DE2711420A1 - Verfahren zur herstellung von beta-lithiumaluminat - Google Patents
Verfahren zur herstellung von beta-lithiumaluminatInfo
- Publication number
- DE2711420A1 DE2711420A1 DE19772711420 DE2711420A DE2711420A1 DE 2711420 A1 DE2711420 A1 DE 2711420A1 DE 19772711420 DE19772711420 DE 19772711420 DE 2711420 A DE2711420 A DE 2711420A DE 2711420 A1 DE2711420 A1 DE 2711420A1
- Authority
- DE
- Germany
- Prior art keywords
- lithium aluminate
- lithium
- hours
- tempering
- aluminate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims description 22
- 238000004519 manufacturing process Methods 0.000 title claims description 9
- YQNQTEBHHUSESQ-UHFFFAOYSA-N lithium aluminate Chemical compound [Li+].[O-][Al]=O YQNQTEBHHUSESQ-UHFFFAOYSA-N 0.000 title description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 239000000203 mixture Substances 0.000 claims description 15
- 238000001556 precipitation Methods 0.000 claims description 12
- 238000005496 tempering Methods 0.000 claims description 11
- 239000003792 electrolyte Substances 0.000 claims description 9
- 239000000446 fuel Substances 0.000 claims description 7
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 6
- 239000003513 alkali Substances 0.000 claims description 6
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 6
- 229910052744 lithium Inorganic materials 0.000 claims description 6
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 5
- 229910052782 aluminium Inorganic materials 0.000 claims description 5
- 239000013078 crystal Substances 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 4
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 229910001416 lithium ion Inorganic materials 0.000 claims description 3
- 229910018068 Li 2 O Inorganic materials 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 229910052751 metal Inorganic materials 0.000 claims description 2
- 239000002184 metal Substances 0.000 claims description 2
- 239000007858 starting material Substances 0.000 claims description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 23
- 235000019441 ethanol Nutrition 0.000 description 13
- 239000000047 product Substances 0.000 description 13
- 229910010093 LiAlO Inorganic materials 0.000 description 11
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 11
- 239000002244 precipitate Substances 0.000 description 11
- 239000000243 solution Substances 0.000 description 8
- 239000000725 suspension Substances 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 6
- 238000002441 X-ray diffraction Methods 0.000 description 5
- QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Substances CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 238000000137 annealing Methods 0.000 description 3
- 239000002243 precursor Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 description 2
- 229910003002 lithium salt Inorganic materials 0.000 description 2
- 159000000002 lithium salts Chemical class 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000008188 pellet Substances 0.000 description 2
- FARHYDJOXLCMRP-UHFFFAOYSA-N 2-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]-1-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]pyrazol-3-yl]oxyacetic acid Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C=1C(=NN(C=1)CC(N1CC2=C(CC1)NN=N2)=O)OCC(=O)O FARHYDJOXLCMRP-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 229910017090 AlO 2 Inorganic materials 0.000 description 1
- 240000006829 Ficus sundaica Species 0.000 description 1
- 229910007857 Li-Al Inorganic materials 0.000 description 1
- 229910008447 Li—Al Inorganic materials 0.000 description 1
- 101100010166 Mus musculus Dok3 gene Proteins 0.000 description 1
- 229910004786 P-Li Inorganic materials 0.000 description 1
- 229910004796 P—Li Inorganic materials 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 description 1
- 229910000288 alkali metal carbonate Inorganic materials 0.000 description 1
- 150000008041 alkali metal carbonates Chemical class 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 150000004645 aluminates Chemical class 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- -1 aluminum hydroxide acetate Chemical compound 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 235000013601 eggs Nutrition 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 description 1
- 229910052808 lithium carbonate Inorganic materials 0.000 description 1
- HPGPEWYJWRWDTP-UHFFFAOYSA-N lithium peroxide Chemical compound [Li+].[Li+].[O-][O-] HPGPEWYJWRWDTP-UHFFFAOYSA-N 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003746 solid phase reaction Methods 0.000 description 1
- 238000010671 solid-state reaction Methods 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000008646 thermal stress Effects 0.000 description 1
- 238000012982 x-ray structure analysis Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/02—Details
- H01M8/0289—Means for holding the electrolyte
- H01M8/0295—Matrices for immobilising electrolyte melts
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/04—Preparation of alkali metal aluminates; Aluminium oxide or hydroxide therefrom
- C01F7/043—Lithium aluminates
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/50—Fuel cells
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Sustainable Energy (AREA)
- Sustainable Development (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Fuel Cell (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Secondary Cells (AREA)
