DE1919603A1 - Verfahren zum Haerten von photographischen lichtempfindlichen Halogensilberelementen - Google Patents
Verfahren zum Haerten von photographischen lichtempfindlichen HalogensilberelementenInfo
- Publication number
- DE1919603A1 DE1919603A1 DE19691919603 DE1919603A DE1919603A1 DE 1919603 A1 DE1919603 A1 DE 1919603A1 DE 19691919603 DE19691919603 DE 19691919603 DE 1919603 A DE1919603 A DE 1919603A DE 1919603 A1 DE1919603 A1 DE 1919603A1
- Authority
- DE
- Germany
- Prior art keywords
- hardening
- treatment
- photographic
- curing
- photographic photosensitive
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 13
- 229910052709 silver Inorganic materials 0.000 title claims description 9
- 239000004332 silver Substances 0.000 title claims description 9
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 title claims description 7
- 229910052736 halogen Inorganic materials 0.000 title description 5
- 150000002367 halogens Chemical class 0.000 title description 5
- 238000011282 treatment Methods 0.000 claims description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- ZNZYKNKBJPZETN-WELNAUFTSA-N Dialdehyde 11678 Chemical compound N1C2=CC=CC=C2C2=C1[C@H](C[C@H](/C(=C/O)C(=O)OC)[C@@H](C=C)C=O)NCC2 ZNZYKNKBJPZETN-WELNAUFTSA-N 0.000 claims description 7
- NRUVTHFIADHCGM-UHFFFAOYSA-N 2,4-diformylbenzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC=C(C=O)C=C1C=O NRUVTHFIADHCGM-UHFFFAOYSA-N 0.000 claims description 5
- 125000003118 aryl group Chemical group 0.000 claims description 5
- IZALUMVGBVKPJD-UHFFFAOYSA-N benzene-1,3-dicarbaldehyde Chemical compound O=CC1=CC=CC(C=O)=C1 IZALUMVGBVKPJD-UHFFFAOYSA-N 0.000 claims description 5
- -1 silver halide Chemical class 0.000 claims description 4
- MFXUVYUPPKVYPH-UHFFFAOYSA-N 4,6-dimethylbenzene-1,3-dicarbaldehyde Chemical compound CC1=CC(C)=C(C=O)C=C1C=O MFXUVYUPPKVYPH-UHFFFAOYSA-N 0.000 claims description 3
- 150000004820 halides Chemical class 0.000 claims description 3
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- KVOOQCGWOPDWCB-UHFFFAOYSA-N 4,6-diformylbenzene-1,3-dicarboxylic acid Chemical compound OC(=O)C1=CC(C(O)=O)=C(C=O)C=C1C=O KVOOQCGWOPDWCB-UHFFFAOYSA-N 0.000 claims 1
- UWLVWAQSMOVZKN-UHFFFAOYSA-N 5-methylbenzene-1,3-dicarbaldehyde Chemical compound CC1=CC(C=O)=CC(C=O)=C1 UWLVWAQSMOVZKN-UHFFFAOYSA-N 0.000 claims 1
- 239000000839 emulsion Substances 0.000 description 17
- 239000000243 solution Substances 0.000 description 17
- 125000002485 formyl group Chemical group [H]C(*)=O 0.000 description 12
- 239000003795 chemical substances by application Substances 0.000 description 11
- 238000001723 curing Methods 0.000 description 10
- IOLCXVTUBQKXJR-UHFFFAOYSA-M potassium bromide Chemical compound [K+].[Br-] IOLCXVTUBQKXJR-UHFFFAOYSA-M 0.000 description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 150000001299 aldehydes Chemical class 0.000 description 8
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 8
- 239000000203 mixture Substances 0.000 description 7
- 238000005406 washing Methods 0.000 description 7
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 6
- 239000004848 polyfunctional curative Substances 0.000 description 5
- 235000010265 sodium sulphite Nutrition 0.000 description 4
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 3
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Chemical compound [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 description 3
- 230000009291 secondary effect Effects 0.000 description 3
- 239000001632 sodium acetate Substances 0.000 description 3
- 235000017281 sodium acetate Nutrition 0.000 description 3
- 229910052938 sodium sulfate Inorganic materials 0.000 description 3
- 235000011152 sodium sulphate Nutrition 0.000 description 3
- ZVNPWFOVUDMGRP-UHFFFAOYSA-N 4-methylaminophenol sulfate Chemical compound OS(O)(=O)=O.CNC1=CC=C(O)C=C1.CNC1=CC=C(O)C=C1 ZVNPWFOVUDMGRP-UHFFFAOYSA-N 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 2
- WTDHULULXKLSOZ-UHFFFAOYSA-N Hydroxylamine hydrochloride Chemical compound Cl.ON WTDHULULXKLSOZ-UHFFFAOYSA-N 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000007844 bleaching agent Substances 0.000 description 2
- 238000004132 cross linking Methods 0.000 description 2
- 235000021317 phosphate Nutrition 0.000 description 2
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- ALWXETURCOIGIZ-UHFFFAOYSA-N 1-nitropropylbenzene Chemical compound CCC([N+]([O-])=O)C1=CC=CC=C1 ALWXETURCOIGIZ-UHFFFAOYSA-N 0.000 description 1
- QHRPBXABWLRILP-UHFFFAOYSA-N 4,6-dihydroxybenzene-1,3-dicarbaldehyde Chemical compound OC1=CC(O)=C(C=O)C=C1C=O QHRPBXABWLRILP-UHFFFAOYSA-N 0.000 description 1
- XPAZGLFMMUODDK-UHFFFAOYSA-N 6-nitro-1h-benzimidazole Chemical compound [O-][N+](=O)C1=CC=C2N=CNC2=C1 XPAZGLFMMUODDK-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 229960000583 acetic acid Drugs 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 235000011126 aluminium potassium sulphate Nutrition 0.000 description 1
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical class [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 1
- 235000019445 benzyl alcohol Nutrition 0.000 description 1
- 229910021538 borax Inorganic materials 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- JJCFRYNCJDLXIK-UHFFFAOYSA-N cyproheptadine Chemical compound C1CN(C)CCC1=C1C2=CC=CC=C2C=CC2=CC=CC=C21 JJCFRYNCJDLXIK-UHFFFAOYSA-N 0.000 description 1
- MQRJBSHKWOFOGF-UHFFFAOYSA-L disodium;carbonate;hydrate Chemical compound O.[Na+].[Na+].[O-]C([O-])=O MQRJBSHKWOFOGF-UHFFFAOYSA-L 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000012362 glacial acetic acid Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 125000000896 monocarboxylic acid group Chemical group 0.000 description 1
- 230000006855 networking Effects 0.000 description 1
- ZWLUXSQADUDCSB-UHFFFAOYSA-N phthalaldehyde Chemical compound O=CC1=CC=CC=C1C=O ZWLUXSQADUDCSB-UHFFFAOYSA-N 0.000 description 1
- 229940050271 potassium alum Drugs 0.000 description 1
- GRLPQNLYRHEGIJ-UHFFFAOYSA-J potassium aluminium sulfate Chemical compound [Al+3].[K+].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O GRLPQNLYRHEGIJ-UHFFFAOYSA-J 0.000 description 1
- 230000002250 progressing effect Effects 0.000 description 1
- 239000003223 protective agent Substances 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Substances [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 235000010339 sodium tetraborate Nutrition 0.000 description 1
- AKHNMLFCWUSKQB-UHFFFAOYSA-L sodium thiosulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=S AKHNMLFCWUSKQB-UHFFFAOYSA-L 0.000 description 1
- 235000019345 sodium thiosulphate Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- BSVBQGMMJUBVOD-UHFFFAOYSA-N trisodium borate Chemical compound [Na+].[Na+].[Na+].[O-]B([O-])[O-] BSVBQGMMJUBVOD-UHFFFAOYSA-N 0.000 description 1
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C5/00—Photographic processes or agents therefor; Regeneration of such processing agents
- G03C5/26—Processes using silver-salt-containing photosensitive materials or agents therefor
- G03C5/29—Development processes or agents therefor
- G03C5/305—Additives other than developers
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/06—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein with non-macromolecular additives
- G03C1/30—Hardeners
- G03C1/301—Aldehydes or derivatives thereof, e.g. bisulfite addition products
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C5/00—Photographic processes or agents therefor; Regeneration of such processing agents
- G03C5/26—Processes using silver-salt-containing photosensitive materials or agents therefor
- G03C5/268—Processing baths not provided for elsewhere, e.g. pre-treatment, stop, intermediate or rinse baths
Landscapes
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Silver Salt Photography Or Processing Solution Therefor (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2634168 | 1968-04-19 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1919603A1 true DE1919603A1 (de) | 1969-10-30 |
Family
ID=12190721
