DE1243945B - Loesungen und Verfahren zur Phosphatierung von Zink und Zinklegierungen - Google Patents
Loesungen und Verfahren zur Phosphatierung von Zink und ZinklegierungenInfo
- Publication number
- DE1243945B DE1243945B DEA42007A DEA0042007A DE1243945B DE 1243945 B DE1243945 B DE 1243945B DE A42007 A DEA42007 A DE A42007A DE A0042007 A DEA0042007 A DE A0042007A DE 1243945 B DE1243945 B DE 1243945B
- Authority
- DE
- Germany
- Prior art keywords
- percent
- weight
- zinc
- solutions
- solutions according
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 title claims description 13
- 229910052725 zinc Inorganic materials 0.000 title claims description 13
- 239000011701 zinc Substances 0.000 title claims description 13
- 229910001297 Zn alloy Inorganic materials 0.000 title claims description 6
- 238000000034 method Methods 0.000 title claims description 6
- 238000000576 coating method Methods 0.000 claims description 15
- 239000002253 acid Substances 0.000 claims description 12
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 claims description 10
- 150000003839 salts Chemical class 0.000 claims description 9
- 229910002651 NO3 Inorganic materials 0.000 claims description 8
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 7
- XYZZKVRWGOWVGO-UHFFFAOYSA-N Glycerol-phosphate Chemical compound OP(O)(O)=O.OCC(O)CO XYZZKVRWGOWVGO-UHFFFAOYSA-N 0.000 claims description 6
- 229910019142 PO4 Inorganic materials 0.000 claims description 6
- 229910052751 metal Inorganic materials 0.000 claims description 6
- 239000002184 metal Substances 0.000 claims description 6
- 239000010452 phosphate Substances 0.000 claims description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 5
- LRXTYHSAJDENHV-UHFFFAOYSA-H zinc phosphate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LRXTYHSAJDENHV-UHFFFAOYSA-H 0.000 claims description 4
- 229910000165 zinc phosphate Inorganic materials 0.000 claims description 4
- 229910001431 copper ion Inorganic materials 0.000 claims description 3
- JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 claims description 2
- VEQPNABPJHWNSG-UHFFFAOYSA-N Nickel(2+) Chemical compound [Ni+2] VEQPNABPJHWNSG-UHFFFAOYSA-N 0.000 claims description 2
- 230000002378 acidificating effect Effects 0.000 claims description 2
- 229910001453 nickel ion Inorganic materials 0.000 claims description 2
- -1 nitrate ions Chemical class 0.000 claims 2
- 239000000243 solution Substances 0.000 description 31
- AWUCVROLDVIAJX-UHFFFAOYSA-N alpha-glycerophosphate Natural products OCC(O)COP(O)(O)=O AWUCVROLDVIAJX-UHFFFAOYSA-N 0.000 description 8
- 239000003973 paint Substances 0.000 description 8
- AWUCVROLDVIAJX-GSVOUGTGSA-N sn-glycerol 3-phosphate Chemical compound OC[C@@H](O)COP(O)(O)=O AWUCVROLDVIAJX-GSVOUGTGSA-N 0.000 description 8
- 239000011248 coating agent Substances 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 5
- 239000012141 concentrate Substances 0.000 description 5
- 150000002222 fluorine compounds Chemical class 0.000 description 5
- IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 238000005452 bending Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 229910001385 heavy metal Inorganic materials 0.000 description 2
- 229910052759 nickel Inorganic materials 0.000 description 2
- 239000007800 oxidant agent Substances 0.000 description 2
- KJFMBFZCATUALV-UHFFFAOYSA-N phenolphthalein Chemical compound C1=CC(O)=CC=C1C1(C=2C=CC(O)=CC=2)C2=CC=CC=C2C(=O)O1 KJFMBFZCATUALV-UHFFFAOYSA-N 0.000 description 2
- RILZRCJGXSFXNE-UHFFFAOYSA-N 2-[4-(trifluoromethoxy)phenyl]ethanol Chemical compound OCCC1=CC=C(OC(F)(F)F)C=C1 RILZRCJGXSFXNE-UHFFFAOYSA-N 0.000 description 1
- MKNQNPYGAQGARI-UHFFFAOYSA-N 4-(bromomethyl)phenol Chemical compound OC1=CC=C(CBr)C=C1 MKNQNPYGAQGARI-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- 229910001335 Galvanized steel Inorganic materials 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 1
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- PTFCDOFLOPIGGS-UHFFFAOYSA-N Zinc dication Chemical compound [Zn+2] PTFCDOFLOPIGGS-UHFFFAOYSA-N 0.000 description 1
- RUXCWHQDIMWELV-UHFFFAOYSA-L [Zn+2].P(=O)([O-])(O)O.[F-] Chemical compound [Zn+2].P(=O)([O-])(O)O.[F-] RUXCWHQDIMWELV-UHFFFAOYSA-L 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001447 alkali salts Chemical class 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 239000008397 galvanized steel Substances 0.000 description 1
- 150000002315 glycerophosphates Chemical class 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000002816 nickel compounds Chemical class 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 230000004580 weight loss Effects 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 239000012224 working solution Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
- C23C22/36—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates
- C23C22/362—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates containing also zinc cations
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Treatment Of Metals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US169997A US3109757A (en) | 1962-01-26 | 1962-01-26 | Method and material for applying phosphate conversion coatings on zinciferous surfaces |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1243945B true DE1243945B (de) | 1967-07-06 |
Family
ID=22618092
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEA42007A Pending DE1243945B (de) | 1962-01-26 | 1962-12-31 | Loesungen und Verfahren zur Phosphatierung von Zink und Zinklegierungen |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3109757A (en, 2012) |
| BE (1) | BE627337A (en, 2012) |
| DE (1) | DE1243945B (en, 2012) |
| GB (1) | GB957379A (en, 2012) |
| NL (2) | NL120662C (en, 2012) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102010025707A1 (de) | 2010-06-30 | 2012-01-05 | Rheinzink Gmbh & Co. Kg | Verfahren zur Herstellung von Schutzschichten auf Flacherzeugnissen aus Titanzink |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3269876A (en) * | 1962-12-13 | 1966-08-30 | Rheem Mfg Co | Glass-coated steel article |
| US3467589A (en) * | 1966-10-19 | 1969-09-16 | Hooker Chemical Corp | Method of forming a copper containing protective coating prior to electrodeposition of paint |
| US3540943A (en) * | 1968-08-08 | 1970-11-17 | United States Steel Corp | Method of making galvannealed ferrous metal of improved solderability |
| US3819424A (en) * | 1971-06-17 | 1974-06-25 | Oxy Metal Finishing Corp | Method and composition for treating metal surfaces |
| US4148670A (en) * | 1976-04-05 | 1979-04-10 | Amchem Products, Inc. | Coating solution for metal surface |
| US4427459A (en) | 1982-01-25 | 1984-01-24 | Pennwalt Corporation | Phosphate conversion coatings for metals with reduced coating weights and crystal sizes |
| JPS6148597A (ja) * | 1984-08-14 | 1986-03-10 | Nippon Paint Co Ltd | リン酸亜鉛化成処理法 |
| USRE35958E (en) * | 1985-08-26 | 1998-11-17 | Henkel Corporation | Method of forming phosphate coating on zinc |
| US4595424A (en) * | 1985-08-26 | 1986-06-17 | Parker Chemical Company | Method of forming phosphate coating on zinc |
| US5082511A (en) * | 1989-09-07 | 1992-01-21 | Henkel Corporation | Protective coating processes for zinc coated steel |
| US6551417B1 (en) | 2000-09-20 | 2003-04-22 | Ge Betz, Inc. | Tri-cation zinc phosphate conversion coating and process of making the same |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE707865C (de) * | 1939-07-15 | 1941-07-05 | I G Farbenindustrie Akt Ges | Verfahren zur Rostschutzbehandlung von Eisen und Stahl |
| US2487137A (en) * | 1947-09-10 | 1949-11-08 | Armco Steel Corp | Producing coatings on metal |
| DE853698C (de) * | 1947-05-12 | 1952-10-27 | Parker Rust Proof Company | Verfahren zur Herstellung von Phosphatueberzuegen auf Zink |
| DE853695C (de) * | 1946-09-11 | 1952-10-27 | Parker Rust Proof Company | Verfahren zur Herstellung von Phosphatueberzuegen auf Metallen |
| DE1053279B (de) | 1952-06-18 | 1959-03-19 | Walterisation Company Ltd | Phosphatierungsgemische zur Herstellung von Phosphatueberzuegen auf Metallflaechen |
-
0
- NL NL288062D patent/NL288062A/xx unknown
- BE BE627337D patent/BE627337A/xx unknown
- NL NL120662D patent/NL120662C/xx active
-
1962
- 1962-01-26 US US169997A patent/US3109757A/en not_active Expired - Lifetime
- 1962-11-08 GB GB42264/62A patent/GB957379A/en not_active Expired
- 1962-12-31 DE DEA42007A patent/DE1243945B/de active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE707865C (de) * | 1939-07-15 | 1941-07-05 | I G Farbenindustrie Akt Ges | Verfahren zur Rostschutzbehandlung von Eisen und Stahl |
| DE853695C (de) * | 1946-09-11 | 1952-10-27 | Parker Rust Proof Company | Verfahren zur Herstellung von Phosphatueberzuegen auf Metallen |
| DE853698C (de) * | 1947-05-12 | 1952-10-27 | Parker Rust Proof Company | Verfahren zur Herstellung von Phosphatueberzuegen auf Zink |
| US2487137A (en) * | 1947-09-10 | 1949-11-08 | Armco Steel Corp | Producing coatings on metal |
| DE1053279B (de) | 1952-06-18 | 1959-03-19 | Walterisation Company Ltd | Phosphatierungsgemische zur Herstellung von Phosphatueberzuegen auf Metallflaechen |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102010025707A1 (de) | 2010-06-30 | 2012-01-05 | Rheinzink Gmbh & Co. Kg | Verfahren zur Herstellung von Schutzschichten auf Flacherzeugnissen aus Titanzink |
Also Published As
| Publication number | Publication date |
|---|---|
| BE627337A (en, 2012) | |
| NL120662C (en, 2012) | |
| NL288062A (en, 2012) | |
| US3109757A (en) | 1963-11-05 |
| GB957379A (en) | 1964-05-06 |
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