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19772711420 DE2711420A1 (de) | 1977-03-16 | 1977-03-16 | Verfahren zur herstellung von beta-lithiumaluminat |
| US05/886,365 US4164557A (en) | 1977-03-16 | 1978-03-14 | Process for the production of β-lithium aluminate and needle-shaped product |
| CA298,964A CA1086920A (en) | 1977-03-16 | 1978-03-15 | PROCEDURE FOR THE PREPARATION .beta.-LITHIUMALUMINATE |
| JP53030506A JPS608971B2 (ja) | 1977-03-16 | 1978-03-16 | β‐リチウムアルミネ−トの製法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19772711420 DE2711420A1 (de) | 1977-03-16 | 1977-03-16 | Verfahren zur herstellung von beta-lithiumaluminat |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2711420A1 true DE2711420A1 (de) | 1978-09-21 |
| DE2711420C2 DE2711420C2 (enExample) | 1988-01-28 |
Family
ID=6003779
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19772711420 Granted DE2711420A1 (de) | 1977-03-16 | 1977-03-16 | Verfahren zur herstellung von beta-lithiumaluminat |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US4164557A (enExample) |
| JP (1) | JPS608971B2 (enExample) |
| CA (1) | CA1086920A (enExample) |
| DE (1) | DE2711420A1 (enExample) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0066751A1 (en) * | 1981-05-20 | 1982-12-15 | Hitachi, Ltd. | Fuel cell provided with electrolyte plate made of electrical insulating long fibers |
| FR2563512A1 (fr) * | 1984-04-25 | 1985-10-31 | Kernforschungsz Karlsruhe | Procede pour la fabrication de poudre frittable de m-lia102 et son utilisation |
| EP0336322A1 (en) * | 1988-04-01 | 1989-10-11 | Hitachi, Ltd. | Process for producing lithium aluminate powder having large specific surface area |
| EP0499639A4 (en) * | 1989-04-12 | 1993-05-26 | Ishikawajima-Harima Heavy Industries Co., Ltd. | Method of producing porous lithium aluminate fiber and coarse particle |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS56118276A (en) * | 1980-02-21 | 1981-09-17 | Hitachi Ltd | Manufacture of electrolyte plate for fuel cell |
| US4405595A (en) * | 1982-01-15 | 1983-09-20 | Ga Technologies Inc. | Method of producing spherical lithium aluminate particles |
| JPS61295227A (ja) * | 1985-06-20 | 1986-12-26 | Sumitomo Chem Co Ltd | リチウムアルミネ−ト粉末の製造方法 |
| RU2245402C2 (ru) * | 2003-02-05 | 2005-01-27 | Федеральное государственное унитарное предприятие "Всероссийский научно-исследовательский институт синтеза минерального сырья" (ФГУП "ВНИИСИМС") | Способ получения монокристаллов алюмината лития |
| JP5025996B2 (ja) * | 2006-06-05 | 2012-09-12 | 電気化学工業株式会社 | リチウムアルミネートの製造方法及びリチウムアルミネート |
| US20080032183A1 (en) * | 2006-08-07 | 2008-02-07 | Gengfu Xu | Coated support material for use in fabricating a fuel cell matrix and method of forming same using alkaline precursors |
| JP6301814B2 (ja) * | 2014-11-06 | 2018-03-28 | Ｊｘ金属株式会社 | アルミニウム含有酸性溶液からのアルミニウム分離方法、リチウム・アルミニウム系複合水酸化物の製造方法 |
| FI20225757A1 (en) * | 2022-08-29 | 2024-03-01 | Metso Outotec Finland Oy | A method for recovering lithium from a stream containing lithium |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2637096A1 (de) * | 1975-08-20 | 1977-02-24 | Inst Gas Technology | Verfahren zur herstellung von beta-lithiumaluminat |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3859427A (en) * | 1969-11-10 | 1975-01-07 | Aluminum Co Of America | Production of beta alumina |
| US3878296A (en) * | 1971-08-18 | 1975-04-15 | United Aircraft Corp | Reaction of lithium carbonate and fibrous aluminum oxide to produce lithium aluminate |
| US4029755A (en) * | 1972-02-07 | 1977-06-14 | The United States Of America As Represented By The Secretary Of The Army | Transparent ultrafine grained ceramics |
-
1977
- 1977-03-16 DE DE19772711420 patent/DE2711420A1/de active Granted
-
1978
- 1978-03-14 US US05/886,365 patent/US4164557A/en not_active Expired - Lifetime
- 1978-03-15 CA CA298,964A patent/CA1086920A/en not_active Expired
- 1978-03-16 JP JP53030506A patent/JPS608971B2/ja not_active Expired
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2637096A1 (de) * | 1975-08-20 | 1977-02-24 | Inst Gas Technology | Verfahren zur herstellung von beta-lithiumaluminat |
Non-Patent Citations (2)
| Title |
|---|
| Russian Journal of Inorganic Chemistry, 13 (2), 1968, S.213-215 * |
| Russian Journal of Inorganic Chemistry, Vol. 12, No. 11, S.1704-1705 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0066751A1 (en) * | 1981-05-20 | 1982-12-15 | Hitachi, Ltd. | Fuel cell provided with electrolyte plate made of electrical insulating long fibers |
| FR2563512A1 (fr) * | 1984-04-25 | 1985-10-31 | Kernforschungsz Karlsruhe | Procede pour la fabrication de poudre frittable de m-lia102 et son utilisation |
| EP0336322A1 (en) * | 1988-04-01 | 1989-10-11 | Hitachi, Ltd. | Process for producing lithium aluminate powder having large specific surface area |
| EP0499639A4 (en) * | 1989-04-12 | 1993-05-26 | Ishikawajima-Harima Heavy Industries Co., Ltd. | Method of producing porous lithium aluminate fiber and coarse particle |
Also Published As
| Publication number | Publication date |
|---|---|
| US4164557A (en) | 1979-08-14 |
| JPS608971B2 (ja) | 1985-03-07 |
| CA1086920A (en) | 1980-10-07 |
| JPS53140300A (en) | 1978-12-07 |
| DE2711420C2 (enExample) | 1988-01-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OGA | New person/name/address of the applicant | ||
| 8110 | Request for examination paragraph 44 | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |