Compounds thereof
    • B01J27/128Halogens; Compounds thereof with iron group metals or platinum group metals
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/18Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
    • B01J31/1845Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms the ligands containing phosphorus
    • B01J31/185Phosphites ((RO)3P), their isomeric phosphonates (R(RO)2P=O) and RO-substitution derivatives thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/18Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
    • B01J31/1845Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms the ligands containing phosphorus
    • B01J31/1875Phosphinites (R2P(OR), their isomeric phosphine oxides (R3P=O) and RO-substitution derivatives thereof)
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/24Phosphines, i.e. phosphorus bonded to only carbon atoms, or to both carbon and hydrogen atoms, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, phosphole or anionic phospholide ligands
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/16Reducing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00Compounds of nickel
    • C01G53/08Halides; Oxyhalides
    • C01G53/09Chlorides; Oxychlorides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F15/00Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table
    • C07F15/04Nickel compounds
    • C07F15/045Nickel compounds without a metal-carbon linkage
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/30Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
    • B01J2231/32Addition reactions to C=C or C-C triple bonds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80Complexes comprising metals of Group VIII as the central metal
    • B01J2531/84Metals of the iron group
    • B01J2531/847Nickel
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/80Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/88Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by thermal analysis data, e.g. TGA, DTA, DSC
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/64Nanometer sized, i.e. from 1-100 nanometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity
    • C01P2006/82Compositional purity water content

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Nanotechnology (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Composite Materials (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
BRPI0214260-0A 2001-11-26 2002-11-14 Processo para a preparação de um catalisador de hidrocianação BR0214260B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US09/994,102 US6893996B2 (en) 2001-11-26 2001-11-26 Process for the preparation of a nickel/phosphorous ligand catalyst for olefin hydrocyanation
US09/994,102 2001-11-26
PCT/US2002/036468 WO2003045555A2 (en) 2001-11-26 2002-11-14 Process for the preparation of a nickel/phosphorus ligand catalyst for olefin hydrocyanation

Publications (2)

Publication Number Publication Date
BR0214260A BR0214260A (pt) 2004-09-21
BR0214260B1 true BR0214260B1 (pt) 2014-07-29

Family

ID=25540279

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0214260-0A BR0214260B1 (pt) 2001-11-26 2002-11-14 Processo para a preparação de um catalisador de hidrocianação

Country Status (17)

