CN107137263A - A kind of anti-ageing face mask liquid and preparation method thereof - Google Patents
A kind of anti-ageing face mask liquid and preparation method thereof Download PDFInfo
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A61Q19/08—Anti-ageing preparations
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
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- A61K2800/524—Preservatives
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Abstract
The invention discloses a kind of ageing-resistant skin care composition, by weight percentage, it is made up of following components, 0.1 10 parts of Saussurea involucrata extract, 1 20 parts of wineberry seed oil, 1 60 parts of polypeptide, 0.1 35 parts of external skin wrinkling-preventing agent, 0.01 0.5 parts of EDETATE SODIUM, 1 150 parts of the first NMF, 0.1 70 parts of the second NMF.Present invention also offers a kind of anti-ageing face mask liquid and preparation method thereof.Compared with prior art, the present invention is rich in Saussurea involucrata extract and the crease-resistant composition of the oily two kinds of plant components and biologically active polypeptide etc. of wineberry seed, simultaneously rich in moisturizing ingredients such as beta glucan and hyaluronic acids, effect of wrinkling is gone with excellent, simultaneously can also replenishing water and preserving moisture, more fully improve skin aging problem, delay skin aging.
Description
Technical field
The present invention relates to daily cosmetics technical field, and in particular to one kind contains plant extracts and biologically active polypeptide
Anti-ageing face mask liquid and preparation method thereof.
Background technology
Skin senescence is the biological process of a series of complex in skin histology, is all endogenous physiological factors and external source
The property coefficient result of environmental factor.Moreover, the influence of inherent cause and associated aging gene and protein expression level, also
It is to cause the key factor of skin senescence to have solar UV irradiation of long-term, high-dose etc..Skin aging not only influences normally
Skin texture and physiological function, also directly affect the outward appearance and appearance of skin outer layer.So, anti-aging, it is anti-oxidant by
Ask the great attention of beautiful person.
Current anti-aging class skin care item species is various, and main composition has skin moisturizer (hyaluronic acid, hyalomitome
Amine, chitosan etc.), skin barrier renovation agent (ceramide, phosphatide, cholesterol etc.), skin-nourishing agent (protein, amino acid,
Polysaccharide etc.), Porcine HGF (epithelical cell growth factor and fibroblast growth factor etc.), antioxidant (super oxygen
Thing mutase and metallothionein etc.), estrogen (animal estrogen and phytoestrogen etc.), vitamins (vitamin E and its
Derivative and vitamin C and its derivative etc.), micro- (selenium and germanium etc.), marine organism extract (fish skin collagen and roe
Collagen etc.), life inhereditary material (DNA DNA and RNA etc.), Chinese medical extract (panaxoside and red
Red-spotted stonecrop saponin etc.), plant extracts (Tea Polyphenols, anthocyanidin and pycnogenol) and natural whiting sun-screening agent (scutellaria glycosides and ursin)
Deng.
Plant extract active component Yin Qigao security and functional activity, significantly to penetrate into food, medicine, cosmetic
The industries such as product, as the current study hotspot in this area, many of nature has crease-resistant, oxidation resistant effective ingredients in plant quilt
The mankind are had found, and are applied to cosmetic skin care field.
Lanatechead saussurea herb with flower is born in rock seam, cliff and ice sulphur ruckle near 2400-4000 meters of high mountain snow lines of height above sea level.It is subzero several
Ten degree of severe cold and the anaerobic environment of extreme create the unique pharmacological action of saussurea involucrata and medical value.Lanatechead saussurea herb with flower is applied in skin care
The metabolism of skin can be accelerated in product, wrinkle is reduced, skin is kept gloss, plentiful, anti-aging.
Wineberry is grown in the Arctic Circle, and in order to resist the polar day sunlight of 24 hours, wineberry fruit generates abundant
Anthocyanin, its antioxygenic property is superpower.Cranberry seed oil is then containing the polyunsaturated fatty acid for being especially suitable for skin ratio.Europe
The application of cranberry seed oil can make skin tackle oxidative pressure, strengthen skin barrier function, and skin malaise symptoms of releiving.
With the development of medical science, Dermatology and molecular biology, polypeptide is by increasingly in-depth study.Polypeptide pair
Skin Cell has various biological activities, relative to peptide and proteins such as Porcine HGFs, and the small polypeptide of molecular weight can
With with higher percutaneous permeability, it is easier to be absorbed by the body, while the underlying biological study mechanism of antiwrinkle active thing triggers
Change to polypeptide, polypeptide is applied to cosmetic field, with the continuous development of scientific technology, and biological active agents are got over
It disclosed come more, further research and probe can provide the weight that the active material of effective anti-aging is studied as this area
Want problem.
The content of the invention
It is an object of the invention to provide a kind of composition of anti aging effect.
The second object of the present invention is to provide a kind of anti aging effect facial mask liquid.
The third object of the present invention is to provide a kind of preparation method of anti aging effect facial mask liquid.
To achieve the above object, present invention firstly provides a kind of ageing-resistant skin care composition, it includes Saussurea involucrata extract
0.1-20 parts, 1-20 parts of wineberry seed oil, 1-60 parts of polypeptide, 0.1-35 parts of external skin wrinkling-preventing agent, 0.01-35 parts of EDETATE SODIUM,
First 1-150 parts of NMF, 0.1-70 parts of the second NMF.
Preferably, the polypeptide is acetyl group octapeptide -3, palmityl tripeptides -1 and one kind or many in palmityl tetrapeptide -7
Kind.
Preferably, the anti wrinkling agent is the one or more in niacinamide, adenosine, tocopherol acetate and collagen.
