DE1142871B - Verfahren zur Herstellung von polyfunktionellen Diazonium-halogeniden - Google Patents
Verfahren zur Herstellung von polyfunktionellen Diazonium-halogenidenInfo
- Publication number
- DE1142871B DE1142871B DEK42717A DEK0042717A DE1142871B DE 1142871 B DE1142871 B DE 1142871B DE K42717 A DEK42717 A DE K42717A DE K0042717 A DEK0042717 A DE K0042717A DE 1142871 B DE1142871 B DE 1142871B
- Authority
- DE
- Germany
- Prior art keywords
- parts
- diazonium
- weight
- diphenylamine
- condensation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000012954 diazonium Substances 0.000 title claims description 26
- 238000000034 method Methods 0.000 title claims description 8
- -1 diazonium halides Chemical class 0.000 title claims description 7
- 238000004519 manufacturing process Methods 0.000 title description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 20
- 239000000203 mixture Substances 0.000 claims description 17
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 12
- 238000009833 condensation Methods 0.000 claims description 12
- 230000005494 condensation Effects 0.000 claims description 12
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 9
- 150000003839 salts Chemical class 0.000 claims description 7
- BMYNFMYTOJXKLE-UHFFFAOYSA-N 3-azaniumyl-2-hydroxypropanoate Chemical compound NCC(O)C(O)=O BMYNFMYTOJXKLE-UHFFFAOYSA-N 0.000 claims description 4
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 4
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 claims description 2
- 230000000737 periodic effect Effects 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 239000007859 condensation product Substances 0.000 description 19
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 12
- 239000002253 acid Substances 0.000 description 10
- 229930040373 Paraformaldehyde Natural products 0.000 description 8
- 238000001704 evaporation Methods 0.000 description 8
- 229920002866 paraformaldehyde Polymers 0.000 description 8
- 230000008020 evaporation Effects 0.000 description 7
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 6
- 230000002378 acidificating effect Effects 0.000 description 6
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 5
- 230000007935 neutral effect Effects 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 150000007513 acids Chemical class 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 150000001989 diazonium salts Chemical class 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- DMBHHRLKUKUOEG-UHFFFAOYSA-N diphenylamine Chemical group C=1C=CC=CC=1NC1=CC=CC=C1 DMBHHRLKUKUOEG-UHFFFAOYSA-N 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 2
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 2
- 150000004820 halides Chemical class 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 235000011118 potassium hydroxide Nutrition 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 2
- FECNOIODIVNEKI-UHFFFAOYSA-N 2-[(2-aminobenzoyl)amino]benzoic acid Chemical class NC1=CC=CC=C1C(=O)NC1=CC=CC=C1C(O)=O FECNOIODIVNEKI-UHFFFAOYSA-N 0.000 description 1
- NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- ICGLOTCMOYCOTB-UHFFFAOYSA-N [Cl].[Zn] Chemical compound [Cl].[Zn] ICGLOTCMOYCOTB-UHFFFAOYSA-N 0.000 description 1
- 150000008043 acidic salts Chemical class 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Inorganic materials 0.000 description 1
- 150000001728 carbonyl compounds Chemical class 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 150000008049 diazo compounds Chemical class 0.000 description 1
- 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 description 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-O diazynium Chemical compound [NH+]#N IJGRMHOSHXDMSA-UHFFFAOYSA-O 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910001507 metal halide Inorganic materials 0.000 description 1
- 150000005309 metal halides Chemical class 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 239000011592 zinc chloride Substances 0.000 description 1
- 235000005074 zinc chloride Nutrition 0.000 description 1
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
- G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
- G03F7/004—Photosensitive materials
- G03F7/016—Diazonium salts or compounds
- G03F7/021—Macromolecular diazonium compounds; Macromolecular additives, e.g. binders
Landscapes
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- General Physics & Mathematics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE613040D BE613040A (en, 2012) | 1961-01-25 | ||
| NL273553D NL273553A (en, 2012) | 1961-01-25 | ||
| DEK42717A DE1142871B (de) | 1961-01-25 | 1961-01-25 | Verfahren zur Herstellung von polyfunktionellen Diazonium-halogeniden |