Country Link
US (1) US6893996B2 (enExample)
EP (2) EP1604954A1 (enExample)
JP (2) JP2005510346A (enExample)
KR (2) KR100912331B1 (enExample)
CN (2) CN100445210C (enExample)
AT (1) ATE307669T1 (enExample)
AU (1) AU2002356942A1 (enExample)
BR (1) BR0214260B1 (enExample)
CA (1) CA2468293A1 (enExample)
DE (1) DE60206958T2 (enExample)
ES (1) ES2250748T3 (enExample)
MX (1) MXPA04004942A (enExample)
MY (1) MY129876A (enExample)
PL (1) PL371463A1 (enExample)
RU (1) RU2301704C2 (enExample)
TW (1) TW592817B (enExample)
WO (1) WO2003045555A2 (enExample)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20030100803A1 (en) * 2001-11-26 2003-05-29 Lu Helen S.M. 3-Alkylated-5,5',6,6',7,7,'8,8'-octahydro-2,2'-binaphthols and 3,3'-dialkylated-5,5',6,6',7,7',8,8'-octahydro-2,2'-binaphthols and processes for making them
FR2849027B1 (fr) * 2002-12-23 2005-01-21 Rhodia Polyamide Intermediates Procede de synthese de composes comprenant des fonctions nitriles a partir de composes a insaturations ethyleniques
US6897329B2 (en) * 2003-01-14 2005-05-24 Invista North America S.A.R.L. Process for the preparation of nickel/phosphorous ligand catalyst for olefin hydrocyanation
FR2850966B1 (fr) 2003-02-10 2005-03-18 Rhodia Polyamide Intermediates Procede de fabrication de composes dinitriles
FR2854892B1 (fr) * 2003-05-12 2005-06-24 Rhodia Polyamide Intermediates Procede de fabrication de dinitriles
FR2854891B1 (fr) 2003-05-12 2006-07-07 Rhodia Polyamide Intermediates Procede de preparation de dinitriles
DE10351000A1 (de) * 2003-10-30 2005-06-09 Basf Ag Verfahren zur Herstellung von Nickel(O)-Phosphorligand-Komplexen
DE10351002A1 (de) * 2003-10-30 2005-05-25 Basf Ag Einsatz von azeotrop-getrockneten Nickel(II)-halogeniden
DE10351003A1 (de) * 2003-10-30 2005-05-25 Basf Ag Verfahren zur Herstellung von Nickel-Phosphorligand-Komplexen
DE102004004718A1 (de) * 2004-01-29 2005-08-18 Basf Ag Verfahren zur Hydrocyanierung
EP1825914A1 (de) * 2006-02-22 2007-08-29 Basf Aktiengesellschaft Verbessertes Verfahren zur Herstellung von Nickel(0)-Phophorligand-Komplexen
JP2009530278A (ja) * 2006-03-17 2009-08-27 インビスタ テクノロジーズ エス エイ アール エル 塩基性添加剤による処理でトリ有機ホスファイトを精製する方法
US7709673B2 (en) * 2006-07-14 2010-05-04 Invista North America S.A R.L. Process for making 3-pentenenitrile by hydrocyanation of butadiene
US7919646B2 (en) * 2006-07-14 2011-04-05 Invista North America S.A R.L. Hydrocyanation of 2-pentenenitrile
US7659422B2 (en) * 2006-07-14 2010-02-09 Invista North America S.A.R.L. Hydrocyanation process with reduced yield losses
US7709674B2 (en) * 2006-07-14 2010-05-04 Invista North America S.A R.L Hydrocyanation process with reduced yield losses
US7880028B2 (en) * 2006-07-14 2011-02-01 Invista North America S.A R.L. Process for making 3-pentenenitrile by hydrocyanation of butadiene
JP5295512B2 (ja) * 2007-03-29 2013-09-18 三井化学株式会社 ゼロ価ニッケルの有機ホスフィン錯体の製造方法
WO2009091790A1 (en) * 2008-01-15 2009-07-23 Invista Technologies S.A.R.L. Hydrocyanation of pentenenitriles
EP2229354B1 (en) * 2008-01-15 2013-03-20 Invista Technologies S.à.r.l. Process for making and refining 3-pentenenitrile, and for refining 2-methyl-3-butenenitrile
JP2013514258A (ja) 2009-12-18 2013-04-25 インビスタ テクノロジーズ エス エイ アール エル 塩基性炭酸ニッケルから生じさせたニッケル金属組成物およびニッケル錯体
CN103502206B (zh) 2010-07-07 2016-01-13 因温斯特技术公司 用于制备腈的方法
DK2614070T3 (en) * 2010-09-07 2017-10-16 Invista Technologies Sarl NICKEL COMPOSITIONS FOR THE MANUFACTURE OF NICKEL METAL AND NICKEL COMPLEXS
JP6054957B2 (ja) * 2011-06-10 2016-12-27 インヴィスタ テクノロジーズ エスアエルエルINVISTA TECHNOLOGIES S.a.r.l. ニッケル結晶子を含む粒子状ニッケル
CN104011014B (zh) 2011-10-07 2016-05-11 因温斯特技术公司 用于制备腈的方法
EP3022172B1 (en) 2013-07-17 2018-10-17 INVISTA Textiles (U.K.) Limited Separating a solvent from a nickel catalyst by distillation
KR102048134B1 (ko) * 2016-01-21 2019-11-22 제이엑스금속주식회사 무수 염화 니켈 및 그 제조 방법
CN114212836A (zh) * 2021-12-31 2022-03-22 金川集团镍盐有限公司 一种无水氯化镍粉体材料的制备方法
CN114835176A (zh) * 2022-05-30 2022-08-02 金川集团镍盐有限公司 一种球形无水氯化镍产品的制备方法
JP2024097610A (ja) * 2023-01-06 2024-07-19 レアメタルリサイクル環境合同会社 無水塩化ニッケル粉末の製造方法

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US3846461A (en) 1972-10-25 1974-11-05 Du Pont Process of preparing a zerovalent nickel complex with organic phosphorus compounds
US3847959A (en) 1972-10-25 1974-11-12 Du Pont Process of preparing a zerovalent nickel complex with organic phosphorus compounds
SU1096223A1 (ru) 1981-11-16 1984-06-07 Ленинградский Ордена Октябрьской Революции И Ордена Трудового Красного Знамени Технологический Институт Им.Ленсовета Способ получени безводного хлорида никел
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US5175335A (en) 1991-11-12 1992-12-29 E. I. Du Pont De Nemours And Company Enantioselective hydrocyanation of aromatic vinyl compounds
ATE192050T1 (de) * 1993-10-12 2000-05-15 Du Pont Synthese von nickelphosphin- und nickelphosphitkomplexen, verwendbar als katalysatoren
ES2122515T3 (es) 1993-11-23 1998-12-16 Du Pont Procedimientos y composiciones cataliticas para hidrocianacion de monoolefinas.
DE4344159A1 (de) 1993-12-23 1995-06-29 Bayer Ag Verfahren zur Herstellung von Dimethylcarbonat
ES2151958T3 (es) * 1994-04-14 2001-01-16 Du Pont Composiciones de catalizador de niquel y fosfito bidentado para hidrocianacion de monoolefinas.
US5512695A (en) 1994-04-14 1996-04-30 E. I. Du Pont De Nemours And Company Bidentate phosphite and nickel catalyst compositions for hydrocyanation of monoolefins
TW315370B (enExample) 1994-10-07 1997-09-11 Du Pont
US5512696A (en) 1995-07-21 1996-04-30 E. I. Du Pont De Nemours And Company Hydrocyanation process and multidentate phosphite and nickel catalyst composition therefor
US5523453A (en) 1995-03-22 1996-06-04 E. I. Du Pont De Nemours And Company Process for hydrocyanation
FR2739378B1 (fr) * 1995-09-29 1997-10-31 Rhone Poulenc Fibres Procede d'hydrocyanation de composes organiques a insaturation ethylenique
US5693843A (en) 1995-12-22 1997-12-02 E. I. Du Pont De Nemours And Company Process for hydrocyanation of diolefins and isomerization of nonconjugated 2 alkyl-3-monoalkenenitriles
JPH1088205A (ja) * 1996-09-10 1998-04-07 Sumitomo Metal Mining Co Ltd 金属ニッケル粉末の製造方法
JPH11263625A (ja) 1998-03-19 1999-09-28 Sumitomo Metal Mining Co Ltd 無水塩化ニッケルの製造方法
JP4918194B2 (ja) * 2001-03-22 2012-04-18 Jfeミネラル株式会社 無水塩化ニッケルの製造方法

Also Published As

Publication number Publication date
DE60206958D1 (de) 2005-12-01
EP1450949A2 (en) 2004-09-01
EP1604954A1 (en) 2005-12-14
ES2250748T3 (es) 2006-04-16
CN1596152A (zh) 2005-03-16
WO2003045555A3 (en) 2003-11-06
RU2301704C2 (ru) 2007-06-27
KR20090048517A (ko) 2009-05-13
DE60206958T2 (de) 2006-08-03
US20030100442A1 (en) 2003-05-29
AU2002356942A1 (en) 2003-06-10
CN1293944C (zh) 2007-01-10
CN1899972A (zh) 2007-01-24
CA2468293A1 (en) 2003-06-05
US6893996B2 (en) 2005-05-17
RU2004116079A (ru) 2005-03-27
ATE307669T1 (de) 2005-11-15
KR20040060989A (ko) 2004-07-06
CN100445210C (zh) 2008-12-24
MXPA04004942A (es) 2004-08-11
PL371463A1 (en) 2005-06-13
BR0214260A (pt) 2004-09-21
JP2009035482A (ja) 2009-02-19
WO2003045555A2 (en) 2003-06-05
EP1450949B1 (en) 2005-10-26
JP2005510346A (ja) 2005-04-21
MY129876A (en) 2007-05-31
TW592817B (en) 2004-06-21
KR100912331B1 (ko) 2009-08-14

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