Preferably, first NMF be glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, succinoglycan,
One in 1,3 butylene glycol, pungent glycol, PEG-400, Natrulon H-10, reed fragrant plant oil, sorbierite, PEG/PPG-14/7 dimethyl ethers
Plant or a variety of.
Preferably, second NMF is NMF, carbohydrate isomer, oat beta-glucan, tetrahydrochysene first
Yl pyrimidines carboxylic acid, Sodium Hyaluronate, Scleroglucan, mushroom glucan, yeast dextran, Aloe Vera Gel, glycine betaine, chitosan and sea
One or more in algae sugar.
Preferably, the preserving moisture and protecting skin composition also includes antiinflammatory, emollient, thickener, emulsifying agent, preservative and day
Use essence.
Preferably, the antiinflammatory is the one or more in dipotassium glycyrrhizinate, allantoin and bisabolol.
Preferably, the emollient is dipentaerythritol three-poly- hydroxy stearic acid ester, pentaerythrite four (thylhexoic acid)
One or more in ester, White Mineral Oil, dimethyl silicone polymer, ring five dimethyl silicone polymer, Miglyol 812N.
Preferably, the thickener is carbomer, xanthans, hydroxyethyl cellulose, PAA/acryloyldimethyl ox
One or more in sodium sulfonate copolymers, C10-30 alkylol acrylamide acid esters cross-linked polymers and the hard ester alcohol of spermaceti.
Preferably, the emulsifying agent is the stearate of polyglycereol -6, the behenate of polyglycereol -6, hydrolecithin, haemolysis
One or more in lecithin, PEG-100 stearates, C12-20 alkyl glucosides and ethylene glycol palmitate.
Preferably, the preservative is parahydroxyacet-ophenone, 1,2- hexylene glycols, methyl hydroxybenzoate, ethyl hydroxy benzoate, oxybenzene third
Ester, imidazolidinyl urea, double imidazolidinyl urea, Phenoxyethanol, methylisothiazolinone, methylchloroisothiazandnone, benzisothia
Oxazoline ketone, iodine propilolic alcohol butyl mephenesin Carbamate, DMDMH, the bromo- 2- nitropropanes -1,3- glycol of 2-, potassium sorbate, benzene
One or more in sodium formate, Chlorphenesin and Sensiva SC50.
Further, the invention provides a kind of anti-ageing face mask liquid, by weight percentage, the facial mask liquid is by following
Component is made, Saussurea involucrata extract 0.01-2%, wineberry seed oil 0.1-2%, polypeptide 0.1-6%, external skin wrinkling-preventing agent 0.01-
3.5%th, EDETATE SODIUM 0.001-0.05%, the first NMF 0.1-15%, the second NMF 0.01-7%, antiinflammatory 0.01-
0.5%th, emollient 0.1-2%, thickener 0.05-0.5%, emulsifying agent 0.1-4%, preservative 0.3-1%, daily essence
0.01-0.2%, NaOH 0.01-0.1% and deionized water:Its surplus.
Preferably, the polypeptide is acetyl group octapeptide -3, palmityl tripeptides -1 and one kind or many in palmityl tetrapeptide -7
Kind.
Preferably, the anti wrinkling agent is the one or more in niacinamide, adenosine, tocopherol acetate and collagen.
Preferably, first NMF be glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, succinoglycan,
One in 1,3 butylene glycol, pungent glycol, PEG-400, Natrulon H-10, reed fragrant plant oil, sorbierite, PEG/PPG-14/7 dimethyl ethers
Plant or a variety of.
Preferably, second NMF is NMF, carbohydrate isomer, oat beta-glucan, tetrahydrochysene first
Yl pyrimidines carboxylic acid, Sodium Hyaluronate, Scleroglucan, mushroom glucan, yeast dextran, Aloe Vera Gel, glycine betaine, chitosan and sea
One or more in algae sugar.
Preferably, by weight percentage, the facial mask liquid is made up of following components, Saussurea involucrata extract 0.05-1%, Europe
Continent cranberry seed oil 0.1-1%, polypeptide 0.1-3%, external skin wrinkling-preventing agent 0.01-1%, EDETATE SODIUM 0.01-0.05%, the first moisturizing
Agent 3-15%, the second NMF 0.1-3.5%, antiinflammatory 0.01-0.1%, emollient 0.1-2%, thickener 0.1-0.3%,
Emulsifying agent 0.2-1%, preservative 0.5-1%, daily essence 0.01-0.1%, pH adjusting agent 0.01-0.05% and deionized water:
Its surplus；The polypeptide is two or more in acetyl group octapeptide -3, palmityl tripeptides -1 and palmityl tetrapeptide -7；It is described anti-
Wrinkle agent is two or more in niacinamide, adenosine, tocopherol acetate；First NMF be glycerine, methyl propanediol,
Two kinds or several in glycerin polyether -26, D-pantothenyl aleohol, succinoglycan, 1,3 butylene glycol, PEG-400, Natrulon H-10, reed fragrant plant oil
Kind；Second NMF be NMF, carbohydrate isomer, oat beta-glucan, tetrahydrochysene methylpyrimidine carboxylic acid, thoroughly
Two or more in the sour sodium of bright matter, mushroom glucan, yeast dextran, pyrenomycetes acid.
