CN103961290A - Chinese mahonia extracting solution as well as preparation method and an application thereof - Google Patents
Chinese mahonia extracting solution as well as preparation method and an application thereof Download PDFInfo
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- CN103961290A CN103961290A CN201410234687.5A CN201410234687A CN103961290A CN 103961290 A CN103961290 A CN 103961290A CN 201410234687 A CN201410234687 A CN 201410234687A CN 103961290 A CN103961290 A CN 103961290A
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Abstract
The invention discloses a Chinese mahonia extracting solution as well as a preparation method and an application thereof. The Chinese mahonia extracting solution prepared by water extraction has good free radical scavenging activity and the effect of inhibiting peroxidation of lipoxygenase and lipid, and due to the characteristics, the Chinese mahonia extracting solution has the effects of scavenging excessive free radicals accumulated in bodies, preventing formation of lipofuscin, protecting cell membranes, maintaining the normal metabolism of cells and prolonging organism senescence; when being applied to cosmetics, the Chinese mahonia extracting solution has remarkable effects of improving facial laxity and reducing generation of wrinkles and black spots.
Description
Technical field
The present invention relates to cosmetic field, particularly relate to a kind of Mahonia fortunei (Lindl.) Fedde extracting solution and its preparation method and application.
Background technology
Along with the raising of people's living standard, cosmetics have become necessary article in people's life.But people are but very high for the prescription of cosmetics, not only require effective, and require be free from side effects.Along with the continuous breakthrough of beauty and skin care science and technology, plant skin protection theory is popular already, be added with natural plants series products targetedly due to its use safety, action temperature and, the advantage such as the successful parent that obtains consumers in general looks at.Be generally to obtain by corresponding processing the plant extract that contains effective ingredient, and add in cosmetics.
The at present plant extract in cosmetics, mostly adopts the methods such as water extraction, alcohol extraction, ultrasonic extraction, microwave extraction to extract gained, extraction process complexity, through operations such as concentrate dryings, also to add antiseptic so that the shelf-life of extract more permanent.The drawback of bringing like this, one is waste resource, and in leaching process, solution is concentrated, generally only gets concentrated fraction elite out, and most solutions discards.This part solution also contains other effective ingredient in fact, can again utilize, and directly discard the waste that has just caused resource.Another drawback is in extract, add antiseptic no doubt can make extract obtain the longer shelf-life, but the while to be also for skin brings sensitization source.
Aging claims again aging, is the only stage which must be passed by any biological vital movement process, and slow down aging is especially one of focus of studying of people to the slow down aging of skin always.Skin aging be multifactor due to, wherein more representational skin aging mechanism causes the basic reason of skin aging to be with regard to disclosing as: free radical causes of senescence: free radical excessive in human body is piled up, cell membrane and other important component are damaged, and unsaturated fatty acid is oxidized to superoxides by the free radical of piling up, form lipofuscin.Cell is owing to being damaged, epidermis cell upgrades and slows down, keratinocyte vigor declines, barrier function weakens, and fibroblast quantity reduces, synthesizes the ability decline of collagen protein and elastin laminin gradually in skin corium, thereby cause the symptoms such as skin appearance is dry, lax, pigmentation, wrinkle.
Therefore, select which kind of plant, how simple, safety, effectively this plant extract is carried out, and by the aging that is applied to delaying skin in cosmetics of its safety, be problem demanding prompt solution.
Summary of the invention
Based on this, the object of the invention is to provide a kind of Mahonia fortunei (Lindl.) Fedde extracting solution and its preparation method and application.
The concrete technical scheme solving the problems of the technologies described above is as follows:
A preparation method for Mahonia fortunei (Lindl.) Fedde extracting solution, comprises the following steps:
By Mahonia fortunei (Lindl.) Fedde drying and crushing, install with the 800-1000 order gauze bag of sterilizing, be placed in vacuum emulsifying pot, by the weight of Mahonia fortunei (Lindl.) Fedde, the deionized water that adds 8-12 doubly to measure, in 90-100 DEG C of extraction, can make Mahonia fortunei (Lindl.) Fedde extracting solution.
In some embodiment, the time of described extraction is 20-50min therein.
Therein in some embodiment, by Mahonia fortunei (Lindl.) Fedde drying and crushing, install with the 800-1000 order gauze bag of sterilizing, be placed in vacuum emulsifying pot, after having extracted, directly gauze bag is taken out, remaining solution is Mahonia fortunei (Lindl.) Fedde extracting solution.In the method, owing to adopting vacuum emulsifying pot, it can, after extraction completes, directly be added other cosmetics adjuvants, carries out Cosmetic Manufacture, and does not need to extract with special herbal extraction equipment, has saved cost; In addition, adopt gauze packed Mahonia fortunei (Lindl.) Fedde powder, extracted and directly gauze bag has been taken out afterwards, need not filter, simplification extraction process, raises the efficiency.
Said method is simple to operation, and the Mahonia fortunei (Lindl.) Fedde extract use of can now withdrawing deposit, does not need to add antiseptic, significantly reduces the sensitization source to skin.In cosmetic formulations, itself is just added with antiseptic, and extract of the present invention is now carried and being added, and has avoided producing spoilage problems because of placement.
