CN103976923A - Japanese saussurea herb extracting solution as well as preparation method and application thereof - Google Patents
Japanese saussurea herb extracting solution as well as preparation method and application thereof Download PDFInfo
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- CN103976923A CN103976923A CN201410242375.9A CN201410242375A CN103976923A CN 103976923 A CN103976923 A CN 103976923A CN 201410242375 A CN201410242375 A CN 201410242375A CN 103976923 A CN103976923 A CN 103976923A
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Abstract
The invention discloses a Japanese saussurea herb extracting solution as well as a preparation method and application thereof. The Japanese saussurea herb extracting solution prepared in a water extract manner is obtained by a lot of experiments and researches of the inventor. The Japanese saussurea herb extracting solution has the characteristic that skin contact anaphylaxis is significantly removed, so that cosmetics containing the Japanese saussurea herb extracting solution have good action on people with sensitive skin, and the using effects of the cosmetics on people with sensitive skin are improved.
Description
Technical field
The present invention relates to cosmetic field, particularly relate to a kind of Herba Saussuseae Japonicae extracting solution and its preparation method and application.
Background technology
Along with the raising of people's living standard, cosmetics have become necessary article in people's life.But the crowd of responsive skin.Along with the development of cosmetics industry, natural plants series products due to use safety, action temperature and, the advantage such as successful welcome.Be generally to obtain by corresponding processing the plant extract that contains effective ingredient, and add in cosmetics.
The at present plant extract in cosmetics, mostly adopts the methods such as water extraction, alcohol extraction, ultrasonic extraction, microwave extraction to extract gained, extraction process complexity, through operations such as concentrate dryings, also to add antiseptic so that the shelf-life of extract more permanent.The drawback of bringing like this, one is waste resource, and in leaching process, solution is concentrated, generally only gets concentrated fraction elite out, and most solutions is thrown away.This part solution still can contain active component in fact, can also again utilize.Directly throw away the waste that has just caused resource.Another drawback is add antiseptic no doubt can make extract obtain the longer shelf-life, but the while to be also for skin brings sensitization source.
Sensitive skin is that current cosmetics circle personage wants a difficult problem of capturing.Cause the basic reason of responsive skin to be: Skin Cell is impaired and make the immunity degradation of skin, and stratum corneum gets thinner causes skin moisturizing degree inadequate, finally causes the barrier function of skin too weak, cannot resist environmental stimuli.Then the nerve fiber of skin is owing to being often subject to environmental stimuli, too excited, thus be easy to produce general red, heating, pruritus, twinge, the generation of the uncomfortable phenomenon such as erythema.
Herba Saussuseae Japonicae is the herb of feverfew hieracioides, is distributed widely in China various places, and in " decoction pieces is newly joined ", recording it has promoting blood circulation by removing wind, effect of loose numbness pain relieving.And modern study shows, Herba Saussuseae Japonicae has certain curative effect for skin allergy.
How simple, safety, effectively extract plant Herba Saussuseae Japonicae, and by being applied in cosmetics of its safety, protection sensitive skin, is problem demanding prompt solution.
Summary of the invention
Based on this, the object of the invention is to provide a kind of Herba Saussuseae Japonicae extracting solution and its preparation method and application.
The concrete technical scheme solving the problems of the technologies described above is as follows:
A preparation method for Herba Saussuseae Japonicae extracting solution, comprises the following steps:
By Herba Saussuseae Japonicae drying and crushing, install with 800 order gauze bags of sterilizing, be placed in vacuum emulsifying pot, by the weight of Herba Saussuseae Japonicae, the deionized water that adds 8-12 doubly to measure, in 90-100 DEG C of extraction, can make Herba Saussuseae Japonicae extracting solution.
In some embodiment, the time of described extraction is 20-50min therein.
Therein in some embodiment, by Herba Saussuseae Japonicae drying and crushing, install with 800 order gauze bags of sterilizing, be placed in vacuum emulsifying pot, after having extracted, directly gauze bag is taken out, remaining solution is Herba Saussuseae Japonicae extracting solution.In the method, owing to adopting vacuum emulsifying pot, it can, after extraction completes, directly be added other cosmetics adjuvants, carries out Cosmetic Manufacture, and does not need to extract with special herbal extraction equipment, has saved cost; In addition, adopt gauze packed Herba Saussuseae Japonicae powder, extracted and directly gauze bag has been taken out afterwards, need not filter, simplification extraction process, raises the efficiency.
The Herba Saussuseae Japonicae extract that said method the makes use of can now withdrawing deposit, does not need to add antiseptic, and skin is reduced to sensitization source.In cosmetic formulations, itself is just added with antiseptic, and extract of the present invention is now carried and being added, and has avoided producing spoilage problems because of placement.
The prepared Herba Saussuseae Japonicae extracting solution of said method has the application in the cosmetics of repairing and protecting sensitive skin effect in preparation.
In some embodiment, in described cosmetics, the content of Herba Saussuseae Japonicae extracting solution is 58-95wt% therein.
In some embodiment, described cosmetics are toner/smoothing toner, health breast, nourishing cream, essence or facial film therein.
The invention provides a kind of toner/smoothing toner, described toner/smoothing toner comprises the component of following weight percentage ratio:
Wetting agent: 5-13wt%,
Thickening agent: 0.05-0.15wt%,
Antiinflammatory: 0.1-0.2wt%,
Nertralizer: 0.05-0.15wt%,
Antiseptic: 0.2-0.7wt%,
The Herba Saussuseae Japonicae extracting solution that above-mentioned preparation method makes: surplus;
Described wetting agent is at least one in glycerol, butanediol, propylene glycol or hyaluronate sodium;
Described thickening agent is at least one in carbomer, xanthan gum or hydroxyethyl-cellulose;
Described antiinflammatory is at least one in allantoin, Flos Inulae extract or bisabolol;
Described nertralizer is at least one in triethanolamine, sodium hydroxide or potassium hydroxide;
Described antiseptic is at least one in phenoxyethanol/Sensiva SC50, DMDM beta-lactam or Kazon.
Therein in some embodiment, described toner/smoothing toner, comprises the component of following weight percentage ratio:
Glycerol: 4-6wt%,
Butanediol: 3-5wt%,
Carbomer: 0.09-0.11wt%,
Allantoin 0.13-0.17wt%,
Hyaluronate sodium: 0.05-0.07wt%,
Triethanolamine: 0.09-0.11wt%,
Phenoxyethanol/Sensiva SC50: 0.2-0.4wt%,
The Herba Saussuseae Japonicae extracting solution that above-mentioned preparation method makes: surplus.
The present invention also provides a kind of health breast, and described health breast comprises the component of following weight percentage ratio:
Emulsifying agent: 1.5-5wt%,
Co-emulsifier: 0.8-2wt%,
Emollient: 2-8wt%,
Skinfeel regulator: 1.5-10wt%,
Thickening agent: 0.1-0.4wt%,
Wetting agent: 4-10wt%,
Antiseptic: 0.05-0.7wt%,
The Herba Saussuseae Japonicae extracting solution that above-mentioned preparation method makes: surplus;
Described emulsifying agent is at least one in methyl glucose sesquistearate, PEG-20 methyl glucose sesquistearate or glyceryl stearate/PEG-100 stearate;
Described co-emulsifier is at least one in cetearyl alcohol, glyceryl stearate or triethanolamine;
Described emollient is at least one in isopropyl palmitate, caprylic/capric triglyceride or hydrogenated jojoba oil;
Described skinfeel regulator is at least one in ring five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane or vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer;
Described thickening agent is at least one in xanthan gum, hydroxyethyl-cellulose or carbomer;
Described wetting agent is at least one in propylene glycol, glycerol or butanediol;
Described antiseptic is at least one in diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate, propyl hydroxybenzoate or methyl hydroxybenzoate.
In some embodiment, described health breast comprises the component of following weight percentage ratio therein:
Methyl glucose sesquistearate: 1.1-1.5wt%,
PEG-20 methyl glucose sesquistearate: 0.8-1.0wt%,
Isopropyl palmitate: 3-5wt%,
Encircle five polydimethylsiloxane/cyclohexasiloxane: 4-6wt%,
Glyceryl stearate/PEG-100 stearate: 0.6-0.8wt%,
Cetearyl alcohol: 1.1-1.3wt%,
Polydimethylsiloxane: 1.8-2.2wt%,
Methyl hydroxybenzoate: 0.15-0.25wt%,
Propyl hydroxybenzoate: 0.09-0.11wt%,
Xanthan gum: 0.25-0.35wt%,
Propylene glycol: 4-6wt%,
Diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate: 0.18-0.22wt%,
Above-mentioned Herba Saussuseae Japonicae extracting solution: surplus.
The invention provides a kind of nourishing cream, described nourishing cream comprises the component of following weight percentage ratio:
Emulsifying agent: 3.5-6.3wt%,
Emollient: 5-10wt%,
Antioxidant: 0.2-0.8wt%,
Wetting agent: 5-15wt%,
Thickening agent: 0.05-0.15wt%,
Antiseptic: 0.3-0.7wt%,
The Herba Saussuseae Japonicae extracting solution that above-mentioned preparation method makes: surplus,
Described emulsifying agent is at least one in cetearyl alcohol/cetearyl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearate, polyacrylamide/C13-14 isoparaffin/laureth-7 or methyl glucose sesquistearate;
Described emollient is at least one in ring five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane, caprylic/capric triglyceride or hydrogenated jojoba oil;
Described antioxidant is at least one that tocopherol or fan change in extract;
Described wetting agent is at least one in propylene glycol, glycerol, hyaluronate sodium, oligofructose or sorbitol;
Described thickening agent is at least one in xanthan gum or sodium carboxymethyl cellulose;
Described antiseptic is at least one in phenoxyethanol/Sensiva SC50, sodium benzoate or germall.
In some embodiment, described nourishing cream comprises the component of following weight percentage ratio therein:
Cetearyl alcohol/cetearyl glucoside: 2.3-2.7wt%,
Cetearyl alcohol: 1-1.4wt%,
Glyceryl stearate/PEG-100 stearate 1-1.4wt%,
Encircle five polydimethylsiloxane/cyclohexasiloxane: 1.8-2.2wt%,
Polydimethylsiloxane: 1.8-2.2wt%,
Caprylic/capric triglyceride: 2.8-3.2wt%,
Tocopherol: 0.4-0.6wt%,
Propylene glycol: 4-6wt%,
Glycerol: 4-6wt%,
Xanthan gum: 0.09-0.11wt%,
Hyaluronate sodium: 0.015-0.025wt%,
Polyacrylamide/C13-14 isoparaffin/laureth-7:0.6-0.8wt%,
Phenoxyethanol/Sensiva SC50: 0.4-0.6wt%,
Oligofructose: 0.08-0.11wt%,
Above-mentioned Herba Saussuseae Japonicae extracting solution: surplus.
The present invention also provides a kind of essence, and described essence comprises the component of following weight percentage ratio:
Chelating agen: 0.01-0.1wt%,
Wetting agent: 5-18wt%,
Antiinflammatory: 0.05-2.5wt%,
Antiseptic: 0.3-0.6wt%,
The Herba Saussuseae Japonicae extract that above-mentioned preparation method makes: surplus;
Described chelating agen is at least one in EDTA-disodium or Etidronic Acid;
Described wetting agent is at least one in glycerol, propylene glycol, Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate, Aloe vulgaris leaf extract or PEG400;
Described antiinflammatory is at least one in allantoin, Hamamelis virginiana extract, glycyrrhizic acid dipotassium or Flos Inulae extract;
Described antiseptic is at least one in methyl hydroxybenzoate, phenoxyethanol/Sensiva SC50 or Kazon.
In some embodiment, described essence comprises the component of following weight percentage ratio therein:
EDTA-disodium: 0.018-0.022wt%,
Glycerol: 4-6wt%,
Propylene glycol: 4-6wt%,
Allantoin: 0.09-0.11wt%,
Methyl hydroxybenzoate: 0.09-0.11wt%,
Hamamelis virginiana extract: 1.8-2.2wt%,
Glycyrrhizic acid dipotassium: 0.045-0.055wt%,
Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate: 0.9-1.1wt%,
Aloe vulgaris leaf extract: 1.8-2.2wt%,
Phenoxyethanol/Sensiva SC50: 0.45-0.55,
Above-mentioned Herba Saussuseae Japonicae extracting solution: surplus.
The present invention also provides a kind of mask, and described mask comprises the component of following weight percentage ratio:
Wetting agent: 5-35wt%,
Thickening agent: 0.05-0.3wt%,
Antiinflammatory: 2.5-5.5wt%,
PH adjusting agent: 0.04-0.08wt%,
Antiseptic: 0.2-0.66wt%,
Above-mentioned Herba Saussuseae Japonicae extract: surplus;
Described wetting agent is at least one in glycerol, butanediol, propylene glycol, hyaluronate sodium, glycerol polymethacrylates/propylene glycol, Ovshinsky Sargassum extract, beta glucan or oligofructose;
Described thickening agent is at least one in hydroxyethyl-cellulose, carbomer or xanthan gum;
Described antiinflammatory is at least one in allantoin, Hamamelis virginiana extract or bisabolol;
Described pH adjusting agent is at least one in triethanolamine, potassium hydroxide or sodium hydroxide;
Described antiseptic is at least one in 1,2-hexanediol/caprylyl glycol or phenoxyethanol/Sensiva SC50.
In some embodiment, described mask comprises the component of following weight percentage ratio therein:
Glycerol: 4-6wt%,
Butanediol: 4-6wt%,
Propylene glycol: 2-4wt%,
Hydroxyethyl-cellulose: 0.04-0.06wt%,
Hyaluronate sodium: 0.025-0.035wt%,
Carbomer: 0.1-0.2wt%,
Allantoin: 0.1-0.2wt%,
Beta glucan: 0.8-1.2wt%,
Glycerol polymethacrylates/propylene glycol: 7-9wt%,
Ovshinsky Sargassum extract: 4-6wt%,
Hamamelis virginiana extract: 3-5wt%,
Potassium hydroxide: 0.05-0.07wt%,
1,2-hexanediol/caprylyl glycol: 0.4-0.6wt%,
Above-mentioned Herba Saussuseae Japonicae extracting solution: surplus.
A kind of Herba Saussuseae Japonicae extracting solution of the present invention and its preparation method and application has the following advantages and beneficial effect:
The present invention is through a large amount of experiment of inventor and research; draw the Herba Saussuseae Japonicae extracting solution making through water extraction, be applied in cosmetics, make obtained cosmetics there is good anti-sensitization; protect the effect of keratodermatitis moisture simultaneously, there is significant reparation and protect sensitive-skinned effect.
Detailed description of the invention
Herba Saussuseae Japonicae of the present invention is the herb of feverfew hieracioides, is distributed widely in all parts of the country.Herba Saussuseae Japonicae sweet in the mouth is cool in nature, has clearing away heat and expelling pathogen in the exterior, removing pathogenic heat from blood and toxic substance from the body effect." decoction pieces is newly joined ": promoting blood circulation by removing wind, loose numb pain relieving.The present invention makes Herba Saussuseae Japonicae extracting solution by Herba Saussuseae Japonicae through water extraction, uses it for preparation and has in reparation and protection sensitive skin cosmetics.
Below with reference to specific embodiment, the present invention will be further described.
In following embodiment, described Hamamelis virginiana extract is purchased from Xi'an Sen Ran biological engineering company limited, Aloe vulgaris leaf extract purchased from Tianfeng Biological Science & Technology Co., Ltd., Xi'an, Ovshinsky Sargassum extract purchased from Rui Ying bio tech ltd, Xi'an, and other raw material is commercially available prod.
In following examples, composition title used is international cosmetic raw material name (International Nomenclature Cosmetic Ingredient, INCI) title of defined, for example phenoxyethanol/Sensiva SC50, encircle five polydimethylsiloxane/cyclohexasiloxane, glyceryl stearate/PEG-100 stearate, diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate, cetearyl alcohol/cetearyl glucoside, caprylic/capric triglyceride, polyacrylamide/C13-14 isoparaffin/laureth-7, Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate, glycerol polymethacrylates/propylene glycol, 1, 2-hexanediol/caprylyl glycol.