Preferably, by weight percentage, the facial mask liquid is made up of following components：Saussurea involucrata extract 0.1%, Europe are got over
(main component is palmityl tripeptides -1 and palmityl four for tangerine seed oil 0.2%, the aqueous solution of acetyl group octapeptide -3 0.2%, base peptide 3000
Peptide -7) 0.2%, EDETATE SODIUM 0.02%, glycerine 3%, methyl propanediol 3%, glycerin polyether -262%, D-pantothenyl aleohol 0.1%, day
Right moisturizing factor 0.03%, carbohydrate isomer 0.2%, oat beta-glucan 0.2%, Scleroglucan 0.1%, Sodium Hyaluronate
0.03%th, niacinamide 0.1%, adenosine 0.04%, antiinflammatory 0.02%, emollient 0.3%, thickener 0.1%, emulsifying agent
0.5%th, preservative 0.9%, daily essence 0.02%, NaOH 0.018%, deionized water：Its surplus.
Preferably, by weight percentage, the facial mask liquid is made up of following components：Saussurea involucrata extract 0.1%, Europe are got over
(main component is palmityl tripeptides -1 and palmityl four for tangerine seed oil 0.2%, the aqueous solution of acetyl group octapeptide -3 0.2%, base peptide 3000
Peptide -7) 0.2%, EDETATE SODIUM 0.02%, glycerine 3%, methyl propanediol 3%, glycerin polyether -262%, D-pantothenyl aleohol 0.1%, day
Right moisturizing factor 0.03%, carbohydrate isomer 0.2%, oat beta-glucan 0.2%, Scleroglucan 0.1%, Sodium Hyaluronate
0.03%th, niacinamide 0.1%, adenosine 0.04%, dipotassium glycyrrhizinate 0.02%, dipentaerythritol three-poly- hydroxy stearic acid ester
0.3%th, carbomer TR-10.12%, PBS60.3%, lysolecithin 0.2%, parahydroxyacet-ophenone 0.5%, 1,2- hexylene glycols
0.4%th, daily essence 0.02%, NaOH 0.024%, deionized water：Its surplus.
Further, the invention provides a kind of preparation method of anti-ageing face mask liquid, including following preparation process：
(1) each component is weighed in proportion：Saussurea involucrata extract, wineberry seed oil, polypeptide, external skin wrinkling-preventing agent, EDETATE SODIUM,
First NMF, the second NMF, antiinflammatory, emollient, thickener, emulsifying agent, preservative, daily essence, pH adjusting agent and
Deionized water.
(2) tocopherol acetate, EDETATE SODIUM, the first NMF, emollient, thickener, emulsifying agent are added residue and gone
Stirred in ionized water at 80-85 DEG C；
(3) component mixture in step (2) is cooled to 45-50 DEG C, and it is red to add the rain life of above-mentioned percentage by weight
Ball algae extract, the second NMF, preservative, daily essence and pH adjusting agent, produce the facial mask liquid after stirring.
Further, the invention provides a kind of anti-ageing face mask, the facial mask includes face mask substrate material, the face mask substrate material
Upper uniform adsorption has above-described facial mask liquid.
Preferably, the face mask substrate material is any one in cotton, silk, non-woven fabrics and biological fiber.
Beneficial effect
The anti-ageing face mask liquid of the present invention, rich in Saussurea involucrata extract and the oily two kinds of plant components of wineberry seed and biology
Active peptides composition, using the crease-resistant biomechanism of the unique pharmacological action Binding peptide of saussurea involucrata, along with adenosine and niacinamide
Two big crease-resistant compositions, while the excellent guarantor such as wineberry seed oil, Sodium Hyaluronate, carbohydrate isomer, oat beta-glucan
The addition of wet skin care ingredient, collaboration resistance skin senescence, effectively repairs wrinkle, improves the skin occurred during skin senescence
Dim, jaundice, while the protection to skin deeper, strengthens skin sparing barrier.
Embodiment
Following examples are used to illustrate the present invention, but are not limited to the scope of the present invention.Unless otherwise specified, of the invention
Employed in each component can be obtained by way of market is bought.Wherein：
Saussurea involucrata extract is that (TOYOBO) production is spun by Japan；Wineberry seed oil is the production of the Hao Bo Co., Ltds of Guangzhou hundred；
Acetyl group octapeptide -3 produces for Li Putai companies of Spain；Base peptide 3000 produces for CORDA；Sodium Hyaluronate is Fu Ruidasheng
Production；Reed fragrant plant oil is the production of ISP companies of the U.S.；PEG-400, hydroxyethyl cellulose produce for Tao Shi, and main component is polyethylene glycol；
Carbohydrate isomer produces for Guangzhou Rui Yu Chemical Industry Science Co., Ltd；Oat beta-glucan produces for fragrant (symrise) of moral,
Mainly include water, glycerine, beta glucan, 1,2- hexylene glycols, pungent glycol, D-pantothenyl aleohol；Mushroom glucan is Lang De companies of South Korea hundred
Production；Pyrenomycetes acid, yeast dextran, C12-20 alkyl glucosides, Natrulon H-10, bisabolol produce for BASF；Adenosine
Produced for sincerity medicine company；Niacinamide produces for DSM (DSM) company；Allantoin produces for Clariant；Dipotassium glycyrrhizinate is general
Plant production；NMF produces for TRI-K；Collagen produces for France Luo Sailuo；Xanthans is Vanderbilt ore deposit
Thing Co., Ltd produces；White Mineral Oil produces for Germany Shu Mei；Parahydroxyacet-ophenone produces for fragrant (symrise) of moral；1,2- second
Glycol produces for Bristol；Carbomer TR-1 produces for Lu Borun, and main component is acrylic acid (ester) class/C10-30 alkylol acrylamides acid
Ester cross-linked polymer；PBS6 produces to win creation；PEG-400 odium stearate is standing grain big (Croda) production, and daily essence is fragrant kindness
Production.
Terminology used in the present invention " NMF ", English name Fision Hydrate, main component is water,
Anjidew NL50, wheat amino acid class, panthenol, glycerine, Sodium Hyaluronate, hydroxyproline.