| DEK44203A DE1154123B (de) | 1961-01-25 | 1961-07-08 | Verfahren zur Herstellung von polyfunktionellen Diazoniumhalogeniden |
| GB1837/62A GB984861A (en) | 1961-01-25 | 1962-01-18 | Process for the preparation of polyfunctional diazonium halides |
| CH87462A CH398632A (de) | 1961-01-25 | 1962-01-24 | Verfahren zur Herstellung von polyfunktionellen Diazoniumhalogeniden |
| FR885766A FR1312770A (fr) | 1961-01-25 | 1962-01-24 | Procédé de préparation d'halogénures de diazonium polyfonctionnels |
| US207800A US3277074A (en) | 1961-01-25 | 1962-07-05 | Method for the preparation of polyfunctional diazonium halides |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEK42717A DE1142871B (de) | 1961-01-25 | 1961-01-25 | Verfahren zur Herstellung von polyfunktionellen Diazonium-halogeniden |
| DEK44203A DE1154123B (de) | 1961-01-25 | 1961-07-08 | Verfahren zur Herstellung von polyfunktionellen Diazoniumhalogeniden |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1142871B true DE1142871B (de) | 1963-01-31 |
Family
ID=25983354
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEK42717A Pending DE1142871B (de) | 1961-01-25 | 1961-01-25 | Verfahren zur Herstellung von polyfunktionellen Diazonium-halogeniden |
| DEK44203A Pending DE1154123B (de) | 1961-01-25 | 1961-07-08 | Verfahren zur Herstellung von polyfunktionellen Diazoniumhalogeniden |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEK44203A Pending DE1154123B (de) | 1961-01-25 | 1961-07-08 | Verfahren zur Herstellung von polyfunktionellen Diazoniumhalogeniden |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3277074A (en, 2012) |
| BE (1) | BE613040A (en, 2012) |
| CH (1) | CH398632A (en, 2012) |
| DE (2) | DE1142871B (en, 2012) |
| GB (1) | GB984861A (en, 2012) |
| NL (1) | NL273553A (en, 2012) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0268790A2 (de) | 1986-10-17 | 1988-06-01 | Hoechst Aktiengesellschaft | Verfahren zur abtragenden Modifizierung von mehrstufig aufgerauhten Trägermaterialien aus Aluminium oder dessen Legierungen und deren Verwendung bei der Herstellung von Offsetdruckplatten |
| US5755949A (en) * | 1993-12-22 | 1998-05-26 | Agfa-Gevaert Ag | Electrochemical graining method |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2007070694A (ja) * | 2005-09-07 | 2007-03-22 | Konica Minolta Medical & Graphic Inc | 帯状アルミニウム板の陽極酸化処理方法、平版印刷版材料用支持体及び陽極酸化処理装置 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE596731C (de) * | 1932-05-23 | 1934-05-09 | Kalle & Co Akt Ges | Verfahren zur Darstellung von hoehermolekularen Diazoverbindungen |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2679498A (en) * | 1954-05-25 | Atent office | ||
| GB220025A (en) * | 1923-04-27 | 1924-07-28 | Meilach Melamid | Improvements in the process of tanning and in the manufacture of tanning substances |
| US2060573A (en) * | 1932-03-23 | 1936-11-10 | Rohm & Haas | Condensation products of phenols and triisobutylene |
| CH168142A (de) * | 1932-05-23 | 1934-03-31 | Kalle & Co Ag | Verfahren zur Darstellung einer hochmolekularen Diazoverbindung. |
| DE604278C (de) * | 1933-03-07 | 1934-10-18 | I G Farbenindustrie Akt Ges | Verfahren zur Herstellung von Diazoniumverbindungen der 4-Aminodiarylamine |
| US3050502A (en) * | 1959-01-29 | 1962-08-21 | Polychrome Corp | Diazo condensation polymers |
| NL273555A (en, 2012) * | 1961-01-25 |
-
0
- BE BE613040D patent/BE613040A/xx unknown
- NL NL273553D patent/NL273553A/xx unknown
-
1961
- 1961-01-25 DE DEK42717A patent/DE1142871B/de active Pending
- 1961-07-08 DE DEK44203A patent/DE1154123B/de active Pending
-
1962
- 1962-01-18 GB GB1837/62A patent/GB984861A/en not_active Expired
- 1962-01-24 CH CH87462A patent/CH398632A/de unknown
- 1962-07-05 US US207800A patent/US3277074A/en not_active Expired - Lifetime
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE596731C (de) * | 1932-05-23 | 1934-05-09 | Kalle & Co Akt Ges | Verfahren zur Darstellung von hoehermolekularen Diazoverbindungen |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0268790A2 (de) | 1986-10-17 | 1988-06-01 | Hoechst Aktiengesellschaft | Verfahren zur abtragenden Modifizierung von mehrstufig aufgerauhten Trägermaterialien aus Aluminium oder dessen Legierungen und deren Verwendung bei der Herstellung von Offsetdruckplatten |
| US5755949A (en) * | 1993-12-22 | 1998-05-26 | Agfa-Gevaert Ag | Electrochemical graining method |
Also Published As
| Publication number | Publication date |
|---|---|
| US3277074A (en) | 1966-10-04 |
| NL273553A (en, 2012) | |
| CH398632A (de) | 1966-03-15 |
| GB984861A (en) | 1965-03-03 |
| BE613040A (en, 2012) | |
| DE1154123B (de) | 1963-09-12 |
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