HRP20180070T1 - Mješavine talinske faze poliestera s poboljšanom termooksidativnom stabilnošću, te postupci njihovog dobivanja i upotrebe - Google Patents
Mješavine talinske faze poliestera s poboljšanom termooksidativnom stabilnošću, te postupci njihovog dobivanja i upotrebe Download PDFInfo
- Publication number
- HRP20180070T1 HRP20180070T1 HRP20180070TT HRP20180070T HRP20180070T1 HR P20180070 T1 HRP20180070 T1 HR P20180070T1 HR P20180070T T HRP20180070T T HR P20180070TT HR P20180070 T HRP20180070 T HR P20180070T HR P20180070 T1 HRP20180070 T1 HR P20180070T1
- Authority
- HR
- Croatia
- Prior art keywords
- mixture
- polyester
- amount
- molar
- ppm
- Prior art date
Links
- 239000000203 mixture Substances 0.000 title claims 19
- 229920000728 polyester Polymers 0.000 title claims 19
- 238000000034 method Methods 0.000 title claims 10
- 229920000139 polyethylene terephthalate Polymers 0.000 claims 9
- 239000005020 polyethylene terephthalate Substances 0.000 claims 9
- 125000003118 aryl group Chemical group 0.000 claims 7
- 239000000178 monomer Substances 0.000 claims 7
- -1 polyethylene terephthalate Polymers 0.000 claims 7
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 6
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 6
- 239000000155 melt Substances 0.000 claims 5
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 claims 4
- RXOHFPCZGPKIRD-UHFFFAOYSA-N naphthalene-2,6-dicarboxylic acid Chemical compound C1=C(C(O)=O)C=CC2=CC(C(=O)O)=CC=C21 RXOHFPCZGPKIRD-UHFFFAOYSA-N 0.000 claims 4
- 229910052719 titanium Inorganic materials 0.000 claims 4
- 239000010936 titanium Substances 0.000 claims 4
- 125000001142 dicarboxylic acid group Chemical group 0.000 claims 3
- XGWFJBFNAQHLEF-UHFFFAOYSA-N 9-anthroic acid Chemical class C1=CC=C2C(C(=O)O)=C(C=CC=C3)C3=CC2=C1 XGWFJBFNAQHLEF-UHFFFAOYSA-N 0.000 claims 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims 2
- HGUJMOWJGKVZGD-UHFFFAOYSA-N dimethyl anthracene-1,5-dicarboxylate Chemical compound C1=CC=C2C=C3C(C(=O)OC)=CC=CC3=CC2=C1C(=O)OC HGUJMOWJGKVZGD-UHFFFAOYSA-N 0.000 claims 2
- ALYSIEHCBBJETD-UHFFFAOYSA-N dimethyl anthracene-1,8-dicarboxylate Chemical compound C1=CC(C(=O)OC)=C2C=C3C(C(=O)OC)=CC=CC3=CC2=C1 ALYSIEHCBBJETD-UHFFFAOYSA-N 0.000 claims 2
- WZBZJYAQKFBFTJ-UHFFFAOYSA-N dimethyl anthracene-2,6-dicarboxylate Chemical compound C1=C(C(=O)OC)C=CC2=CC3=CC(C(=O)OC)=CC=C3C=C21 WZBZJYAQKFBFTJ-UHFFFAOYSA-N 0.000 claims 2
- GYUVMLBYMPKZAZ-UHFFFAOYSA-N dimethyl naphthalene-2,6-dicarboxylate Chemical compound C1=C(C(=O)OC)C=CC2=CC(C(=O)OC)=CC=C21 GYUVMLBYMPKZAZ-UHFFFAOYSA-N 0.000 claims 2
- 238000002844 melting Methods 0.000 claims 2
- 230000008018 melting Effects 0.000 claims 2
- 229910052698 phosphorus Inorganic materials 0.000 claims 2
- 239000011574 phosphorus Substances 0.000 claims 2
- 238000006116 polymerization reaction Methods 0.000 claims 2
- 239000002253 acid Substances 0.000 claims 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 1
- 229910052787 antimony Inorganic materials 0.000 claims 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 claims 1
- 150000002009 diols Chemical class 0.000 claims 1
- 229910052732 germanium Inorganic materials 0.000 claims 1
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 claims 1
- 125000004437 phosphorous atom Chemical group 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 150000003503 terephthalic acid derivatives Chemical class 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
- C08G63/16—Dicarboxylic acids and dihydroxy compounds
- C08G63/18—Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
- C08G63/181—Acids containing aromatic rings
- C08G63/185—Acids containing aromatic rings containing two or more aromatic rings
- C08G63/187—Acids containing aromatic rings containing two or more aromatic rings containing condensed aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
- C08L67/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
- C08L67/03—Polyesters derived from dicarboxylic acids and dihydroxy compounds the dicarboxylic acids and dihydroxy compounds having the carboxyl- and the hydroxy groups directly linked to aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
- C08G63/16—Dicarboxylic acids and dihydroxy compounds
- C08G63/18—Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
- C08G63/181—Acids containing aromatic rings
- C08G63/183—Terephthalic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/78—Preparation processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/78—Preparation processes
- C08G63/82—Preparation processes characterised by the catalyst used
- C08G63/85—Germanium, tin, lead, arsenic, antimony, bismuth, titanium, zirconium, hafnium, vanadium, niobium, tantalum, or compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyesters Or Polycarbonates (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Claims (14)
1. Poliesterska mješavina, naznačena time što sadrži: talinsku fazu polietilen-tereftalatnog poliestera koja u sebi sadrži uključene ostatke monomera koji ima dva ili više kondenziranih aromatskih prstena, u količini od 0,5%, molarno, do 2,5%, molarno, na osnovi ukupne količine ostataka dikarboksilne kiseline u talinskoj fazi polietilen-tereftalatnog poliestera koju čini 100%, molarno; i titanij; gdje je titanij prisutan u količini od 3 ppm do 100 ppm atoma titanija, na osnovi ukupne težine poliesterske mješavine.
2. Poliesterska mješavina u skladu s patentnim zahtjevom 1, naznačena time što monomer koji ima dva ili više kondenziranih aromatskih prstena sadrži jedno ili više od: 2,6-naftalendikarboksilne kiseline; dimetil-2,6-naftalendikarboksilata; 9-antracenkarboksilne kiseline; 2,6-antracendikarboksilne kiseline; dimetil-2,6-antracendikarboksilata; 1,5-antracendikarboksilne kiseline; dimetil-1,5-antracendikarboksilata; 1,8-antracendikarboksilne kiseline; ili dimetil-1,8-antracendikarboksilata.
3. Poliesterska mješavina u skladu s patentnim zahtjevom 1, naznačena time što monomer koji ima dva ili više kondenziranih aromatskih prstena sadrži 2,6-naftalendikarboksilnu kiselinu, prisutnu u količini od 0,5%, molarno, do 2,5%, molarno.
4. Poliesterska mješavina u skladu s patentnim zahtjevom 1, naznačena time što poliesterska mješavina dodatno sadrži ostatke fosforne kiseline.
5. Poliesterska mješavina u skladu s patentnim zahtjevom 1, naznačena time što poliesterska mješavina dodatno sadrži atome fosfora prisutne u količini od 5 ppm do 300 ppm.
6. Poliesterska mješavina u skladu s patentnim zahtjevom 1, naznačena time što dobivena talinska faza polietilen-tereftalatnog poliestera iz talinske faze reakcijom polimerizacije ima I. V. od najmanje 0,72 dl/g.
7. Postupak dobivanja talinske faze polietilen-tereftalatnog poliestera, naznačen time što se sastoji u: dobivanju smjese koja sadrži etilen-glikol, najmanje jednu kiselinu, koju se bira između tereftalne kiseline i derivata tereftalne kiseline, te monomer koji ima dva ili više kondenziranih aromatskih prstena, gdje je monomer koji ima dva ili više kondenziranih aromatskih prstena prisutan u količini od 0,5%, molarno, do 2,5%, molarno, na osnovi ukupne količine ostataka dikarboksilne kiseline u smjesi koju čini 100%, molarno; zatim u reakciji smjese u prisutnosti titanija kako bi se dobilo talinsku fazu polietilen-tereftalatnog poliestera; gdje smjesa ne sadrži antimon, gdje je titanij prisutan u količini od 1 ppm do 150 ppm atoma titanija, na osnovi ukupne težine dobivene talinske faze polietilen-tereftalatnog poliestera.
8. Postupak u skladu s patentnim zahtjevom 7, naznačen time što: smjesa sadrži tereftalnu kiselinu, prisutnu u količini od najmanje 90%, molarno, na osnovi ukupne količine ostataka dikarboksilne kiseline u smjesi koju čini 100%, molarno, a etilen-glikol je prisutan u smjesi u količini od najmanje 90%, molarno, na osnovi ukupne količine diola u smjesi koju čini 100%, molarno.
9. Postupak u skladu s patentnim zahtjevom 8, naznačen time što monomer koji ima dva ili više kondenziranih aromatskih prstena sadrži jedno ili više od: 2,6-naftalendikarboksilne kiseline; dimetil-2,6-naftalendikarboksilata; 9-antracenkarboksilne kiseline; 2,6-antracendikarboksilne kiseline; dimetil-2,6-antracendikarboksilata; 1,5-antracendikarboksilne kiseline; dimetil-1,5-antracendikarboksilata; 1,8-antracendikarboksilne kiseline; ili dimetil-1,8-antracendikarboksilata.
10. Postupak u skladu s patentnim zahtjevom 7, naznačen time što monomer koji ima dva ili više kondenziranih aromatskih prstena sadrži 2,6-naftalendikarboksilnu kiselinu, prisutnu u količini od 0,5%, molarno, do 2,5%, molarno.
11. Postupak u skladu s patentnim zahtjevom 7, naznačen time što smjesa ne sadrži germanij.
12. Postupak u skladu s patentnim zahtjevom 7, naznačen time što dodatno uključuje korak: dodavanja fosfora u dobivenu talinsku fazu polietilen-tereftalatnog poliestera, u količini od 5 ppm do 300 ppm fosfora, na osnovi ukupne težine dobivene talinske faze polietilen-tereftalatnog poliestera.
13. Postupak u skladu s patentnim zahtjevom 7, naznačen time što dobivena talinska faza polietilen-tereftalatnog poliestera ima I.V. od najmanje 0,72 dl/g postignut u talinskoj fazi.
14. Postupak u skladu s patentnim zahtjevom 7, naznačen time što postupak ne uključuje polimerizaciju u čvrstom stanju.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US9804308P | 2008-09-18 | 2008-09-18 | |
| PCT/US2009/005045 WO2010033162A1 (en) | 2008-09-18 | 2009-09-08 | Polyester melt-phase compositions having improved thermo-oxidative stability, and methods of making and using them |
| EP09789276.4A EP2331604B1 (en) | 2008-09-18 | 2009-09-08 | Polyester melt-phase compositions having improved thermo-oxidative stability, and methods of making and using them |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| HRP20180070T1 true HRP20180070T1 (hr) | 2018-02-23 |
Family
ID=41467063
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| HRP20180070TT HRP20180070T1 (hr) | 2008-09-18 | 2018-01-15 | Mješavine talinske faze poliestera s poboljšanom termooksidativnom stabilnošću, te postupci njihovog dobivanja i upotrebe |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US20100069556A1 (hr) |
| EP (1) | EP2331604B1 (hr) |
| JP (1) | JP5677957B2 (hr) |
| KR (1) | KR101732743B1 (hr) |
| CN (1) | CN102177191A (hr) |
| BR (1) | BRPI0918554B1 (hr) |
| CA (1) | CA2737532C (hr) |
| ES (1) | ES2658828T3 (hr) |
| HR (1) | HRP20180070T1 (hr) |
| HU (1) | HUE035957T2 (hr) |
| LT (1) | LT2331604T (hr) |
| MX (1) | MX2011002922A (hr) |
| RU (1) | RU2550211C2 (hr) |
| SG (1) | SG190635A1 (hr) |
| WO (1) | WO2010033162A1 (hr) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102250622B (zh) * | 2011-08-15 | 2013-09-04 | 金发科技股份有限公司 | 一种制备不易流动的物料的方法 |
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| US4745402A (en) * | 1987-02-19 | 1988-05-17 | Rca Licensing Corporation | Input device for a display system using phase-encoded signals |
| EP0282660B1 (en) * | 1987-03-17 | 1991-06-05 | Unitika Ltd. | Polyester fiber and process for producing the same |
| JPH03231918A (ja) * | 1990-02-07 | 1991-10-15 | Teijin Ltd | ポリエステルの製造法 |
| US5418318A (en) * | 1993-08-09 | 1995-05-23 | Eastman Chemical Company | Naphthalenedicarboxylic acid containing polymer/halogen compound compositions having reduced fluorescence |
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| CA2189286C (en) * | 1995-11-16 | 2000-05-30 | Shinji Tai | Copolyesters and molded articles comprising the same |
| JPH09221541A (ja) * | 1996-02-15 | 1997-08-26 | Nippon Ester Co Ltd | 共重合ポリエステルの製造法 |
| DE69716894T2 (de) * | 1996-04-05 | 2003-07-03 | Teijin Ltd., Osaka | Ethylenterephtalat-ethylen 2,6-naphthalendicarboxylat copolymer für flaschen |
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-
2009
- 2009-08-28 US US12/549,821 patent/US20100069556A1/en not_active Abandoned
- 2009-09-08 BR BRPI0918554-2A patent/BRPI0918554B1/pt active IP Right Grant
- 2009-09-08 SG SG2013034921A patent/SG190635A1/en unknown
- 2009-09-08 CN CN2009801368836A patent/CN102177191A/zh active Pending
- 2009-09-08 KR KR1020117008629A patent/KR101732743B1/ko active IP Right Grant
- 2009-09-08 MX MX2011002922A patent/MX2011002922A/es active IP Right Grant
- 2009-09-08 RU RU2011114980/04A patent/RU2550211C2/ru active
- 2009-09-08 ES ES09789276.4T patent/ES2658828T3/es active Active
- 2009-09-08 HU HUE09789276A patent/HUE035957T2/hu unknown
- 2009-09-08 WO PCT/US2009/005045 patent/WO2010033162A1/en active Application Filing
- 2009-09-08 EP EP09789276.4A patent/EP2331604B1/en active Active
- 2009-09-08 LT LTEP09789276.4T patent/LT2331604T/lt unknown
- 2009-09-08 CA CA2737532A patent/CA2737532C/en active Active
- 2009-09-08 JP JP2011527805A patent/JP5677957B2/ja active Active
-
2018
- 2018-01-15 HR HRP20180070TT patent/HRP20180070T1/hr unknown
Also Published As
| Publication number | Publication date |
|---|---|
| KR20110087266A (ko) | 2011-08-02 |
| KR101732743B1 (ko) | 2017-05-04 |
| CA2737532C (en) | 2017-08-29 |
| CA2737532A1 (en) | 2010-03-25 |
| MX2011002922A (es) | 2011-07-04 |
| BRPI0918554B1 (pt) | 2019-06-25 |
| US20100069556A1 (en) | 2010-03-18 |
| WO2010033162A1 (en) | 2010-03-25 |
| JP2012503067A (ja) | 2012-02-02 |
| LT2331604T (lt) | 2018-02-12 |
| SG190635A1 (en) | 2013-06-28 |
| HUE035957T2 (hu) | 2018-06-28 |
| RU2011114980A (ru) | 2012-10-27 |
| EP2331604A1 (en) | 2011-06-15 |
| RU2550211C2 (ru) | 2015-05-10 |
| JP5677957B2 (ja) | 2015-02-25 |
| CN102177191A (zh) | 2011-09-07 |
| BRPI0918554A2 (pt) | 2015-12-01 |
| EP2331604B1 (en) | 2017-12-27 |
| ES2658828T3 (es) | 2018-03-12 |
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