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19691919603 Pending DE1919603A1 (de) | 1968-04-19 | 1969-04-17 | Verfahren zum Haerten von photographischen lichtempfindlichen Halogensilberelementen |
| DE19691919604 Pending DE1919604A1 (de) | 1968-04-19 | 1969-04-17 | Verfahren zum Haerten eines photographischen lichtempfindlichen Halogensilberelements |
| DE19691919592 Pending DE1919592A1 (de) | 1968-04-19 | 1969-04-17 | Verfahren zum Haerten eines photographischen lichtempfindlichen Halogensilberelementes |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19691919604 Pending DE1919604A1 (de) | 1968-04-19 | 1969-04-17 | Verfahren zum Haerten eines photographischen lichtempfindlichen Halogensilberelements |
| DE19691919592 Pending DE1919592A1 (de) | 1968-04-19 | 1969-04-17 | Verfahren zum Haerten eines photographischen lichtempfindlichen Halogensilberelementes |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3677760A (enrdf_load_stackoverflow) |
| BE (1) | BE731638A (enrdf_load_stackoverflow) |
| DE (3) | DE1919603A1 (enrdf_load_stackoverflow) |
| FR (1) | FR2006527A1 (enrdf_load_stackoverflow) |
| GB (3) | GB1238574A (enrdf_load_stackoverflow) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3989529A (en) * | 1974-10-29 | 1976-11-02 | Gaf Corporation | Hydrophilic coupler solutions |
| US5424177A (en) * | 1991-07-05 | 1995-06-13 | Konica Corporation | Stabilizer for silver halide color photographic light-sensitive materials and its concentrated composition, and processing method using said stabilizer |
| US5441852A (en) * | 1991-12-27 | 1995-08-15 | Konica Corporation | Method of stabilizing a color silver halide image |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1590126B1 (de) * | 1966-06-22 | 1970-10-08 | Bbc Brown Boveri & Cie | Elektrisches Installationsgeraet,insbesondere Wippen- oder Tastschalter |
| US3994729A (en) * | 1973-04-06 | 1976-11-30 | Fuji Photo Film Co., Ltd. | Method for processing photographic light-sensitive material |
| GB1550356A (en) * | 1975-05-01 | 1979-08-15 | Agfa Gevaert | Hardening developers for silver halide photography |
| US4247625A (en) * | 1978-12-20 | 1981-01-27 | Eastman Kodak Company | Imaging processes, elements and compositions featuring dye-retaining binders for reaction products of cobalt complexes and aromatic dialdehyde |
| CH642479A5 (en) * | 1979-04-05 | 1984-04-13 | Feller Ag | Push-button switch having a small lamp for visual switch marking |
-
1969
- 1969-04-17 BE BE731638D patent/BE731638A/xx unknown
- 1969-04-17 DE DE19691919603 patent/DE1919603A1/de active Pending
- 1969-04-17 DE DE19691919604 patent/DE1919604A1/de active Pending
- 1969-04-17 FR FR6911951A patent/FR2006527A1/fr not_active Withdrawn
- 1969-04-17 DE DE19691919592 patent/DE1919592A1/de active Pending
- 1969-04-21 GB GB1238574D patent/GB1238574A/en not_active Expired
- 1969-04-21 GB GB1238573D patent/GB1238573A/en not_active Expired
- 1969-04-21 US US818101A patent/US3677760A/en not_active Expired - Lifetime
- 1969-04-21 GB GB1238572D patent/GB1238572A/en not_active Expired
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3989529A (en) * | 1974-10-29 | 1976-11-02 | Gaf Corporation | Hydrophilic coupler solutions |
| US5424177A (en) * | 1991-07-05 | 1995-06-13 | Konica Corporation | Stabilizer for silver halide color photographic light-sensitive materials and its concentrated composition, and processing method using said stabilizer |
| US5441852A (en) * | 1991-12-27 | 1995-08-15 | Konica Corporation | Method of stabilizing a color silver halide image |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2006527A1 (enrdf_load_stackoverflow) | 1969-12-26 |
| DE1919592A1 (de) | 1969-10-30 |
| DE1919604A1 (de) | 1969-10-30 |
| US3677760A (en) | 1972-07-18 |
| GB1238574A (enrdf_load_stackoverflow) | 1971-07-07 |
| GB1238573A (enrdf_load_stackoverflow) | 1971-07-07 |
| GB1238572A (enrdf_load_stackoverflow) | 1971-07-07 |
| BE731638A (enrdf_load_stackoverflow) | 1969-10-01 |
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