DE2635397C3 - Stromlos arbeitende Verkupferungsbäder - Google Patents
Stromlos arbeitende VerkupferungsbäderInfo
- Publication number
- DE2635397C3 DE2635397C3 DE2635397A DE2635397A DE2635397C3 DE 2635397 C3 DE2635397 C3 DE 2635397C3 DE 2635397 A DE2635397 A DE 2635397A DE 2635397 A DE2635397 A DE 2635397A DE 2635397 C3 DE2635397 C3 DE 2635397C3
- Authority
- DE
- Germany
- Prior art keywords
- copper plating
- bath
- compound
- formaldehyde
- electroless copper
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910052802 copper Inorganic materials 0.000 title claims description 17
- 239000010949 copper Substances 0.000 title claims description 17
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 title claims description 16
- 238000007747 plating Methods 0.000 title claims description 13
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 25
- 150000001875 compounds Chemical class 0.000 claims description 10
- 150000002500 ions Chemical class 0.000 claims description 6
- -1 aromatic nitro compound Chemical class 0.000 claims description 5
- 239000000654 additive Substances 0.000 claims description 3
- 230000000996 additive effect Effects 0.000 claims description 3
- 230000008021 deposition Effects 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 125000002768 hydroxyalkyl group Chemical group 0.000 claims description 2
- IQZPDFORWZTSKT-UHFFFAOYSA-N nitrosulphonic acid Chemical compound OS(=O)(=O)[N+]([O-])=O IQZPDFORWZTSKT-UHFFFAOYSA-N 0.000 claims description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims description 2
- 125000003545 alkoxy group Chemical group 0.000 claims 1
- 125000002947 alkylene group Chemical group 0.000 claims 1
- 229920001515 polyalkylene glycol Polymers 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- LQNUZADURLCDLV-UHFFFAOYSA-N nitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC=C1 LQNUZADURLCDLV-UHFFFAOYSA-N 0.000 description 3
- 150000005181 nitrobenzenes Chemical class 0.000 description 3
- JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 description 2
- 229920013816 TRITON QS-44 Polymers 0.000 description 2
- 239000003638 chemical reducing agent Substances 0.000 description 2
- 239000008139 complexing agent Substances 0.000 description 2
- 150000001879 copper Chemical class 0.000 description 2
- 229910001431 copper ion Inorganic materials 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 150000002828 nitro derivatives Chemical class 0.000 description 2
- LJCNRYVRMXRIQR-OLXYHTOASA-L potassium sodium L-tartrate Chemical compound [Na+].[K+].[O-]C(=O)[C@H](O)[C@@H](O)C([O-])=O LJCNRYVRMXRIQR-OLXYHTOASA-L 0.000 description 2
- 125000001424 substituent group Chemical group 0.000 description 2
- WDCYWAQPCXBPJA-UHFFFAOYSA-N 1,3-dinitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC([N+]([O-])=O)=C1 WDCYWAQPCXBPJA-UHFFFAOYSA-N 0.000 description 1
- CMWKITSNTDAEDT-UHFFFAOYSA-N 2-nitrobenzaldehyde Chemical compound [O-][N+](=O)C1=CC=CC=C1C=O CMWKITSNTDAEDT-UHFFFAOYSA-N 0.000 description 1
- ZETIVVHRRQLWFW-UHFFFAOYSA-N 3-nitrobenzaldehyde Chemical compound [O-][N+](=O)C1=CC=CC(C=O)=C1 ZETIVVHRRQLWFW-UHFFFAOYSA-N 0.000 description 1
- BXRFQSNOROATLV-UHFFFAOYSA-N 4-nitrobenzaldehyde Chemical compound [O-][N+](=O)C1=CC=C(C=O)C=C1 BXRFQSNOROATLV-UHFFFAOYSA-N 0.000 description 1
- ZPTVNYMJQHSSEA-UHFFFAOYSA-N 4-nitrotoluene Chemical compound CC1=CC=C([N+]([O-])=O)C=C1 ZPTVNYMJQHSSEA-UHFFFAOYSA-N 0.000 description 1
- ONMOULMPIIOVTQ-UHFFFAOYSA-N 98-47-5 Chemical compound OS(=O)(=O)C1=CC=CC([N+]([O-])=O)=C1 ONMOULMPIIOVTQ-UHFFFAOYSA-N 0.000 description 1
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 1
- 101150003085 Pdcl gene Proteins 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000009918 complex formation Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- LCCNCVORNKJIRZ-UHFFFAOYSA-N parathion Chemical compound CCOP(=S)(OCC)OC1=CC=C([N+]([O-])=O)C=C1 LCCNCVORNKJIRZ-UHFFFAOYSA-N 0.000 description 1
- 229920000233 poly(alkylene oxides) Polymers 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 235000011006 sodium potassium tartrate Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
- C23C18/31—Coating with metals
- C23C18/38—Coating with copper
- C23C18/40—Coating with copper using reducing agents
- C23C18/405—Formaldehyde
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemically Coating (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL7509824.A NL164906C (nl) | 1975-08-19 | 1975-08-19 | Werkwijze voor de bereiding van een waterig alkalische verkoperbad. |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2635397A1 DE2635397A1 (de) | 1977-02-24 |
| DE2635397B2 DE2635397B2 (de) | 1978-03-23 |
| DE2635397C3 true DE2635397C3 (de) | 1978-11-16 |
Family
ID=19824317
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2635397A Expired DE2635397C3 (de) | 1975-08-19 | 1976-08-06 | Stromlos arbeitende Verkupferungsbäder |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US4118234A (en:Method) |
| JP (1) | JPS5224939A (en:Method) |
| AR (1) | AR221469A1 (en:Method) |
| AT (1) | AT345057B (en:Method) |
| AU (1) | AU501210B2 (en:Method) |
| BE (1) | BE845254A (en:Method) |
| BR (1) | BR7605351A (en:Method) |
| CA (1) | CA1067652A (en:Method) |
| CH (1) | CH624994A5 (en:Method) |
| DE (1) | DE2635397C3 (en:Method) |
| FR (1) | FR2321551A1 (en:Method) |
| GB (1) | GB1521364A (en:Method) |
| HK (1) | HK42179A (en:Method) |
| IT (1) | IT1066104B (en:Method) |
| NL (1) | NL164906C (en:Method) |
| SE (1) | SE430615B (en:Method) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4229218A (en) * | 1979-02-05 | 1980-10-21 | Shipley Company Inc. | Self-monitoring electroless plating solution |
| US4666858A (en) * | 1984-10-22 | 1987-05-19 | International Business Machines Corporation | Determination of amount of anionic material in a liquid sample |
| US4857233A (en) * | 1988-05-26 | 1989-08-15 | Potters Industries, Inc. | Nickel particle plating system |
| US5130168A (en) * | 1988-11-22 | 1992-07-14 | Technic, Inc. | Electroless gold plating bath and method of using same |
| JP4482744B2 (ja) * | 2001-02-23 | 2010-06-16 | 株式会社日立製作所 | 無電解銅めっき液、無電解銅めっき方法、配線板の製造方法 |
| PE20211337A1 (es) | 2014-01-31 | 2021-07-26 | Goldcorp Inc | Proceso para la separacion y recuperacion de sulfuros de metales de una mena o concentrado de sulfuros mixtos |
| CN106460182B (zh) * | 2014-04-10 | 2019-07-09 | 安美特德国有限公司 | 镀浴组合物和用于钯的无电镀覆的方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1266099B (de) * | 1965-02-20 | 1968-04-11 | Schering Ag | Bad fuer die reduktive Kupferabscheidung |
| US3649350A (en) * | 1970-06-29 | 1972-03-14 | Gen Electric | Electroless copper plating |
| US3708329A (en) * | 1971-09-10 | 1973-01-02 | Bell Telephone Labor Inc | Electroless copper plating |
| BE794048A (fr) * | 1972-01-17 | 1973-07-16 | Dynachem Corp | Procede et solution de revetement de cuivre sans traitement electrique |
-
1975
- 1975-08-19 NL NL7509824.A patent/NL164906C/xx not_active IP Right Cessation
-
1976
- 1976-08-06 DE DE2635397A patent/DE2635397C3/de not_active Expired
- 1976-08-13 AR AR264333A patent/AR221469A1/es active
- 1976-08-13 US US05/714,111 patent/US4118234A/en not_active Expired - Lifetime
- 1976-08-16 SE SE7609126A patent/SE430615B/xx not_active IP Right Cessation
- 1976-08-16 CH CH1041976A patent/CH624994A5/de not_active IP Right Cessation
- 1976-08-16 AU AU16861/76A patent/AU501210B2/en not_active Expired
- 1976-08-16 CA CA259,187A patent/CA1067652A/en not_active Expired
- 1976-08-16 AT AT608876A patent/AT345057B/de not_active IP Right Cessation
- 1976-08-16 GB GB33998/76A patent/GB1521364A/en not_active Expired
- 1976-08-16 IT IT50910/76A patent/IT1066104B/it active
- 1976-08-16 BR BR7605351A patent/BR7605351A/pt unknown
- 1976-08-17 BE BE169864A patent/BE845254A/xx not_active IP Right Cessation
- 1976-08-17 JP JP51097490A patent/JPS5224939A/ja active Granted
- 1976-08-18 FR FR7625075A patent/FR2321551A1/fr active Granted
-
1979
- 1979-06-28 HK HK421/79A patent/HK42179A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CH624994A5 (en:Method) | 1981-08-31 |
| NL7509824A (nl) | 1977-02-22 |
| NL164906C (nl) | 1981-02-16 |
| FR2321551B1 (en:Method) | 1980-05-23 |
| AU1686176A (en) | 1978-02-23 |
| FR2321551A1 (fr) | 1977-03-18 |
| BR7605351A (pt) | 1977-08-16 |
| SE7609126L (sv) | 1977-02-20 |
| CA1067652A (en) | 1979-12-11 |
| AR221469A1 (es) | 1981-02-13 |
| SE430615B (sv) | 1983-11-28 |
| AT345057B (de) | 1978-08-25 |
| DE2635397A1 (de) | 1977-02-24 |
| DE2635397B2 (de) | 1978-03-23 |
| HK42179A (en) | 1979-07-06 |
| ATA608876A (de) | 1977-12-15 |
| JPS5224939A (en) | 1977-02-24 |
| US4118234A (en) | 1978-10-03 |
| GB1521364A (en) | 1978-08-16 |
| BE845254A (fr) | 1977-02-17 |
| JPS5344405B2 (en:Method) | 1978-11-29 |
| NL164906B (nl) | 1980-09-15 |
| IT1066104B (it) | 1985-03-04 |
| AU501210B2 (en) | 1979-06-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |