CN103976914A - China creeper root extracting solution as well as preparation method and application thereof - Google Patents
China creeper root extracting solution as well as preparation method and application thereof Download PDFInfo
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- CN103976914A CN103976914A CN201410238492.8A CN201410238492A CN103976914A CN 103976914 A CN103976914 A CN 103976914A CN 201410238492 A CN201410238492 A CN 201410238492A CN 103976914 A CN103976914 A CN 103976914A
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- extracting solution
- toner
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- radix parthenocissi
- parthenocissi heterophyllae
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- 238000009499 grossing Methods 0.000 claims description 21
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- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims description 6
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- HHGZABIIYIWLGA-UHFFFAOYSA-N bisabolol Natural products CC1CCC(C(C)(O)CCC=C(C)C)CC1 HHGZABIIYIWLGA-UHFFFAOYSA-N 0.000 claims description 2
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- Cosmetics (AREA)
Abstract
The invention discloses a china creeper root extracting solution as well as a preparation method and application thereof. The china creeper root extracting solution prepared in a water extraction manner has significant effects of inhibiting the activity of pathogenic microorganisms, removing inflammation and restraining cutin cell hyperplasia. The china creeper root extracting solution has the effects of resisting bacterial infection, repairing connective tissue with inflammatory damage, improving the skin immunity and preventing excessive diversification of hair follicle cells, and has significant efficacy of improving and repairing acne skin when being applied to cosmetics.
Description
Technical field
The present invention relates to cosmetic field, particularly relate to a kind of Radix Parthenocissi Heterophyllae extracting solution and its preparation method and application.
Background technology
Along with the raising of people's living standard, having healthy and beautiful skin is that each female friend that likes to be beautiful yearns for, so people are more and more higher to the prescription of cosmetics, not only require effective, and require be free from side effects.Along with the development of cosmetics industry, natural plants series products due to its use safety, action temperature and, the advantage such as the successful parent that is subject to consumers in general looks at.Be generally to obtain by corresponding processing the plant extract that contains effective ingredient, and add in cosmetics.
The at present plant extract in cosmetics, mostly adopts the methods such as water extraction, alcohol extraction, ultrasonic extraction, microwave extraction to extract gained, extraction process complexity, through operations such as concentrate dryings, also to add antiseptic so that the shelf-life of extract more permanent.The drawback of bringing like this, one is waste resource, and in leaching process, solution is concentrated, generally only gets concentrated fraction elite out, and most solutions discards.This part solution also contains other effective ingredient in fact, can again utilize, and directly discard the waste that has just caused resource.Another drawback is in extract, add antiseptic no doubt can make extract obtain the longer shelf-life, but the while to be also for skin brings sensitization source.
Acne is the common a kind of chronic inflammatory disease dermatosis of adolescence, is also common in the middle age in 30-40 year, brings very large misery usually to patient's spirit psychology and even the human body.Cause the basic reason of acne skin to be: hypersteatosis, the dyskeratosis of pilosebaceous duct adds that the absorption such as extraneous dust cause conduit to stop up simultaneously, dyssebacia, especially propionibacterium acnes amount reproduction of multiple-microorganism in hair follicle, the lipase that propionibacterium acnes produces decomposes sebum and generates free fatty, chemotactic inflammatory cell and medium simultaneously, final induction exacerbate inflammation reaction, thereby make skin produce acne, inflammatory pimple, pustule, even occur the symptoms such as cyst.
Therefore, select which kind of plant, how simple, safety, effectively this plant extract is carried out, and being applied to of its safety improved in cosmetics and repaired acne skin, be problem demanding prompt solution.
Summary of the invention
Based on this, the object of the invention is to provide a kind of Radix Parthenocissi Heterophyllae extracting solution and its preparation method and application.
The concrete technical scheme solving the problems of the technologies described above is as follows:
A preparation method for Radix Parthenocissi Heterophyllae extracting solution, comprises the following steps:
By Radix Parthenocissi Heterophyllae drying and crushing, install with the 800-1000 order gauze bag of sterilizing, be placed in vacuum emulsifying pot, by the weight of Radix Parthenocissi Heterophyllae, the deionized water that adds 8-12 doubly to measure, in 90-100 DEG C of extraction, can make Radix Parthenocissi Heterophyllae extracting solution.
In some embodiment, the time of described extraction is 20-50min therein.
Therein in some embodiment, by Radix Parthenocissi Heterophyllae drying and crushing, install with the 800-1000 order gauze bag of sterilizing, be placed in vacuum emulsifying pot, after having extracted, directly gauze bag is taken out, remaining solution is Radix Parthenocissi Heterophyllae extracting solution.In the method, owing to adopting vacuum emulsifying pot, it can, after extraction completes, directly be added other cosmetics adjuvants, carries out Cosmetic Manufacture, and does not need to extract with special herbal extraction equipment, has saved cost; In addition, adopt gauze packed Radix Parthenocissi Heterophyllae powder, extracted and directly gauze bag has been taken out afterwards, need not filter, simplification extraction process, raises the efficiency.
Said method is simple to operation, and the Radix Parthenocissi Heterophyllae extract use of can now withdrawing deposit, does not need to add antiseptic, significantly reduces the sensitization source to skin.In cosmetic formulations, itself is just added with antiseptic, and extract of the present invention is now carried and being added, and has avoided producing spoilage problems because of placement.
The prepared Radix Parthenocissi Heterophyllae extracting solution of said method has the application in the cosmetics that improve and repair acne skin effect in preparation.
In some embodiment, the content of described cosmetics intermediate cam wind extracting solution is 58-95wt% therein.
In some embodiment, described cosmetics are toner/smoothing toner therein.
The invention provides a kind of toner/smoothing toner, described toner/smoothing toner comprises the component of following weight percentage ratio:
Thickening agent: 0.1-0.6wt%,
Wetting agent: 0.5-2.7wt%,
Antiinflammatory: 0.1-0.4wt%,
Nertralizer: 0.1-0.15wt%,
Opacifier: 0.05-0.15wt%,
Antiseptic: 0.2-0.7wt%,
Radix Parthenocissi Heterophyllae extracting solution as claimed in claim 2: surplus;
Described thickening agent is at least one in carbomer, xanthan gum or hydroxyethyl-cellulose;
Described wetting agent is at least one in glycerol, sorbitol, propylene glycol or hyaluronate sodium;
Described antiinflammatory is at least one in allantoin, Flos Inulae extract or bisabolol;
Described nertralizer is at least one in triethanolamine, sodium hydroxide or potassium hydroxide;
Described opacifier is styrene/acrylic (ester) analog copolymer;
Described antiseptic is phenoxyethanol/Sensiva SC50,1, at least one in 2-hexanediol/caprylyl glycol or Kazon.
In some embodiment, described toner/smoothing toner comprises the component of following weight percentage ratio therein:
Thickening agent: 0.2-0.5wt%,
Wetting agent: 0.6-2.6wt%,
Antiinflammatory: 0.1-0.3wt%,
Nertralizer: 0.1-0.15wt%,
Opacifier: 0.05-0.1wt%,
Antiseptic: 0.3-0.6wt%,
The Radix Parthenocissi Heterophyllae extracting solution that above-mentioned preparation method makes: surplus;
Described thickening agent is at least one in carbomer, hydroxyethyl-cellulose;
Described wetting agent is at least one in glycerol, sorbitol, propylene glycol or hyaluronate sodium;
Described antiinflammatory is allantoin;
Described nertralizer is triethanolamine;
Described opacifier is styrene/acrylic (ester) analog copolymer;
Described antiseptic is 1,2-hexanediol/caprylyl glycol.
In some embodiment, described toner/smoothing toner comprises the component of following weight percentage ratio therein:
Hydroxyethyl-cellulose: 0.1-0.3wt%,
Carbomer: 0.1-0.15wt%,
Propylene glycol: 0.5-2.5wt%,
Hyaluronate sodium: 0.02-0.06wt%,
Allantoin 0.1-0.3wt%,
Triethanolamine: 0.1-0.15wt%,
Styrene/acrylic (ester) analog copolymer: 0.05-0.08wt%,
1,2-hexanediol/caprylyl glycol: 0.3-0.6wt%,
The Radix Parthenocissi Heterophyllae extracting solution that above-mentioned preparation method makes: surplus.
A kind of Radix Parthenocissi Heterophyllae extracting solution of the present invention and its preparation method and application has the following advantages and beneficial effect:
The present invention is through a large amount of experiment of inventor and research, draw at optimum process---prepared Radix Parthenocissi Heterophyllae extracting solution under water extraction, it has significant inhibition pathogenic microorganism activity, diminish inflammation, suppress horn cell proliferative effect, this specific character makes Radix Parthenocissi Heterophyllae extracting solution possess bacterial-infection resisting, repair the connective tissue of inflammatory damage, improve skin immunization power, prevent the Hyperkeratotic effect of hair follicle cell, be applied to effect that in cosmetics, tool was significantly improved and repaired acne skin.
Detailed description of the invention
Radix Parthenocissi Heterophyllae of the present invention is root or the stem of vitaceae great Ye parthenocissus, is born in hill, and south China all has distribution.Radix Parthenocissi Heterophyllae bitter in the mouth is warm in nature, nontoxic, has expelling wind and removing dampness, dredging collateral, hemostasis, Detoxication." Guizhou folk medicine ": " dispel the wind, removing toxic substances, synthetism." " Tianmu Mountains of Zhejiang Province medicine is planted will ": " control furuncle poison, wound." " Zhejiang conventional medical herbs among the people ": " wind-damp dispelling, the meridian dredging, hemostasis." the present invention makes Radix Parthenocissi Heterophyllae extracting solution by Radix Parthenocissi Heterophyllae through water extraction, use it for preparation and have and improve and repair in acne cosmetics for skin.
Below with reference to specific embodiment, the present invention will be further described.
In following embodiment, described raw material is commercially available prod.
In following examples, composition title used is international cosmetic raw material name (International NomenclatureCosmeticIngredient, INCI) title of defined, for example styrene/acrylic (ester) analog copolymer, 1,2-hexanediol/caprylyl glycol.
Embodiment 1 toner/smoothing toner
Described in the present embodiment, in toner/smoothing toner, contain Radix Parthenocissi Heterophyllae extracting solution, the preparation method of described Radix Parthenocissi Heterophyllae extracting solution, comprise the following steps: 1 kilogram of Radix Parthenocissi Heterophyllae is cleaned, dried drying and crushing to 80 order, install with 800 order gauze bags of sterilizing, be placed in vacuum emulsifying pot, add the deionized water of 10 kilograms, extract 20min in 90 DEG C, filter, obtain Radix Parthenocissi Heterophyllae extracting solution.
The component of described toner/smoothing toner and content are in table 1:
The component of table 1 toner/smoothing toner and content
| Composition | Percentage by weight (wt%) |
| Radix Parthenocissi Heterophyllae extracting solution | Surplus |
| Hydroxyethyl-cellulose | 0.2 |
| Carbomer | 0.12 |
| Propylene glycol | 2 |
| Hyaluronate sodium | 0.04 |
| Allantoin | 0.2 |
| Triethanolamine | 0.12 |
| Styrene/acrylic (ester) analog copolymer | 0.07 |
| 1,2-hexanediol/caprylyl glycol | 0.5 |
| Add up to | 100 |
Comparative example 1 toner/smoothing toner
The component of described toner/smoothing toner and content are in table 2:
The component of table 2 toner/smoothing toner and content
| Composition | Percentage by weight (wt%) |
| Deionized water | Surplus |
| Hydroxyethyl-cellulose | 0.2 |
| Carbomer | 0.12 |
| Propylene glycol | 2 |
| Hyaluronate sodium | 0.04 |
| Allantoin | 0.2 |
| Triethanolamine | 0.12 |
| Styrene/acrylic (ester) analog copolymer | 0.07 |
| 1,2-hexanediol/caprylyl glycol | 0.5 |
| Add up to | 100 |
Embodiment 2 effect evaluations
One, experiment purpose
Evaluate the improvement of prepared cosmetics in the various embodiments described above and the effect of repairing acne skin by relative analysis.
Two, experimental technique
This experiment is divided into experimental group and matched group, and wherein, experimental group is: embodiment 1-toner/smoothing toner; Matched group is comparative example 1-toner/smoothing toner, a certain commercially available toner/smoothing toner that improves and repair acne skin that has.
Collect 200 volunteers above-mentioned each product on probation 28 days, trier uses identical cleaning agent to clean after face, and in the selected same area in trier face left and right, as trial zone, embodiment product is smeared in left side, the corresponding comparative example product of equivalent, observed result are smeared in right side.Wherein, women 60 people, male 140 people, maximum 30 years old age, minimal ages 14 years old, 20 years old mean age.
The main manifestations of described acne skin is: face length has acne, corse sweat pore, inflammation, red point, local glossy, and severe patient has pustule etc.
Three, experimental result
Result is referring to table 3
The efficacy outcomes table of table 3 experimental group and matched group
Know from table 3: matched group product is comparative example 1-toner/smoothing toner, a certain commercially available toner/smoothing toner and experimental group product embodiments 1-toner/smoothing toner opposite minister have acne, corse sweat pore, inflammation, red point, local glossy, pustule all has improvement in various degree, can find out from experimental data, in experimental group, product opposite minister has acne, corse sweat pore, inflammation, red point, local glossy, the improvement degree of pustule is obviously high than the improvement degree of each product in matched group, hence one can see that, the cosmetics tool that contains Radix Parthenocissi Heterophyllae extracting solution is significantly improved and repairs effect of acne skin.
The above embodiment has only expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but can not therefore be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (6)
1. a preparation method for Radix Parthenocissi Heterophyllae extracting solution, is characterized in that, comprises the following steps:
Radix Parthenocissi Heterophyllae be dry, pulverize, pack the 800-1000 order gauze bag of sterilizing into, be placed in vacuum emulsifying pot, by the weight of Radix Parthenocissi Heterophyllae, the deionized water that adds 8-12 doubly to measure, in 90-100 DEG C of extraction.
2. the Radix Parthenocissi Heterophyllae extracting solution that preparation method as claimed in claim 1 makes.
3. Radix Parthenocissi Heterophyllae extracting solution as prepared in claim 2 has the application in the cosmetics that improve and repair acne skin effect in preparation.
4. application according to claim 3, is characterized in that, the content of described cosmetics intermediate cam wind extracting solution is 58-95wt%.
5. according to the application described in claim 3 or 4, it is characterized in that, described cosmetics are toner/smoothing toner.
6. a toner/smoothing toner, is characterized in that, described toner/smoothing toner comprises the component of following weight percentage ratio:
Thickening agent: 0.1-0.6wt%,
Wetting agent: 0.5-2.7wt%,
Antiinflammatory: 0.1-0.4wt%,
Nertralizer: 0.1-0.15wt%,
Opacifier: 0.05-0.15wt%,
Antiseptic: 0.2-0.7wt%,
Radix Parthenocissi Heterophyllae extracting solution as claimed in claim 2: surplus;
Described thickening agent is at least one in carbomer, xanthan gum or hydroxyethyl-cellulose;
Described wetting agent is at least one in glycerol, sorbitol, propylene glycol or hyaluronate sodium;
Described antiinflammatory is at least one in allantoin, Flos Inulae extract or bisabolol;
Described nertralizer is at least one in triethanolamine, sodium hydroxide or potassium hydroxide;
Described opacifier is styrene/acrylic (ester) analog copolymer;
Described antiseptic is phenoxyethanol/Sensiva SC50,1, at least one in 2-hexanediol/caprylyl glycol or Kazon.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104547306A (en) * | 2014-12-11 | 2015-04-29 | 无锡市第三人民医院 | Method for preparing parthenocissus dalzielii extract and anti-osteoporosis medicine |
| CN105662968A (en) * | 2016-03-02 | 2016-06-15 | 广州千百度化妆品有限公司 | Face cleanser for removing acne marks |
| CN105748351A (en) * | 2016-03-04 | 2016-07-13 | 佛山市聚成生化技术研发有限公司 | Plant composition and application thereof |
| CN107998039A (en) * | 2018-01-23 | 2018-05-08 | 璧电健 | Natural crease-resistant smoothing wrinkle composition for cosmetics |
| CN108078858A (en) * | 2018-01-23 | 2018-05-29 | 璧电健 | For the natural smoothing wrinkle moisture-keeping composition of cosmetics |
| CN110694015A (en) * | 2019-10-09 | 2020-01-17 | 江苏省中医院 | Acne removing gel and preparation method thereof |
| CN111961702A (en) * | 2020-07-22 | 2020-11-20 | 上海珈蓓生物科技有限公司 | Cytological evaluation method for anti-skin infectious inflammatory reaction of plant extract and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103656349A (en) * | 2013-12-15 | 2014-03-26 | 卞永兴 | Traditional Chinese medicine complexing agent used for treatment of acne vulgaris |
-
2014
- 2014-05-30 CN CN201410238492.8A patent/CN103976914B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103656349A (en) * | 2013-12-15 | 2014-03-26 | 卞永兴 | Traditional Chinese medicine complexing agent used for treatment of acne vulgaris |
Non-Patent Citations (2)
| Title |
|---|
| 冉先德: "《中华药海》", 31 August 1993, 哈尔滨出版社 * |
| 唐宇龙等: ""三角风化学成分分析与抗菌效果研究"", 《中国兽医杂志》 * |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104547306A (en) * | 2014-12-11 | 2015-04-29 | 无锡市第三人民医院 | Method for preparing parthenocissus dalzielii extract and anti-osteoporosis medicine |
| CN104547306B (en) * | 2014-12-11 | 2019-03-15 | 无锡市第三人民医院 | Prepare the method and osteosporosis resistant medicament of different leaf Radix seu Caulis Parthenocissi tricuspidatae extract |
| CN105662968A (en) * | 2016-03-02 | 2016-06-15 | 广州千百度化妆品有限公司 | Face cleanser for removing acne marks |
| CN105748351A (en) * | 2016-03-04 | 2016-07-13 | 佛山市聚成生化技术研发有限公司 | Plant composition and application thereof |
| CN107998039A (en) * | 2018-01-23 | 2018-05-08 | 璧电健 | Natural crease-resistant smoothing wrinkle composition for cosmetics |
| CN108078858A (en) * | 2018-01-23 | 2018-05-29 | 璧电健 | For the natural smoothing wrinkle moisture-keeping composition of cosmetics |
| CN110694015A (en) * | 2019-10-09 | 2020-01-17 | 江苏省中医院 | Acne removing gel and preparation method thereof |
| CN111961702A (en) * | 2020-07-22 | 2020-11-20 | 上海珈蓓生物科技有限公司 | Cytological evaluation method for anti-skin infectious inflammatory reaction of plant extract and application thereof |
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