Terminology used in the present invention " PBS6 ", main component is the stearate of polyglycereol -6 and the behenate of polyglycereol -6.
Terminology used in the present invention " pentaerythrite four (thylhexoic acid) ester ", No. CAS be 7299-99-2, code name UN-219,
It is a kind of light emollient.
Terminology used in the present invention " C12-20 alkyl glucosides " be carbon chain lengths be 12-20 natural fatty alcohol with grape
A kind of material of sugar synthesis, commonly uses code name APG.
The term " PEG-400 odium stearate " of the present invention is conventional emulsifying agent, and PEG is the English name of poly- diethanol
Polyethylene glycol abbreviation, the chemical composition of poly- diethanol (PEG) class is generally used as different type area using numeral
Point, such as：PEG-4, PEG-100 etc., numeral are smaller, represent chemical composition and are more easily absorbed by the skin.
Terminology used in the present invention " PEG/PPG-14/7 dimethyl ethers " is methyl oxirane and oxirane dimethyl
The polymer of ether, alias has PEG/PPG-3/6 dimethyl ethers, PEG/PPG-9/2 dimethyl ethers, and No. CAS is 61419-46-3.
Terminology used in the present invention " DMDMH " is 1,3- dihydroxymethyl -5,5- dimethyl hydantoins, also known as
1,3- dihydroxymethyl -5,5- DMH, No. CAS is 6440-58-0, and DMDM is diformazan hydroxyl dimethyl (Dimethylol
Dimethyl abbreviation).
Acetyl group octapeptide -3, also known as SNAP-8, are the upgradings made in argireline.Acetyl group octapeptide -3 is class meat poisoning
Plain mechanism, by suppressing the synthesis of SNARE acceptors, the catecholamine and acetylcholine for suppressing skin excessively discharge, local resistance
Disconnected neurotransmission contraction of muscle message, loosens facial muscle, reaches the flat purpose for comforting microgroove, and reduction is received by facial expression muscle
The depth for the wrinkle that contracting is caused, particularly around forehead and eyes.
Base peptide 3000, English name Matrixyl 3000, main component is palmityl tripeptides -1 and palmityl tetrapeptide -7, is made
For star's oligopeptides of anti-wrinkle, palmityl tripeptides -1 can promote the generation of skin collagen, elastin laminin, make skin full
It is flexible.Palmityl tetrapeptide -7 can reduce the generation of interleukins, diminish inflammation, and make skin smoothly delicate, and youth light is presented
Pool.
Carbohydrate isomer is referred to as " water lock magnetite ", is a kind of natural moisture preserving extracted from sugarcane carbohydrate synthesis
Agent, moisturizing, the keratin assisted in moisture content combined with stratum corneum, with up to moistening effect.Water lock magnetite is used as a kind of good water conservation
Agent and emollients, the isomerization D- manufactured with reparation epidermal layer cells, lifting skin moisturizing ability, via Measurement for Biochemistry
Glucan, with the composition structure close with human keratinous layer, can be combined using on skin with epsilon-amino acid functional group, just as
Firmly combined as magnetite, long-acting can maintain the hydromagnetic field energy power of skin.
Oat beta-glucan is a kind of SNSP for being present in oat endosperm and gluten cell wall, can improve skin
Texture, lifts skin elasticity, with excellent moisture-keeping function and repair.
Adenosine participates in wrinkle repair process as ATP precursor, and energy is provided for skin wrinkle reparation.
Niacinamide is a kind of derivative of vitamin B3, be also the generally acknowledged skin anti-aging in cosmetic dermatology field into
Part, increasingly paid attention in recent years by people, its most important effect in terms of skin anti-aging is that mitigation and prevention skin exist
Colour of skin dimness, the jaundice produced in early stage aging course；Impaired Stratum corneum lipids barrier can also be repaired, skin resistance is improved
Power.
Hyaluronic acid is also known as sodium hyaluronate sodium, and basic structure is by two dissacharide units D-Glucose aldehydic acid and N- Acetylglucos
The large-scale polysaccharide of amine composition.It is different from other mucopolysaccharides, its not sulfur-bearing.Its hyalomitome molecule can carry more than 500 times
Moisture, is current recognized optimal moisturizing ingredient, is widely applied in skin care products and cosmetics.
Embodiment 1
A kind of anti-ageing face mask liquid, by weight percentage, it is made up of following components:Saussurea involucrata extract 0.02%, Europe
Continent cranberry seed oil 0.2%, the solution of acetyl group octapeptide -3 0.3%, base peptide 30000.1%, niacinamide 0.02%, EDETATE SODIUM
0.01%th, glycerine 5%, 1,3 butylene glycol 3%, glycerin polyether -260.3%, D-pantothenyl aleohol 0.02%, carbohydrate isomer
0.2%th, oat beta-glucan 0.02%, Scleroglucan 0.02%, Sodium Hyaluronate 0.03%, allantoin 0.02%, dimerization season penta
Tetrol three-poly- hydroxy stearic acid ester 0.2%, carbomer TR-10.05%, PEG-100 stearate 0.5%, hydrolecithin
0.4%th, parahydroxyacet-ophenone 0.5%, 1,2- hexylene glycols 0.4%, daily essence 0.02%, NaOH 0.024% and deionization
Water：Its surplus.
By said components and percentage by weight, the preparation process of the facial mask liquid includes：
(1) each component is weighed in proportion：Saussurea involucrata extract, wineberry seed oil, the solution of acetyl group octapeptide -3, base peptide
3000th, niacinamide, EDETATE SODIUM, glycerine, 1,3 butylene glycol, glycerin polyether -26, D-pantothenyl aleohol, carbohydrate isomer, oat Portugal
Glycan, Scleroglucan, Sodium Hyaluronate, allantoin, dipentaerythritol three-poly- hydroxy stearic acid ester, carbomer TR-1, PEG-
100 stearates, hydrolecithin, parahydroxyacet-ophenone, 1,2- hexylene glycols, daily essence, NaOH and deionized water：Remaining
Amount.
