JPS608971B2 - β‐リチウムアルミネ−トの製法 - Google Patents
β‐リチウムアルミネ−トの製法Info
- Publication number
- JPS608971B2 JPS608971B2 JP53030506A JP3050678A JPS608971B2 JP S608971 B2 JPS608971 B2 JP S608971B2 JP 53030506 A JP53030506 A JP 53030506A JP 3050678 A JP3050678 A JP 3050678A JP S608971 B2 JPS608971 B2 JP S608971B2
- Authority
- JP
- Japan
- Prior art keywords
- lithium
- lithium aluminate
- hours
- heat treatment
- aluminate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 17
- 239000000203 mixture Substances 0.000 claims description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 238000000034 method Methods 0.000 claims description 15
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 8
- 239000013078 crystal Substances 0.000 claims description 7
- 229910052744 lithium Inorganic materials 0.000 claims description 7
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 6
- 229910052782 aluminium Inorganic materials 0.000 claims description 6
- YQNQTEBHHUSESQ-UHFFFAOYSA-N lithium aluminate Chemical compound [Li+].[O-][Al]=O YQNQTEBHHUSESQ-UHFFFAOYSA-N 0.000 claims description 6
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 claims description 5
- 239000012736 aqueous medium Substances 0.000 claims description 5
- 229910001416 lithium ion Inorganic materials 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 5
- 230000001788 irregular Effects 0.000 claims description 4
- 229910052751 metal Inorganic materials 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 4
- 239000013081 microcrystal Substances 0.000 claims description 3
- 238000001556 precipitation Methods 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 2
- 230000009466 transformation Effects 0.000 claims 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 26
- 239000000047 product Substances 0.000 description 20
- 239000002244 precipitate Substances 0.000 description 17
- 235000019441 ethanol Nutrition 0.000 description 15
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 9
- 239000000243 solution Substances 0.000 description 8
- 239000000725 suspension Substances 0.000 description 8
- 239000003792 electrolyte Substances 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 239000000446 fuel Substances 0.000 description 5
- 238000002441 X-ray diffraction Methods 0.000 description 4
- 239000003513 alkali Substances 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 229910052808 lithium carbonate Inorganic materials 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 3
- 238000000635 electron micrograph Methods 0.000 description 3
- 239000012467 final product Substances 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 241000276425 Xiphophorus maculatus Species 0.000 description 2
- 150000004645 aluminates Chemical class 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 101100010166 Mus musculus Dok3 gene Proteins 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- FCVHBUFELUXTLR-UHFFFAOYSA-N [Li].[AlH3] Chemical compound [Li].[AlH3] FCVHBUFELUXTLR-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 description 1
- HPGPEWYJWRWDTP-UHFFFAOYSA-N lithium peroxide Chemical compound [Li+].[Li+].[O-][O-] HPGPEWYJWRWDTP-UHFFFAOYSA-N 0.000 description 1
- 229910003002 lithium salt Inorganic materials 0.000 description 1
- 159000000002 lithium salts Chemical class 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003746 solid phase reaction Methods 0.000 description 1
- 238000010671 solid-state reaction Methods 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000011282 treatment Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/02—Details
- H01M8/0289—Means for holding the electrolyte
- H01M8/0295—Matrices for immobilising electrolyte melts
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/04—Preparation of alkali metal aluminates; Aluminium oxide or hydroxide therefrom
- C01F7/043—Lithium aluminates
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/50—Fuel cells
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Sustainable Energy (AREA)
- Sustainable Development (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Fuel Cell (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Secondary Cells (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19772711420 DE2711420A1 (de) | 1977-03-16 | 1977-03-16 | Verfahren zur herstellung von beta-lithiumaluminat |