The prepared Mahonia fortunei (Lindl.) Fedde extracting solution of said method has the application in the cosmetics that improve cutis laxa, reduce wrinkle and black speck generation effect in preparation.
In some embodiment, in described cosmetics, the content of Mahonia fortunei (Lindl.) Fedde extracting solution is 58-95wt% therein.
In some embodiment, described cosmetics are toner/smoothing toner, health breast, nourishing cream, essence or mask therein.
The invention provides a kind of toner/smoothing toner, described toner/smoothing toner comprises the component of following weight percentage ratio:
Wetting agent: 5-13wt%,
Thickening agent: 0.05-0.15wt%,
Antiinflammatory: 0.1-0.2wt%,
Nertralizer: 0.05-0.15wt%,
Antiseptic: 0.2-0.7wt%,
The Mahonia fortunei (Lindl.) Fedde extracting solution that above-mentioned preparation method makes: surplus;
Described wetting agent is at least one in glycerol, butanediol, propylene glycol or hyaluronate sodium;
Described thickening agent is at least one in carbomer, xanthan gum or hydroxyethyl-cellulose;
Described antiinflammatory is at least one in allantoin, Flos Inulae extract or bisabolol;
Described nertralizer is at least one in triethanolamine, sodium hydroxide or potassium hydroxide;
Described antiseptic is at least one in phenoxyethanol/Sensiva SC50, DMDM beta-lactam or Kazon.
In some embodiment, described toner/smoothing toner comprises the component of following weight percentage ratio therein:
Wetting agent: 7-11.1wt%,
Thickening agent: 0.09-0.11wt%,
Antiinflammatory: 0.13-0.17wt%,
Nertralizer: 0.09-0.11wt%,
Antiseptic: 0.2-0.4wt%,
The Mahonia fortunei (Lindl.) Fedde extracting solution that above-mentioned preparation method makes: surplus;
Described wetting agent is at least one in glycerol, butanediol, propylene glycol or hyaluronate sodium;
Described thickening agent is carbomer;
Described antiinflammatory is allantoin;
Described nertralizer is triethanolamine;
Described antiseptic is phenoxyethanol/Sensiva SC50.
In some embodiment, described toner/smoothing toner comprises the component of following weight percentage ratio therein:
Glycerol: 4-6wt%,
Butanediol: 3-5wt%,
Carbomer: 0.09-0.11wt%,
Allantoin 0.13-0.17wt%,
Hyaluronate sodium: 0.05-0.07wt%,
Triethanolamine: 0.09-0.11wt%,
Phenoxyethanol/Sensiva SC50: 0.2-0.4wt%,
The Mahonia fortunei (Lindl.) Fedde extracting solution that above-mentioned preparation method makes: surplus.
The present invention also provides a kind of health breast, and described health breast comprises the component of following weight percentage ratio:
Emulsifying agent: 1.5-5wt%,
Co-emulsifier: 0.8-2wt%,
Emollient: 2-8wt%,
Skinfeel regulator: 1.5-10wt%,
Thickening agent: 0.1-0.4wt%,
Wetting agent: 4-10wt%,
Antiseptic: 0.05-0.7wt%,
The Mahonia fortunei (Lindl.) Fedde extracting solution that above-mentioned preparation method makes: surplus;
Described emulsifying agent is at least one in methyl glucose sesquistearate, PEG-20 methyl glucose sesquistearate or glyceryl stearate/PEG-100 stearate;
Described co-emulsifier is at least one in cetearyl alcohol, glyceryl stearate or triethanolamine;
Described emollient is at least one in isopropyl palmitate, caprylic/capric triglyceride or hydrogenated jojoba oil;
Described skinfeel regulator is at least one in ring five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane or vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer;
Described thickening agent is at least one in xanthan gum, hydroxyethyl-cellulose or carbomer;
Described wetting agent is at least one in propylene glycol, glycerol or butanediol;
Described antiseptic is at least one in diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate, propyl hydroxybenzoate or methyl hydroxybenzoate.
In some embodiment, described health breast comprises the component of following weight percentage ratio therein:
Emulsifying agent: 2.5-3.3wt%,
Co-emulsifier: 1.1-1.3wt%,
Emollient: 3-5wt%,
Skinfeel regulator: 5.8-8.2wt%,
Thickening agent: 0.25-0.35wt%,
Wetting agent: 4-6wt%,
Antiseptic: 0.4-0.6wt%,
The Mahonia fortunei (Lindl.) Fedde extracting solution that above-mentioned preparation method makes: surplus;
Described emulsifying agent is at least one in methyl glucose sesquistearate, PEG-20 methyl glucose sesquistearate or glyceryl stearate/PEG-100 stearate;
Described co-emulsifier is cetearyl alcohol;
Described emollient is isopropyl palmitate;
Described skinfeel regulator is at least one in ring five polydimethylsiloxane/cyclohexasiloxane or polydimethylsiloxane;
Described thickening agent is xanthan gum;
Described wetting agent is at least one in propylene glycol, glycerol or butanediol;
Described antiseptic is at least one in diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate, propyl hydroxybenzoate or methyl hydroxybenzoate.
In some embodiment, described health breast comprises the component of following weight percentage ratio therein:
Methyl glucose sesquistearate: 1.1-1.5wt%,
PEG-20 methyl glucose sesquistearate: 0.8-1.0wt%,
Isopropyl palmitate: 3-5wt%,
Encircle five polydimethylsiloxane/cyclohexasiloxane: 4-6wt%,
Glyceryl stearate/PEG-100 stearate: 0.6-0.8wt%,
Cetearyl alcohol: 1.1-1.3wt%,
Polydimethylsiloxane: 1.8-2.2wt%,
Methyl hydroxybenzoate: 0.15-0.25wt%,
Propyl hydroxybenzoate: 0.09-0.11wt%,
Xanthan gum: 0.25-0.35wt%,
Propylene glycol: 4-6wt%,
Diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate: 0.18-0.22wt%,
Above-mentioned Mahonia fortunei (Lindl.) Fedde extracting solution: surplus.
The invention provides a kind of nourishing cream, described nourishing cream comprises the component of following weight percentage ratio:
Emulsifying agent: 3.5-6.3wt%,
Emollient: 5-10wt%,
Antioxidant: 0.2-0.8wt%,
Wetting agent: 5-15wt%,
Thickening agent: 0.05-0.15wt%,
Antiseptic: 0.3-0.7wt%,
The Mahonia fortunei (Lindl.) Fedde extracting solution that above-mentioned preparation method makes: surplus,
Described emulsifying agent is at least one in cetearyl alcohol/cetearyl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearate, polyacrylamide/C13-14 isoparaffin/laureth-7 or methyl glucose sesquistearate;
Described emollient is at least one in ring five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane, caprylic/capric triglyceride or hydrogenated jojoba oil;
Described antioxidant is at least one that tocopherol or fan change in extract;
Described wetting agent is at least one in propylene glycol, glycerol, hyaluronate sodium, oligofructose or sorbitol;
Described thickening agent is at least one in xanthan gum or sodium carboxymethyl cellulose;
Described antiseptic is at least one in phenoxyethanol/Sensiva SC50, sodium benzoate or germall.
In some embodiment, described nourishing cream comprises the component of following weight percentage ratio therein:
Emulsifying agent: 4.9-6.3wt%,
Emollient: 6.4-7.6wt%,
Antioxidant: 0.4-0.6wt%,
Wetting agent: 8-12.15wt%,
Thickening agent: 0.09-0.11wt%,
Antiseptic: 0.4-0.6wt%,
The Mahonia fortunei (Lindl.) Fedde extracting solution that above-mentioned preparation method makes: surplus,
Described emulsifying agent is at least one in cetearyl alcohol/cetearyl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearate or polyacrylamide/C13-14 isoparaffin/laureth-7;
Described emollient is at least one in ring five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane or caprylic/capric triglyceride;
Described antioxidant is tocopherol;
Described wetting agent is at least one in propylene glycol, glycerol, hyaluronate sodium or oligofructose;
Described thickening agent is xanthan gum;
Described antiseptic is phenoxyethanol/Sensiva SC50.
In some embodiment, described nourishing cream comprises the component of following weight percentage ratio therein:
Cetearyl alcohol/cetearyl glucoside: 2.3-2.7wt%,
Cetearyl alcohol: 1-1.4wt%,
Glyceryl stearate/PEG-100 stearate 1-1.4wt%,
Encircle five polydimethylsiloxane/cyclohexasiloxane: 1.8-2.2wt%,
Polydimethylsiloxane: 1.8-2.2wt%,
Caprylic/capric triglyceride: 2.8-3.2wt%,
Tocopherol: 0.4-0.6wt%,
Propylene glycol: 4-6wt%,
Glycerol: 4-6wt%,
Xanthan gum: 0.09-0.11wt%,
Hyaluronate sodium: 0.015-0.025wt%,
Polyacrylamide/C13-14 isoparaffin/laureth-7:0.6-0.8wt%,
Phenoxyethanol/Sensiva SC50: 0.4-0.6wt%,
Oligofructose: 0.08-0.11wt%,
Above-mentioned Mahonia fortunei (Lindl.) Fedde extracting solution: surplus.
The present invention also provides a kind of essence, and described essence comprises the component of following weight percentage ratio:
Chelating agen: 0.01-0.1wt%,
Wetting agent: 5-18wt%,
Antiinflammatory: 0.05-2.5wt%,
Antiseptic: 0.3-0.66wt%,
The Mahonia fortunei (Lindl.) Fedde extract that above-mentioned preparation method makes: surplus;
Described chelating agen is at least one in EDTA-disodium or Etidronic Acid;
Described wetting agent is at least one in glycerol, propylene glycol, Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate, Aloe vulgaris leaf extract or PEG400;
Described antiinflammatory is at least one in allantoin, Hamamelis virginiana extract, glycyrrhizic acid dipotassium or Flos Inulae extract;
Described antiseptic is at least one in methyl hydroxybenzoate, phenoxyethanol/Sensiva SC50 or Kazon.
In some embodiment, described essence comprises the component of following weight percentage ratio therein:
Chelating agen: 0.01-0.025wt%,
Wetting agent: 10-15.5wt%,
Antiinflammatory: 1.9-2.4wt%,
Antiseptic: 0.54-0.66wt%,
The Mahonia fortunei (Lindl.) Fedde extract that above-mentioned preparation method makes: surplus;
Described chelating agen is EDTA-disodium;
Described wetting agent is at least one in glycerol, propylene glycol, Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate or Aloe vulgaris leaf extract;
Described antiinflammatory is at least one in allantoin, Hamamelis virginiana extract or glycyrrhizic acid dipotassium;
Described antiseptic is at least one in methyl hydroxybenzoate or phenoxyethanol/Sensiva SC50.
In some embodiment, described essence comprises the component of following weight percentage ratio therein:
EDTA-disodium: 0.018-0.022wt%,
Glycerol: 4-6wt%,
Propylene glycol: 4-6wt%,
Allantoin: 0.09-0.11wt%,
Methyl hydroxybenzoate: 0.09-0.11wt%,
Hamamelis virginiana extract: 1.8-2.2wt%,
Glycyrrhizic acid dipotassium: 0.045-0.055wt%,
Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate: 0.9-1.1wt%,
Aloe vulgaris leaf extract: 1.8-2.2wt%,
Phenoxyethanol/Sensiva SC50: 0.45-0.55,
Above-mentioned Mahonia fortunei (Lindl.) Fedde extracting solution: surplus.
The present invention also provides a kind of mask, and described mask comprises the component of following weight percentage ratio:
Wetting agent: 5-35wt%,
Thickening agent: 0.05-0.3wt%,
Antiinflammatory: 2.5-5.5wt%,
PH adjusting agent: 0.04-0.08wt%,
Antiseptic: 0.2-0.6wt%,
Above-mentioned Mahonia fortunei (Lindl.) Fedde extract: surplus;
Described wetting agent is at least one in glycerol, butanediol, propylene glycol, hyaluronate sodium, glycerol polymethacrylates/propylene glycol, Ovshinsky Sargassum extract, beta glucan or oligofructose;
Described thickening agent is at least one in hydroxyethyl-cellulose, carbomer or xanthan gum;
Described antiinflammatory is at least one in allantoin, Hamamelis virginiana extract or bisabolol;
Described pH adjusting agent is at least one in triethanolamine, potassium hydroxide or sodium hydroxide;
Described antiseptic is at least one in 1,2-hexanediol/caprylyl glycol or phenoxyethanol/Sensiva SC50.
In some embodiment, described mask comprises the component of following weight percentage ratio therein:
Wetting agent: 21.5-32.3wt%,
Thickening agent: 0.14-0.26wt%,
Antiinflammatory: 3.1-5.5wt%,
PH adjusting agent: 0.05-0.07wt%,
Antiseptic: 0.4-0.6wt%,
Above-mentioned Mahonia fortunei (Lindl.) Fedde extract: surplus;
Described wetting agent is at least one in glycerol, butanediol, propylene glycol, hyaluronate sodium, glycerol polymethacrylates/propylene glycol, Ovshinsky Sargassum extract or beta glucan;
Described thickening agent is at least one in hydroxyethyl-cellulose or carbomer;
Described antiinflammatory is at least one in allantoin or Hamamelis virginiana extract;
Described pH adjusting agent is at least one in potassium hydroxide or sodium hydroxide;
Described antiseptic is 1,2-hexanediol/caprylyl glycol.
In some embodiment, described mask comprises the component of following weight percentage ratio therein:
Glycerol: 4-6wt%,
Butanediol: 4-6wt%,
Propylene glycol: 2-4wt%,
Hydroxyethyl-cellulose: 0.04-0.06wt%,
Hyaluronate sodium: 0.025-0.035wt%,
Carbomer: 0.1-0.2wt%,
Allantoin: 0.1-0.2wt%,
Beta glucan: 0.8-1.2wt%,
Glycerol polymethacrylates/propylene glycol: 7-9wt%,
Ovshinsky Sargassum extract: 4-6wt%,
Hamamelis virginiana extract: 3-5wt%,
Potassium hydroxide: 0.05-0.07wt%,
1,2-hexanediol/caprylyl glycol: 0.4-0.6wt%,
Above-mentioned Mahonia fortunei (Lindl.) Fedde extracting solution: surplus.
A kind of Mahonia fortunei (Lindl.) Fedde extracting solution of the present invention and its preparation method and application has the following advantages and beneficial effect:
The present invention is through a large amount of experiment of inventor and research; draw at optimum process---prepared Mahonia fortunei (Lindl.) Fedde extracting solution under water extraction; it has good free radical scavenging activity and suppresses lipoxidase and lipid peroxidation; this specific character makes Mahonia fortunei (Lindl.) Fedde extracting solution possess the excessive free radicals of removing body inner accumulated; prevent the formation of lipofuscin; Cell protection film; maintain cell homergy; delay the effect of body aging, be applied to effect that tool in cosmetics is significantly improved cutis laxa, reduces wrinkle and black speck generation.
Detailed description of the invention
Mahonia fortunei (Lindl.) Fedde of the present invention is Berberidaceae Mahonia plant Mahonia bealei (Fort.) Carr. and Mahonia fortunei, and Herb can hyoscine, is mainly distributed in Guangxi, Sichuan, Guizhou, Hubei, Jiangxi, zhejiang and other places.Mahonia fortunei (Lindl.) Fedde bitter in the mouth is cold in nature, has nourishing YIN and clearing away heat, antipyretic and antidote functions.The present invention makes Mahonia fortunei (Lindl.) Fedde extracting solution by Mahonia fortunei (Lindl.) Fedde through water extraction, uses it for preparation and has in the cosmetics that improve cutis laxa, reduce wrinkle and black speck generation.
Below with reference to specific embodiment, the present invention will be further described.
In following embodiment, described Hamamelis virginiana extract purchased from Xi'an Sen Ran biological engineering company limited, Aloe vulgaris leaf extract purchased from Tianfeng Biological Science & Technology Co., Ltd., Xi'an, Ovshinsky Sargassum extract purchased from Rui Ying bio tech ltd, Xi'an, the equal commercially available prod of other raw materials.
In following examples, composition title used is international cosmetic raw material name (InternationalNomenclature Cosmetic Ingredient, INCI) title of defined, for example phenoxyethanol/Sensiva SC50, encircle five polydimethylsiloxane/cyclohexasiloxane, glyceryl stearate/PEG-100 stearate, diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate, cetearyl alcohol/cetearyl glucoside, caprylic/capric triglyceride, polyacrylamide/C13-14 isoparaffin/laureth-7, Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate, glycerol polymethacrylates/propylene glycol, 1, 2-hexanediol/caprylyl glycol.
Embodiment 1 toner/smoothing toner
Described in the present embodiment, in toner/smoothing toner, contain Mahonia fortunei (Lindl.) Fedde extracting solution, the preparation method of described Mahonia fortunei (Lindl.) Fedde extracting solution, comprise the following steps: 1 kilogram of Mahonia fortunei (Lindl.) Fedde is cleaned, dried drying and crushing to 80 order, install with 800 order gauze bags of sterilizing, be placed in vacuum emulsifying pot, add the deionized water of 10 kilograms, extract 20min in 90 DEG C, filter, obtain Mahonia fortunei (Lindl.) Fedde extracting solution.
The component of described toner/smoothing toner and content are in table 1:
The component of table 1 toner/smoothing toner and content
| Composition | Percentage by weight (wt%) |
| Mahonia fortunei (Lindl.) Fedde extracting solution | Surplus |
| Glycerol | 5 |
| Butanediol | 4 |
| Carbomer | 0.1 |
| Allantoin | 0.15 |
| Hyaluronate sodium | 0.06 |
| Triethanolamine | 0.1 |
| Phenoxyethanol/Sensiva SC50 | 0.3 |
| Add up to | 100 |
Embodiment 2 health breasts
Described in the present embodiment, Mahonia fortunei (Lindl.) Fedde extracting solution is contained in health Ruzhong, and the preparation method of described Mahonia fortunei (Lindl.) Fedde extracting solution, comprises the following steps: 1 kilogram of Mahonia fortunei (Lindl.) Fedde is cleaned, dry, drying and crushing to 60 order, installs with 900 order gauze bags of sterilizing, gauze bag by it with sterilizing installs, be tamping, be placed in vacuum emulsifying pot, add the deionized water of 8 kilograms, in 95 DEG C of lixiviate 30min, gauze bag is taken out, and remaining solution, obtains Mahonia fortunei (Lindl.) Fedde extracting solution.
The component of described health breast and content are in table 2:
Component and the content of table 2 health breast
Embodiment 3 nourishing cream
Described in the present embodiment, in nourishing cream, contain Mahonia fortunei (Lindl.) Fedde extracting solution, the preparation method of described Mahonia fortunei (Lindl.) Fedde extracting solution, comprises the following steps: 1 kilogram of Mahonia fortunei (Lindl.) Fedde is cleaned, dry, drying and crushing to 100 order, installs with 1000 order gauze bags of sterilizing, gauze bag by it with sterilizing installs, be tamping, be placed in vacuum emulsifying pot, add the deionized water of 12 kilograms, in 100 DEG C of lixiviate 50min, gauze bag is taken out, and remaining solution, obtains Mahonia fortunei (Lindl.) Fedde extracting solution.
The component of described nourishing cream and content are in table 3:
The component of table 3 nourishing cream and content
Embodiment 4 essences
Described in the present embodiment, in essence, contain Mahonia fortunei (Lindl.) Fedde extracting solution, the preparation method of described Mahonia fortunei (Lindl.) Fedde extracting solution, with reference to embodiment 1.
The component of described essence and content are in table 4:
The component of table 4 essence and content
| Composition | Percentage by weight (wt%) |
| Mahonia fortunei (Lindl.) Fedde extracting solution | Surplus |
| EDTA-disodium | 0.02 |
| Glycerol | 5 |
| Butanediol | 5 |
| Allantoin | 0.1 |
| Methyl hydroxybenzoate | 0.1 |
| Hamamelis virginiana extract | 2 |
| Glycyrrhizic acid dipotassium | 0.05 |
| Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate | 1 |
| Aloe vulgaris leaf extract | 2 |
| Phenoxyethanol/Sensiva SC50 | 0.5 |
| Add up to | 100 |
Embodiment 5 masks
Described in the present embodiment, in mask, contain Mahonia fortunei (Lindl.) Fedde extracting solution, the preparation method of described Mahonia fortunei (Lindl.) Fedde extracting solution, with reference to embodiment 2.
The component of described mask and content are in table 5:
The component of table 5 mask and content
| Composition | Percentage by weight (wt%) |
| Mahonia fortunei (Lindl.) Fedde extracting solution | Surplus |
| Glycerol | 5 |
| Butanediol | 5 |
| Propylene glycol | 3 |
| Hydroxyethyl-cellulose | 0.05 |
| Hyaluronate sodium | 0.03 |
| Carbomer | 0.15 |
| Allantoin | 0.15 |
| Beta glucan | 1 |
| Glycerol polymethacrylates/propylene glycol | 8 |
| Ovshinsky Sargassum extract | 5 |
| Hamamelis virginiana extract | 4 |
| Potassium hydroxide | 0.06 |
| Deionized water | 1 |
| 1,2-hexanediol/caprylyl glycol | 0.5 |
| Add up to | 100 |
Comparative example 1 toner/smoothing toner
The component of described toner/smoothing toner and content are in table 6:
The component of table 6 toner/smoothing toner and content
| Composition | Percentage by weight (wt%) |
| Deionized water | Surplus |
| Glycerol | 5 |
| Butanediol | 4 |
| Carbomer | 0.1 |
| Allantoin | 0.15 |
| Hyaluronate sodium | 0.06 |
| Triethanolamine | 0.1 |
| Phenoxyethanol/Sensiva SC50 | 0.3 |
| Add up to | 100 |
Comparative example 2 health breasts
The component of described health breast and content are in table 7:
Component and the content of table 7 health breast
Comparative example 3 nourishing cream
The component of described nourishing cream and content are in table 8:
The component of table 8 nourishing cream and content
| Composition | Percentage by weight (wt%) |
| Deionized water | Surplus |
| Cetearyl alcohol/cetearyl glucoside | 2.5 |
| Cetearyl alcohol | 1.2 |
| Glyceryl stearate/PEG-100 stearate | 1.2 |
| Encircle five polydimethylsiloxane/cyclohexasiloxane | 2 |
| Polydimethylsiloxane | 2 |
| Caprylic/capric triglyceride | 3 |
| Tocopherol (vitamin E) | 0.5 |
| Propylene glycol | 5 |
| Glycerol | 5 |
| Xanthan gum | 0.1 |
| Hyaluronate sodium | 0.02 |
| Polyacrylamide/C13-14 isoparaffin/laureth-7 | 0.7 |
| Phenoxyethanol/Sensiva SC50 | 0.5 |
| Oligofructose | 0.1 |
| Add up to | 100 |
Comparative example 4 essences
The component of described essence and content are in table 9:
The component of table 9 essence and content
| Composition | Percentage by weight (wt%) |
| Deionized water | Surplus |
| EDTA-disodium | 0.02 |
| Glycerol | 5 |
| Butanediol | 5 |
| Allantoin | 0.1 |
| Methyl hydroxybenzoate | 0.1 |
| Hamamelis virginiana extract | 2 |
| Glycyrrhizic acid dipotassium | 0.05 |
| Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate | 1 |
| Aloe vulgaris leaf extract | 2 |
| Phenoxyethanol/Sensiva SC50 | 0.5 |
| Add up to | 100 |
Comparative example 5 masks
The component of described mask and content are in table 10:
The component of table 10 mask and content
| Composition | Percentage by weight (wt%) |
| Deionized water | Surplus |
| Glycerol | 5 |
| Butanediol | 5 |
| Propylene glycol | 3 |
| Hydroxyethyl-cellulose | 0.05 |
| Hyaluronate sodium | 0.03 |
| Carbomer | 0.15 |
| Allantoin | 0.15 |
| Beta glucan | 1 |
| Glycerol polymethacrylates/propylene glycol | 8 |
| Ovshinsky Sargassum extract | 5 |
| Hamamelis virginiana extract | 4 |
| Potassium hydroxide | 0.06 |
| Deionized water | 1 |
| 1,2-hexanediol/caprylyl glycol | 0.5 |
| Add up to | 100 |
Embodiment 6 effect evaluations
One, experiment purpose
Evaluate the effect of improving cutis laxa, minimizing wrinkle and black speck generation of prepared cosmetics in the various embodiments described above by relative analysis.
Two, experimental technique
This experiment is divided into experimental group and matched group, and wherein, experiment component is: embodiment 1-toner/smoothing toner, embodiment 2-health breast, embodiment 3-nourishing cream, embodiment 4-essence, embodiment 5-facial film; Matched group is comparative example 1-toner/smoothing toner, comparative example 2-health breast, comparative example 3-nourishing cream, comparative example 4-essence, comparative example 5-facial film, a certain commercially available essence that improves and repair acne skin that has.
Collect 200 volunteers above-mentioned each product on probation 28 days, trier uses identical gentle cleaning agent to clean after face, and in the selected same area in trier face left and right, as trial zone, embodiment product is smeared in left side, the corresponding comparative example product of equivalent, observed result are smeared in right side.Wherein, women 150 people, male 50 people, maximum 55 years old age, minimal ages 30 years old, 42 years old mean age.
The main manifestations of described skin aging is: cutis laxa, wrinkle, black speck, xerosis cutis, coarse or skin is matt etc.
Three, experimental result
Result is referring to table 11.
The efficacy outcomes table of table 11 experimental group and matched group
As known from Table 11: the each product of matched group is comparative example 1-toner/smoothing toner, comparative example 2-health breast, comparative example 3-nourishing cream, comparative example 4-essence, comparative example 5-facial film, the each product embodiments 1-toner/smoothing toner of a certain commercially available essence and experimental group, embodiment 2-health breast, embodiment 3-nourishing cream, embodiment 4-essence, embodiment 5-facial film is to cutis laxa, wrinkle, black speck, xerosis cutis, coarse or skin glossiness all has improvement in various degree, can find out from experimental data, in experimental group, each product is to cutis laxa, wrinkle, black speck, xerosis cutis, improvement degree coarse or skin glossiness is obviously high than the improvement degree of each product in matched group, hence one can see that, the cosmetics tool that contains Mahonia fortunei (Lindl.) Fedde extracting solution is significantly improved cutis laxa, reduce effect that wrinkle and black speck generate.
The above embodiment has only expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but can not therefore be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (10)
1. a preparation method for Mahonia fortunei (Lindl.) Fedde extracting solution, is characterized in that, comprises the following steps:
Mahonia fortunei (Lindl.) Fedde be dry, pulverize, pack the 800-1000 order gauze bag of sterilizing into, be placed in vacuum emulsifying pot, by the weight of Mahonia fortunei (Lindl.) Fedde, the deionized water that adds 8-12 doubly to measure, in 90-100 DEG C of extraction.
2. the Mahonia fortunei (Lindl.) Fedde extracting solution that preparation method as claimed in claim 1 makes.
3. Mahonia fortunei (Lindl.) Fedde extracting solution as prepared in claim 2 has the application in the cosmetics that improve cutis laxa minimizing wrinkle and black speck generation effect in preparation.
4. application according to claim 3, is characterized in that, in described cosmetics, the content of Mahonia fortunei (Lindl.) Fedde extracting solution is 58-95wt%.
5. according to the application described in claim 3 or 4, it is characterized in that, described cosmetics are toner/smoothing toner, health breast, nourishing cream, essence or mask.
6. a toner/smoothing toner, is characterized in that, described toner/smoothing toner comprises the component of following weight percentage ratio:
Wetting agent: 5-13wt%,
Thickening agent: 0.05-0.15wt%,
Antiinflammatory: 0.1-0.2wt%,
Nertralizer: 0.05-0.15wt%,
Antiseptic: 0.2-0.7wt%,
Mahonia fortunei (Lindl.) Fedde extracting solution as claimed in claim 2: surplus;
Described wetting agent is at least one in glycerol, butanediol, propylene glycol or hyaluronate sodium;
Described thickening agent is at least one in carbomer, xanthan gum or hydroxyethyl-cellulose;
Described antiinflammatory is at least one in allantoin, Flos Inulae extract or bisabolol;
Described nertralizer is at least one in triethanolamine, sodium hydroxide or potassium hydroxide;
Described antiseptic is at least one in phenoxyethanol/Sensiva SC50, DMDM beta-lactam or Kazon.
7. a health breast, is characterized in that, described health breast comprises the component of following weight percentage ratio:
Emulsifying agent: 1.5-5wt%,
Co-emulsifier: 0.8-2wt%,
Emollient: 2-8wt%,
Skinfeel regulator: 1.5-10wt%,
Thickening agent: 0.1-0.4wt%,
Wetting agent: 4-10wt%,
Antiseptic: 0.05-0.7wt%,
Mahonia fortunei (Lindl.) Fedde extracting solution as claimed in claim 2: surplus;
Described emulsifying agent is at least one in methyl glucose sesquistearate, PEG-20 methyl glucose sesquistearate or glyceryl stearate/PEG-100 stearate;
Described co-emulsifier is at least one in cetearyl alcohol, glyceryl stearate or triethanolamine;
Described emollient is at least one in isopropyl palmitate, caprylic/capric triglyceride or hydrogenated jojoba oil;
Described skinfeel regulator is at least one in ring five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane or vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer;
Described thickening agent is at least one in xanthan gum, hydroxyethyl-cellulose or carbomer;
Described wetting agent is at least one in propylene glycol, glycerol or butanediol;
Described antiseptic is at least one in diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate, propyl hydroxybenzoate or methyl hydroxybenzoate.