(2) portions of de-ionized water is taken, NaOH is added in deionized water and configures NaOH solution；
(3) by niacinamide, EDETATE SODIUM, glycerine, 1,3 butylene glycol, glycerin polyether -26, D-pantothenyl aleohol, dipentaerythritol
Three-poly- hydroxy stearic acid ester, allantoin, carbomer TR-1, PEG-100 stearate, hydrolecithin add remaining deionization
Stirred in water at 80-85 DEG C；
(4) component mixture in step (3) is cooled to 45-50 DEG C, and adds the saussurea involucrata of above-mentioned percentage by weight and carried
Take thing, wineberry seed oil, the solution of acetyl group octapeptide -3, base peptide 3000, carbohydrate isomer, oat beta-glucan, pyrenomycetes
Glue, Sodium Hyaluronate, parahydroxyacet-ophenone, 1,2- hexylene glycols, daily essence and NaOH solution, produce the face after stirring
Film liquid.
Preparing saussurea involucrata anti-ageing face mask then needs to proceed following step：
(5) face mask substrate material cut out (such as facial mask with non-woven fabrics) is immersed in step (4) in the facial mask liquid of gained, its
The mass volume ratio of middle face mask substrate material (such as facial mask non-woven fabrics) and facial mask liquid is 1g:25ml, soak time is 30 minutes, immersion
After produce saussurea involucrata anti-ageing face mask.
Embodiment 2
A kind of anti-ageing face mask liquid, by weight percentage, it is made up of following components:Saussurea involucrata extract 1.8%, Europe
Cranberry seed oil 2%, the solution of acetyl group octapeptide -3 3%, niacinamide 0.1%, adenosine 0.04%, EDETATE SODIUM 0.02%, glycerine
3%th, methyl propanediol 5%, glycerin polyether -264%, NMF 1%, carbohydrate isomer 0.02%, Jiao Mai Portugals
Glycan 2%, Scleroglucan 1%, dipotassium glycyrrhizinate 0.4%, dimethyl silicone polymer 1.5%, xanthans 0.5%, haemolysis lecithin
Fat 2%, parahydroxyacet-ophenone 0.5%, 1,2- hexylene glycols 0.5%, daily essence 0.2%, NaOH 0.1% and deionized water：Its
Surplus.
By said components and percentage by weight, the preparation process of the facial mask liquid includes：
(1) each component is weighed in proportion：Saussurea involucrata extract, wineberry seed oil, the solution of acetyl group octapeptide -3, niacinamide,
Adenosine, EDETATE SODIUM, glycerine, methyl propanediol, glycerin polyether -26, NMF, carbohydrate isomer, Jiao Mai Portugals
Glycan, Scleroglucan, dipotassium glycyrrhizinate, dimethyl silicone polymer, xanthans, lysolecithin, parahydroxyacet-ophenone, 1,2- oneself
Glycol, daily essence, NaOH and deionized water：Its surplus.
(2) portions of de-ionized water is taken, NaOH is added in deionized water and configures NaOH solution；
(3) by niacinamide, adenosine, EDETATE SODIUM, glycerine, methyl propanediol, glycerin polyether -26, dipotassium glycyrrhizinate, poly- two
Methylsiloxane, xanthans, lysolecithin are added to stir in remaining deionized water at 80-85 DEG C；
(4) component mixture in step (3) is cooled to 45-50 DEG C, and adds the saussurea involucrata of above-mentioned percentage by weight and carried
Take thing, it is wineberry seed oil, the solution of acetyl group octapeptide -3, NMF, carbohydrate isomer, ferment wheat glucan, small
Pyrenomycetes glue, parahydroxyacet-ophenone, 1,2- hexylene glycols, daily essence and NaOH solution, produce the facial mask liquid after stirring.
Preparing saussurea involucrata anti-ageing face mask then needs to proceed following step：
(5) face mask substrate material cut out (such as facial mask with non-woven fabrics) is immersed in step (4) in the facial mask liquid of gained, its
The mass volume ratio of middle face mask substrate material (such as facial mask non-woven fabrics) and facial mask liquid is 1g:25ml, soak time is 30 minutes, immersion
After produce saussurea involucrata anti-ageing face mask.
Embodiment 3
A kind of anti-ageing face mask liquid, by weight percentage, it is made up of following components:Saussurea involucrata extract 0.06%, Europe
Continent cranberry seed oil 0.4%, the solution of acetyl group octapeptide -3 0.1%, base peptide 30000.1%, niacinamide 0.05%, adenosine 0.03%,
EDETATE SODIUM 0.02%, glycerine 1%, methyl propanediol 5%, glycerin polyether -262%, D-pantothenyl aleohol 0.1%, NMF
0.02%th, carbohydrate isomer 0.2%, oat beta-glucan 0.2%, Scleroglucan 0.1%, Sodium Hyaluronate 0.02%, sweet
Oxalic acid dipotassium 0.02%, White Mineral Oil 0.4%, hydroxyethyl cellulose 0.08%, hydrolecithin 0.2%, lysolecithin
0.2%th, parahydroxyacet-ophenone 0.3%, 1,2- hexylene glycols 0.2%, daily essence 0.02%, NaOH 0.02% and deionized water：
Its surplus.
