DE1059446B - Verfahren zur Herstellung von Thiophosphorsaeureestern - Google Patents
Verfahren zur Herstellung von ThiophosphorsaeureesternInfo
- Publication number
- DE1059446B DE1059446B DEF22735A DEF0022735A DE1059446B DE 1059446 B DE1059446 B DE 1059446B DE F22735 A DEF22735 A DE F22735A DE F0022735 A DEF0022735 A DE F0022735A DE 1059446 B DE1059446 B DE 1059446B
- Authority
- DE
- Germany
- Prior art keywords
- acid esters
- preparation
- solutions
- thiophosphoric acid
- ester
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 4
- 150000003580 thiophosphoric acid esters Chemical class 0.000 title claims description 4
- 238000002360 preparation method Methods 0.000 title description 5
- 239000002253 acid Substances 0.000 claims description 7
- 229910052760 oxygen Inorganic materials 0.000 claims description 3
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 2
- 150000007513 acids Chemical class 0.000 claims description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical group [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 2
- 239000011230 binding agent Substances 0.000 claims description 2
- 239000001301 oxygen Substances 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- 229910052717 sulfur Chemical group 0.000 claims description 2
- 239000011593 sulfur Chemical group 0.000 claims description 2
- -1 cyclohexyl mercapto Chemical class 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 1
- 125000004962 sulfoxyl group Chemical group 0.000 claims 1
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 12
- 150000002148 esters Chemical class 0.000 description 12
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
- 241001124076 Aphididae Species 0.000 description 8
- 230000009885 systemic effect Effects 0.000 description 8
- 241001454295 Tetranychidae Species 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 238000009835 boiling Methods 0.000 description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 241000239290 Araneae Species 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 240000006677 Vicia faba Species 0.000 description 2
- 235000010749 Vicia faba Nutrition 0.000 description 2
- 235000002098 Vicia faba var. major Nutrition 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 230000000749 insecticidal effect Effects 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 238000010626 work up procedure Methods 0.000 description 2
- 241000238876 Acari Species 0.000 description 1
- 241001425390 Aphis fabae Species 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 241000488583 Panonychus ulmi Species 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 241001454293 Tetranychus urticae Species 0.000 description 1
- IBGKZCJDWXXWNU-UHFFFAOYSA-N azane;diethoxy-hydroxy-sulfanylidene-$l^{5}-phosphane Chemical compound [NH4+].CCOP([O-])(=S)OCC IBGKZCJDWXXWNU-UHFFFAOYSA-N 0.000 description 1
- GIUYHMYPEVIYCM-UHFFFAOYSA-N azane;hydroxy-dimethoxy-sulfanylidene-$l^{5}-phosphane Chemical compound [NH4+].COP([O-])(=S)OC GIUYHMYPEVIYCM-UHFFFAOYSA-N 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000012230 colorless oil Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000013601 eggs Nutrition 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
- C07F9/165—Esters of thiophosphoric acids
- C07F9/1651—Esters of thiophosphoric acids with hydroxyalkyl compounds with further substituents on alkyl
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE566416D BE566416A (hu) | 1957-04-04 | ||
| FR1194070D FR1194070A (hu) | 1957-04-04 | ||
| DEF22735A DE1059446B (de) | 1957-04-04 | 1957-04-04 | Verfahren zur Herstellung von Thiophosphorsaeureestern |
| CH5685358A CH380103A (de) | 1957-04-04 | 1958-03-10 | Verfahren zur Herstellung von Thiophosphorsäureestern |
| GB1011858A GB843309A (en) | 1957-04-04 | 1958-03-28 | Thiophosphoric acid esters |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF22735A DE1059446B (de) | 1957-04-04 | 1957-04-04 | Verfahren zur Herstellung von Thiophosphorsaeureestern |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1059446B true DE1059446B (de) | 1959-06-18 |
Family
ID=7090556
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEF22735A Pending DE1059446B (de) | 1957-04-04 | 1957-04-04 | Verfahren zur Herstellung von Thiophosphorsaeureestern |
Country Status (5)
| Country | Link |
|---|---|
| BE (1) | BE566416A (hu) |
| CH (1) | CH380103A (hu) |
| DE (1) | DE1059446B (hu) |
| FR (1) | FR1194070A (hu) |
| GB (1) | GB843309A (hu) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE848041C (de) * | 1949-07-13 | 1952-09-01 | Borchers A G Geb | Verfahren zur Herstellung von Estern der Orthophosphorsaeure und Thiophosphorsaeure |
| DE864252C (de) * | 1950-05-06 | 1953-01-22 | Geigy Ag J R | Verfahren zur Herstellung von Phosphorsaeureestern |
| US2690451A (en) * | 1951-09-28 | 1954-09-28 | Allied Chem & Dye Corp | Method for preparation of sulfur-containing esters of phosphoric acid |
| FR1103577A (fr) * | 1953-04-24 | 1955-11-04 | Ciba Geigy | Composés organiques renfermant du phosphore, procédé pour leur préparation, et utilisation de ces produits dans l'industrie |
-
0
- FR FR1194070D patent/FR1194070A/fr not_active Expired
- BE BE566416D patent/BE566416A/xx unknown
-
1957
- 1957-04-04 DE DEF22735A patent/DE1059446B/de active Pending
-
1958
- 1958-03-10 CH CH5685358A patent/CH380103A/de unknown
- 1958-03-28 GB GB1011858A patent/GB843309A/en not_active Expired
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE848041C (de) * | 1949-07-13 | 1952-09-01 | Borchers A G Geb | Verfahren zur Herstellung von Estern der Orthophosphorsaeure und Thiophosphorsaeure |
| DE864252C (de) * | 1950-05-06 | 1953-01-22 | Geigy Ag J R | Verfahren zur Herstellung von Phosphorsaeureestern |
| US2690451A (en) * | 1951-09-28 | 1954-09-28 | Allied Chem & Dye Corp | Method for preparation of sulfur-containing esters of phosphoric acid |
| FR1103577A (fr) * | 1953-04-24 | 1955-11-04 | Ciba Geigy | Composés organiques renfermant du phosphore, procédé pour leur préparation, et utilisation de ces produits dans l'industrie |
Also Published As
| Publication number | Publication date |
|---|---|
| FR1194070A (hu) | 1959-11-06 |
| CH380103A (de) | 1964-07-31 |
| BE566416A (hu) | |
| GB843309A (en) | 1960-08-04 |
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