8. a nourishing cream, is characterized in that, described nourishing cream comprises the component of following weight percentage ratio:
Emulsifying agent: 3.5-6.3wt%,
Emollient: 5-10wt%,
Antioxidant: 0.2-0.8wt%,
Wetting agent: 5-15wt%,
Thickening agent: 0.05-0.15wt%,
Antiseptic: 0.3-0.7wt%,
Mahonia fortunei (Lindl.) Fedde extracting solution as claimed in claim 2: surplus;
Described emulsifying agent is at least one in cetearyl alcohol/cetearyl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearate, polyacrylamide/C13-14 isoparaffin/laureth-7 or methyl glucose sesquistearate;
Described emollient is at least one in ring five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane, caprylic/capric triglyceride or hydrogenated jojoba oil;
Described antioxidant is at least one that tocopherol or fan change in extract;
Described wetting agent is at least one in propylene glycol, glycerol, hyaluronate sodium, oligofructose or sorbitol;
Described thickening agent is at least one in xanthan gum or sodium carboxymethyl cellulose;
Described antiseptic is at least one in phenoxyethanol/Sensiva SC50, sodium benzoate or germall.
9. an essence, is characterized in that, described essence comprises the component of following weight percentage ratio:
Chelating agen: 0.01-0.1wt%,
Wetting agent: 5-18wt%,
Antiinflammatory: 0.05-2.5wt%,
Antiseptic: 0.3-0.66wt%,
Mahonia fortunei (Lindl.) Fedde extract as claimed in claim 2: surplus;
Described chelating agen is at least one in EDTA-disodium or Etidronic Acid;
Described wetting agent is at least one in glycerol, propylene glycol, Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate, Aloe vulgaris leaf extract or PEG400;
Described antiinflammatory is at least one in allantoin, Hamamelis virginiana extract, glycyrrhizic acid dipotassium or Flos Inulae extract;
Described antiseptic is at least one in methyl hydroxybenzoate, phenoxyethanol/Sensiva SC50 or Kazon.
10. a mask, is characterized in that, described mask comprises the component of following weight percentage ratio:
Wetting agent: 5-35wt%,
Thickening agent: 0.05-0.3wt%,
Antiinflammatory: 2.5-5.5wt%,
PH adjusting agent: 0.04-0.08wt%,
Antiseptic: 0.2-0.6wt%,
Mahonia fortunei (Lindl.) Fedde extract as claimed in claim 2: surplus;
Described wetting agent is at least one in glycerol, butanediol, propylene glycol, hyaluronate sodium, glycerol polymethacrylates/propylene glycol, Ovshinsky Sargassum extract, beta glucan or oligofructose;
Described thickening agent is at least one in hydroxyethyl-cellulose, carbomer or xanthan gum;
Described antiinflammatory is at least one in allantoin, Hamamelis virginiana extract or bisabolol;
Described pH adjusting agent is at least one in triethanolamine, potassium hydroxide or sodium hydroxide;
Described antiseptic is at least one in 1,2-hexanediol/caprylyl glycol or phenoxyethanol/Sensiva SC50.
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105534829A (en) * | 2016-03-02 | 2016-05-04 | 广州丹奇日用化工厂有限公司 | Anti-aging plant extract composition and application thereof to cosmetics |
| CN105616522A (en) * | 2016-03-02 | 2016-06-01 | 广州千百度化妆品有限公司 | Traditional Chinese medicine acne cream |
| CN106176483A (en) * | 2016-08-31 | 2016-12-07 | 南京禾宇化工有限公司 | A kind of Fructus Hippophae cervical region essence |
| CN107126390A (en) * | 2017-05-13 | 2017-09-05 | 佛山文森特知识产权服务有限公司 | A kind of man's skin care cosmetic compositions |
| CN107137263A (en) * | 2017-04-19 | 2017-09-08 | 北京赛尔佳人化妆品有限公司 | A kind of anti-ageing face mask liquid and preparation method thereof |
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| CN107823003A (en) * | 2017-12-08 | 2018-03-23 | 佛山实瑞先导材料研究院（普通合伙） | A kind of skin conditioning composition |
| CN109481322A (en) * | 2018-10-10 | 2019-03-19 | 广州雷诺生物科技有限公司 | A kind of fullerene essence cream |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105534829A (en) * | 2016-03-02 | 2016-05-04 | 广州丹奇日用化工厂有限公司 | Anti-aging plant extract composition and application thereof to cosmetics |
| CN105616522A (en) * | 2016-03-02 | 2016-06-01 | 广州千百度化妆品有限公司 | Traditional Chinese medicine acne cream |
| CN106176483A (en) * | 2016-08-31 | 2016-12-07 | 南京禾宇化工有限公司 | A kind of Fructus Hippophae cervical region essence |
| CN107137263A (en) * | 2017-04-19 | 2017-09-08 | 北京赛尔佳人化妆品有限公司 | A kind of anti-ageing face mask liquid and preparation method thereof |
| CN107126390A (en) * | 2017-05-13 | 2017-09-05 | 佛山文森特知识产权服务有限公司 | A kind of man's skin care cosmetic compositions |
| CN107412095A (en) * | 2017-05-17 | 2017-12-01 | 秀瑞斯（天津）科技有限公司 | Evil spirit thin slim formula, preparation method and application method |
| CN107823003A (en) * | 2017-12-08 | 2018-03-23 | 佛山实瑞先导材料研究院（普通合伙） | A kind of skin conditioning composition |
| CN109481322A (en) * | 2018-10-10 | 2019-03-19 | 广州雷诺生物科技有限公司 | A kind of fullerene essence cream |
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