By said components and percentage by weight, the preparation process of the facial mask liquid includes：
(1) each component is weighed in proportion：Saussurea involucrata extract, wineberry seed oil, the solution of acetyl group octapeptide -3, base peptide
3000th, niacinamide, adenosine, EDETATE SODIUM, glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, NMF, sugar
Class isomer, oat beta-glucan, Scleroglucan, Sodium Hyaluronate, dipotassium glycyrrhizinate, White Mineral Oil, hydroxyethyl cellulose, hydrogen
Change lecithin, lysolecithin, parahydroxyacet-ophenone, 1,2- hexylene glycols, daily essence, NaOH and deionized water.
(2) portions of de-ionized water is taken, NaOH is added in deionized water and configures NaOH solution；
(3) by niacinamide, adenosine, EDETATE SODIUM, glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, glycyrrhizic acid two
Potassium, White Mineral Oil, hydroxyethyl cellulose, hydrolecithin, lysolecithin are added in remaining deionized water in stirring at 80-85 DEG C
Uniformly；
(4) component mixture in step (3) is cooled to 45-50 DEG C, and adds the saussurea involucrata of above-mentioned percentage by weight and carried
Take thing, wineberry seed oil, the solution of acetyl group octapeptide -3, base peptide 3000, NMF, carbohydrate isomer, oat
Glucan, Scleroglucan, Sodium Hyaluronate, parahydroxyacet-ophenone, 1,2- hexylene glycols, daily essence and NaOH solution, stirring are equal
The facial mask liquid is produced after even.
Preparing saussurea involucrata anti-ageing face mask then needs to proceed following step：
(5) face mask substrate material cut out (such as facial mask with non-woven fabrics) is immersed in step (4) in the facial mask liquid of gained, its
The mass volume ratio of middle face mask substrate material (such as facial mask non-woven fabrics) and facial mask liquid is 1g:25ml, soak time is 30 minutes, immersion
After produce saussurea involucrata anti-ageing face mask.
Embodiment 4
A kind of anti-ageing face mask liquid, by weight percentage, it is made up of following components:Saussurea involucrata extract 0.8%, Europe
Cranberry seed oil 1%, the solution of acetyl group octapeptide -3 1.5%, base peptide 30001.5%, niacinamide 0.5%, adenosine 0.3%, EDTA bis-
Sodium 0.05%, glycerine 5%, methyl propanediol 4%, glycerin polyether -262%, D-pantothenyl aleohol 1%, NMF 0.05%, sugar
Class isomer 0.1%, oat beta-glucan 0.1%, Scleroglucan 0.5%, Sodium Hyaluronate 0.08%, bisabolol
0.08%th, dimethyl silicone polymer 1.2%, carbomer TR-10.25%, hydrolecithin 0.9%, parahydroxyacet-ophenone
0.5%th, 1,2- hexylene glycols 0.5%, daily essence 0.08%, NaOH 0.05% and deionized water：Its surplus.
By said components and percentage by weight, the preparation process of the facial mask liquid includes：
(1) each component is weighed in proportion：Saussurea involucrata extract, wineberry seed oil, the solution of acetyl group octapeptide -3, base peptide
3000th, niacinamide, adenosine, EDETATE SODIUM, glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, NMF, sugar
Class isomer, oat beta-glucan, Scleroglucan, Sodium Hyaluronate, bisabolol, dimethyl silicone polymer, carbomer TR-
1st, hydrolecithin, parahydroxyacet-ophenone, 1,2- hexylene glycols, daily essence, NaOH and deionized water.
(2) portions of de-ionized water is taken, NaOH is added in deionized water and configures NaOH solution；
(3) by EDETATE SODIUM, glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, niacinamide, adenosine, opopanax
Alcohol, dimethyl silicone polymer, carbomer TR-1, hydrolecithin are added to stir in remaining deionized water at 80-85 DEG C；
(4) component mixture in step (3) is cooled to 45-50 DEG C, and adds the saussurea involucrata of above-mentioned percentage by weight and carried
Take thing, wineberry seed oil, the solution of acetyl group octapeptide -3, base peptide 3000, NMF, carbohydrate isomer, ferment wheat
Glucan, Scleroglucan, parahydroxyacet-ophenone, 1,2- hexylene glycols, daily essence and NaOH solution, are produced described after stirring
Facial mask liquid.
Preparing saussurea involucrata anti-ageing face mask then needs to proceed following step：
(5) face mask substrate material cut out (such as facial mask with non-woven fabrics) is immersed in step (4) in the facial mask liquid of gained, its
The mass volume ratio of middle face mask substrate material (such as facial mask non-woven fabrics) and facial mask liquid is 1g:25ml, soak time is 30 minutes, immersion
After produce saussurea involucrata anti-ageing face mask.
Embodiment 5
A kind of anti-ageing face mask liquid, by weight percentage, it is made up of following components:Saussurea involucrata extract 0.1%, Europe
Cranberry seed oil 0.3%, the solution of acetyl group octapeptide -3 0.2%, base peptide 30000.2%, EDETATE SODIUM 0.02%, glycerine 3%, methyl
Propane diols 3%, glycerin polyether -262%, D-pantothenyl aleohol 0.1%, NMF 0.03%, carbohydrate isomer 0.2%,
Oat beta-glucan 0.2%, Scleroglucan 0.1%, Sodium Hyaluronate 0.03%, niacinamide 0.1%, adenosine 0.04%, glycyrrhizic acid
Dipotassium 0.02%, dipentaerythritol three-poly- hydroxy stearic acid ester 0.3%, carbomer TR-10.12%, PBS60.3%, haemolysis
Lecithin 0.2%, parahydroxyacet-ophenone 0.5%, 1,2- hexylene glycols 0.4%, daily essence 0.02%, NaOH 0.024% and go
Ionized water：Its surplus.