| DE2711420.1 | 1977-03-16 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS53140300A JPS53140300A (en) | 1978-12-07 |
| JPS608971B2 true JPS608971B2 (ja) | 1985-03-07 |
Family
ID=6003779
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP53030506A Expired JPS608971B2 (ja) | 1977-03-16 | 1978-03-16 | β‐リチウムアルミネ−トの製法 |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US4164557A (enExample) |
| JP (1) | JPS608971B2 (enExample) |
| CA (1) | CA1086920A (enExample) |
| DE (1) | DE2711420A1 (enExample) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS56118276A (en) * | 1980-02-21 | 1981-09-17 | Hitachi Ltd | Manufacture of electrolyte plate for fuel cell |
| JPS57191962A (en) * | 1981-05-20 | 1982-11-25 | Hitachi Ltd | Fuel cell |
| US4405595A (en) * | 1982-01-15 | 1983-09-20 | Ga Technologies Inc. | Method of producing spherical lithium aluminate particles |
| DE3415324C2 (de) * | 1984-04-25 | 1986-11-06 | Kernforschungszentrum Karlsruhe Gmbh, 7500 Karlsruhe | Verfahren zur Herstellung von sinterfähigem Pulver aus γ-LiAl0↓2↓ und dessen Verwendung |
| JPS61295227A (ja) * | 1985-06-20 | 1986-12-26 | Sumitomo Chem Co Ltd | リチウムアルミネ−ト粉末の製造方法 |
| JP2539483B2 (ja) * | 1988-04-01 | 1996-10-02 | 株式会社日立製作所 | 比表面積の大きなリチウムアルミネ―ト粉体の製造法 |
| JPH02271911A (ja) * | 1989-04-12 | 1990-11-06 | Ishikawajima Harima Heavy Ind Co Ltd | 多孔質リチウムアルミネート繊維の製造方法 |
| RU2245402C2 (ru) * | 2003-02-05 | 2005-01-27 | Федеральное государственное унитарное предприятие "Всероссийский научно-исследовательский институт синтеза минерального сырья" (ФГУП "ВНИИСИМС") | Способ получения монокристаллов алюмината лития |
| JP5025996B2 (ja) * | 2006-06-05 | 2012-09-12 | 電気化学工業株式会社 | リチウムアルミネートの製造方法及びリチウムアルミネート |
| US20080032183A1 (en) * | 2006-08-07 | 2008-02-07 | Gengfu Xu | Coated support material for use in fabricating a fuel cell matrix and method of forming same using alkaline precursors |
| JP6301814B2 (ja) * | 2014-11-06 | 2018-03-28 | Ｊｘ金属株式会社 | アルミニウム含有酸性溶液からのアルミニウム分離方法、リチウム・アルミニウム系複合水酸化物の製造方法 |
| FI20225757A1 (en) * | 2022-08-29 | 2024-03-01 | Metso Outotec Finland Oy | A method for recovering lithium from a stream containing lithium |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3859427A (en) * | 1969-11-10 | 1975-01-07 | Aluminum Co Of America | Production of beta alumina |
| US3878296A (en) * | 1971-08-18 | 1975-04-15 | United Aircraft Corp | Reaction of lithium carbonate and fibrous aluminum oxide to produce lithium aluminate |
| US4029755A (en) * | 1972-02-07 | 1977-06-14 | The United States Of America As Represented By The Secretary Of The Army | Transparent ultrafine grained ceramics |
| US3998939A (en) * | 1975-08-20 | 1976-12-21 | Institute Of Gas Technology | Production of beta-lithium aluminate (LiAlO2) |
-
1977
- 1977-03-16 DE DE19772711420 patent/DE2711420A1/de active Granted
-
1978
- 1978-03-14 US US05/886,365 patent/US4164557A/en not_active Expired - Lifetime
- 1978-03-15 CA CA298,964A patent/CA1086920A/en not_active Expired
- 1978-03-16 JP JP53030506A patent/JPS608971B2/ja not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| US4164557A (en) | 1979-08-14 |
| DE2711420A1 (de) | 1978-09-21 |
| CA1086920A (en) | 1980-10-07 |
| JPS53140300A (en) | 1978-12-07 |
| DE2711420C2 (enExample) | 1988-01-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPS608971B2 (ja) | β‐リチウムアルミネ−トの製法 | |
| CN102275987A (zh) | 一种纳微米级板片碳酸氧铋材料及其制备方法 | |
| CN101570348A (zh) | 一种致密晶型氢氧化钴的制备方法 | |
| KR102097728B1 (ko) | 왕겨 또는 왕겨재를 이용한 물유리의 제조방법 | |
| CN113105246B (zh) | 一种一步升温碳热还原氮化快速制备纯相AlON细粉的方法 | |
| CN101279758A (zh) | 纳米氧化铜粉体的制备方法 | |
| CN105111189B (zh) | 一种泮托拉唑钠化合物一水合物球形晶体及其制备方法 | |
| KR100367839B1 (ko) | 초본류 식물로 부터 실리카를 추출하는 방법 | |
| CN114477247A (zh) | 一种微波诱导燃烧合成纳米氧化镁的方法 | |
| JP2683389B2 (ja) | 薄片状酸化亜鉛粉末及びその製造法 | |
| CN112777617B (zh) | 一种工业级氢氧化镁微波法制备阻燃剂用氢氧化镁的方法 | |
| CN101186300A (zh) | 微波辐照制备钛硅化合物及其掺杂材料的方法 | |
| CN109607559B (zh) | 一种采用金属粉助熔剂合成三元层状化合物的方法 | |
| CN117385469A (zh) | 一种利用天然石膏制备α-半水石膏晶种的方法 | |
| CN105540651B (zh) | 一种制备球形氧化亚锡纳米材料的方法 | |
| CN115676830A (zh) | 一种碳化锆粉体的制备方法 | |
| CN100376508C (zh) | 制备掺钕钆镓石榴石纳米粉的凝胶燃烧合成方法 | |
| CN115403560B (zh) | 一种艾普拉唑镁晶型及其制备方法 | |
| CN102583295A (zh) | 一种液相制备无碳球形纳米磷酸铁锂的方法 | |
| JPS63500097A (ja) | クロロタロニルの製造方法 | |
| JPH09137152A (ja) | 紫外線吸収剤 | |
| JPH0229606B2 (enExample) | ||
| JPS59227723A (ja) | スズ酸鉛微粒子の製造方法 | |
| JPH0262487B2 (enExample) | ||
| CN116332211B (zh) | 一种低晶粒、高活性、球状体薄水铝石的制备方法 |