By said components and percentage by weight, the preparation process of the facial mask liquid includes：
(1) each component is weighed in proportion：Saussurea involucrata extract, wineberry seed oil, the solution of acetyl group octapeptide -3, base peptide 3000
(main component be palmityl tripeptides -1 and palmityl tetrapeptide -7), EDETATE SODIUM, glycerine, methyl propanediol, glycerin polyether -26,
D-pantothenyl aleohol, NMF, carbohydrate isomer, oat beta-glucan, Scleroglucan, Sodium Hyaluronate, niacinamide, gland
Glycosides, dipotassium glycyrrhizinate, dipentaerythritol three-poly- hydroxy stearic acid ester, carbomer TR-1, PBS6, lysolecithin, to hydroxyl
Acetophenone, 1,2- hexylene glycols, daily essence, NaOH and deionized water.
(2) portions of de-ionized water is taken, NaOH is added in deionized water and configures NaOH solution；
(3) by EDETATE SODIUM, glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, niacinamide, adenosine, glycyrrhizic acid two
Potassium, dipentaerythritol three-poly- hydroxy stearic acid ester, carbomer TR-1, PBS6, lysolecithin are added in remaining deionized water
Stirred at 80-85 DEG C；
(4) component mixture in step (3) is cooled to 45-50 DEG C, and adds the saussurea involucrata of above-mentioned percentage by weight and carried
Take thing, wineberry seed oil, the solution of acetyl group octapeptide -3, base peptide 3000, NMF, carbohydrate isomer, oat
Glucan, Scleroglucan, Sodium Hyaluronate, parahydroxyacet-ophenone, 1,2- hexylene glycols, daily essence and NaOH solution, stirring are equal
The facial mask liquid is produced after even.
Preparing saussurea involucrata anti-ageing face mask then needs to proceed following step：
(5) face mask substrate material cut out (such as facial mask with non-woven fabrics) is immersed in step (4) in the facial mask liquid of gained, its
The mass volume ratio of middle face mask substrate material (such as facial mask non-woven fabrics) and facial mask liquid is 1g:25ml, soak time is 30 minutes, immersion
After produce saussurea involucrata anti-ageing face mask.
Embodiment 6
Respectively by anti-ageing face mask liquid made from embodiment 1-5, filling, unlimited bottle cap is carried out with dark brown vial, is put
In the environment of 40 DEG C of environment temperature, relative humidity 60%, continuous observation is simultaneously tested, and concrete outcome see the table below 1.Detect microorganism
Level, specific detection project, detection method and examination criteria are carried out according to QB/T2872-2007.
The preservative efficacy testing of the anti-ageing face mask of table 1
| Observe phenomenon | |
| Embodiment 1 | No abnormality seen after 60 days, pure in smell does not detect microorganism |
| Embodiment 2 | No abnormality seen after 60 days, pure in smell does not detect microorganism |
| Embodiment 3 | No abnormality seen after 60 days, pure in smell does not detect microorganism |
| Embodiment 4 | No abnormality seen after 60 days, pure in smell does not detect microorganism |
| Embodiment 5 | No abnormality seen after 60 days, pure in smell does not detect microorganism |
Embodiment 7
Randomly select female volunteers of 100 ages in 18-45 one full year of life to be tested, be randomly divided into five groups, every group 20
People, volunteer signs voluntary book before test.After volunteer's cleaning face, in constant temperature and humidity (22-25 DEG C of indoor temperature, humidity
Environmental balance 40-60%), by profilograph and the skin of face situation for the assessment volunteer that takes pictures, is obtained after 40 minutes
Initial value.Then the sample in the embodiment of the present invention 1,2,3,4 is used to four groups of volunteers respectively, volunteer is daily in one side of something
Face uses and once tests film sample, after continuously using 2 months, then uses by profilograph and assessment of taking pictures and test facial mask
Sample rear face skin, obtains last value eventually.
1st, anti-wrinkle effect
The initial value and whole last Value Data of volunteer's face skin wrinkle situation are analyzed using statistical method, aspiration is judged
Person uses the situation of change of test film sample rear face wrinkle of skin, p>=0.05 is without significant difference, p<0.05 is to have aobvious
Write difference, p<0.01 is has highly significant difference, as a result as shown in table 2.
The anti-wrinkle effect of table 2
Test result shows there is the facial mask of obvious crease-resistant effect, embodiment 4 and embodiment 5 using facial mask of the present invention
Sample has more preferable crease-resistant effect than embodiment 1,2,3, there is good anti-wrinkle effect from every aspect.
2nd, skin pliability and skin color improvement
Compare and measure volunteer's skin of face water content, the initial value of elasticity and whole last value, count volunteer's moisture of skin
Increase number, elastic increase number contrasts the difference of assessment of scenario volunteer's colour of skin, statistics with sensory evaluation method and before and after taking pictures
The number of skin brightness lifting, as a result as shown in table 3.
The skin senescence improvement of table 3
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | |
| Moisture increase | 15 | 18 | 17 | 15 | 20 |
| Elasticity increase | 12 | 15 | 13 | 16 | 19 |
| Skin brightness | 9 | 14 | 12 | 15 | 19 |
Test result shows that facial mask of the present invention, which has, improves skin pliability, improves effect of skin dimness jaundice, from 5
This it appears that other samples of the film sample comparative example of embodiment 5 are with obvious excellent in the contrast of individual embodiment
Gesture.
Although above the present invention is described in detail with a general description of the specific embodiments,
On the basis of the present invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.Cause
This, these modifications or improvements, belong to the scope of protection of present invention without departing from theon the basis of the spirit of the present invention.
Claims (10)
1. a kind of ageing-resistant skin care composition, it is characterised in that count by weight, it includes：
2. composition as claimed in claim 1, it is characterised in that the polypeptide is acetyl group octapeptide -3, palmityl tripeptides -1
With the one or more in palmityl tetrapeptide -7；The anti wrinkling agent is in niacinamide, adenosine, tocopherol acetate and collagen
One or more；First NMF be glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, succinoglycan, 1,
One kind in 3- butanediols, pungent glycol, PEG-400, Natrulon H-10, reed fragrant plant oil, sorbierite, PEG/PPG-14/7 dimethyl ethers
Or it is a variety of；Second NMF is NMF, carbohydrate isomer, oat beta-glucan, tetrahydrochysene methylpyrimidine carboxylic
In acid, Sodium Hyaluronate, Scleroglucan, mushroom glucan, yeast dextran, Aloe Vera Gel, glycine betaine, chitosan and trehalose
It is one or more.
3. composition as claimed in claim 1, it is characterised in that the composition also includes：Antiinflammatory, emollient, thickening
Agent, emulsifying agent, preservative, pH adjusting agent and/or daily essence.
4. composition as claimed in claim 3, it is characterised in that the antiinflammatory is dipotassium glycyrrhizinate, allantoin and red do not had
One or more in medicine alcohol；The emollient is dipentaerythritol three-poly- hydroxy stearic acid ester, (ethyl of pentaerythrite four
Caproic acid) ester, White Mineral Oil, dimethyl silicone polymer, ring five dimethyl silicone polymer, one kind in Miglyol 812N or many
Kind；The thickener is carbomer, xanthans, hydroxyethyl cellulose, PAA/sodium acryloyldimethyl taurate copolymerization
One or more in thing, C10-30 alkylol acrylamide acid esters cross-linked polymers and the hard ester alcohol of spermaceti；The emulsifying agent be polyglycereol-
6 stearates, the behenate of polyglycereol -6, hydrolecithin, lysolecithin, PEG-100 stearates, C12-20 alkyl Portugal
One or more in glucosides and ethylene glycol palmitate；The preservative is parahydroxyacet-ophenone, 1,2- hexylene glycols, oxybenzene first
Ester, ethyl hydroxy benzoate, Nipasol, imidazolidinyl urea, double imidazolidinyl urea, Phenoxyethanol, methylisothiazolinone, methyl chloride are different
Thiazolinone, BIT, iodine propilolic alcohol butyl mephenesin Carbamate, DMDMH, bromo- 2- nitropropane -1 of 2-,
One or more in 3- glycol, potassium sorbate, sodium benzoate, Chlorphenesin and Sensiva SC50.
5. a kind of anti-ageing face mask liquid, it is characterised in that by weight percentage, it is made up of following component：
6. facial mask liquid as claimed in claim 5, it is characterised in that the polypeptide is acetyl group octapeptide -3, palmityl tripeptides -1
With the one or more in palmityl tetrapeptide -7；The anti wrinkling agent is in niacinamide, adenosine, tocopherol acetate and collagen
One or more；First NMF be glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, succinoglycan, 1,
One kind in 3- butanediols, pungent glycol, PEG-400, Natrulon H-10, reed fragrant plant oil, sorbierite, PEG/PPG-14/7 dimethyl ethers
Or it is a variety of；Second NMF is NMF, carbohydrate isomer, oat beta-glucan, tetrahydrochysene methylpyrimidine carboxylic
In acid, Sodium Hyaluronate, Scleroglucan, mushroom glucan, yeast dextran, Aloe Vera Gel, glycine betaine, chitosan and trehalose
It is one or more.
7. facial mask liquid as claimed in claim 5, it is characterised in that by weight percentage, it is made up of following components：
The polypeptide is two or more in acetyl group octapeptide -3, palmityl tripeptides -1 and palmityl tetrapeptide -7；It is described crease-resistant
Agent is two or more in niacinamide, adenosine, tocopherol acetate；First NMF is glycerine, methyl propanediol, sweet
Two kinds or several in oily polyethers -26, D-pantothenyl aleohol, succinoglycan, 1,3 butylene glycol, PEG-400, Natrulon H-10, reed fragrant plant oil
Kind；Second NMF be NMF, carbohydrate isomer, oat beta-glucan, tetrahydrochysene methylpyrimidine carboxylic acid, thoroughly
Two or more in the sour sodium of bright matter, mushroom glucan, yeast dextran, pyrenomycetes acid.
8. facial mask liquid as claimed in claim 7, it is characterised in that by weight percentage, it is made up of following components：
9. facial mask liquid as claimed in claim 8, it is characterised in that by weight percentage, it is made up of following components：
10. the preparation method of a kind of facial mask liquid as described in one of claim 5-9, it is characterised in that prepare step including following
Suddenly：
(1) each component is weighed in proportion：Saussurea involucrata extract, wineberry seed oil, polypeptide, external skin wrinkling-preventing agent, EDETATE SODIUM, first
NMF, the second NMF, antiinflammatory, emollient, thickener, emulsifying agent, preservative, daily essence, pH adjusting agent and go from
Sub- water；
(2) by EDETATE SODIUM, the first NMF, antiinflammatory, emollient, thickener, emulsifying agent add in remaining deionized water in
Stirred at 80-85 DEG C；
(3) component mixture in step (2) is cooled to 45-50 DEG C, and add above-mentioned percentage by weight Saussurea involucrata extract,
Wineberry seed oil, polypeptide, external skin wrinkling-preventing agent, the second NMF, preservative, daily essence and NaOH solution, after stirring
Produce the facial mask liquid.
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