Embodiment 1 toner/smoothing toner
Described in the present embodiment, in toner/smoothing toner, contain Herba Saussuseae Japonicae extracting solution, the preparation method of described Herba Saussuseae Japonicae extracting solution, comprise the following steps: 1 kilogram of Herba Saussuseae Japonicae is cleaned, dry, drying and crushing to 80 order, is placed in vacuum emulsifying pot, add the deionized water of 10 kilograms, in 90 DEG C of extraction 20min, filter, obtain Herba Saussuseae Japonicae extracting solution.
The component of described toner/smoothing toner and content are in table 1:
The component of table 1 toner/smoothing toner and content
| Composition | Percentage by weight (wt%) |
| Herba Saussuseae Japonicae extracting solution | Surplus |
| Glycerol | 5 |
| Butanediol | 4 |
| Carbomer | 0.1 |
| Allantoin | 0.15 |
| Hyaluronate sodium | 0.06 |
| Triethanolamine | 0.1 |
| Phenoxyethanol/Sensiva SC50 | 0.3 |
| Add up to | 100 |
Embodiment 2 health breasts
Described in the present embodiment, Herba Saussuseae Japonicae extracting solution is contained in health Ruzhong, and the preparation method of described Herba Saussuseae Japonicae extracting solution, comprises the following steps: 1 kilogram of Herba Saussuseae Japonicae is cleaned, dry, drying and crushing to 60 order, the gauze bag by it with sterilizing installs, and is tamping, be placed in vacuum emulsifying pot, add the deionized water of 8 kilograms, in 95 DEG C of lixiviate 30min, gauze bag is taken out, remaining solution, obtains Herba Saussuseae Japonicae extracting solution.
The component of described health breast and content are in table 2:
Component and the content of table 2 health breast
| Composition | Percentage by weight (wt%) |
| Herba Saussuseae Japonicae extracting solution | Surplus |
| Methyl glucose sesquistearate | 1.3 |
| PEG-20 methyl glucose sesquistearate | 0.9 |
| Isopropyl palmitate | 4 |
| Encircle five polydimethylsiloxane/cyclohexasiloxane | 5 |
| Glyceryl stearate/PEG-100 stearate | 0.7 |
| Cetearyl alcohol | 1.2 |
| Polydimethylsiloxane | 2 |
| Methyl hydroxybenzoate | 0.2 |
| Propyl hydroxybenzoate | 0.1 |
| Xanthan gum | 0.3 |
| Propylene glycol | 5 |
| Diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate | 0.2 |
| Add up to | 100 |
Embodiment 3 nourishing cream
Described in the present embodiment, in nourishing cream, contain Herba Saussuseae Japonicae extracting solution, the preparation method of described Herba Saussuseae Japonicae extracting solution, comprises the following steps: 1 kilogram of Herba Saussuseae Japonicae is cleaned, dry, drying and crushing to 100 order, the gauze bag by it with sterilizing installs, and is tamping, be placed in vacuum emulsifying pot, add the deionized water of 12 kilograms, in 100 DEG C of lixiviate 50min, gauze bag is taken out, remaining solution, obtains Herba Saussuseae Japonicae extracting solution.
The component of described nourishing cream and content are in table 3:
The component of table 3 nourishing cream and content
| Composition | Percentage by weight (wt%) |
| Herba Saussuseae Japonicae extracting solution | Surplus |
| Cetearyl alcohol/cetearyl glucoside | 2.5 |
| Cetearyl alcohol | 1.2 |
| Glyceryl stearate/PEG-100 stearate | 1.2 |
| Encircle five polydimethylsiloxane/cyclohexasiloxane | 2 |
| Polydimethylsiloxane | 2 |
| Caprylic/capric triglyceride | 3 |
| Tocopherol (vitamin E) | 0.5 |
| Propylene glycol | 5 |
| Glycerol | 5 |
| Xanthan gum | 0.1 |
| Hyaluronate sodium | 0.02 |
| Polyacrylamide/C13-14 isoparaffin/laureth-7 | 0.7 |
| Phenoxyethanol/Sensiva SC50 | 0.5 |
| Oligofructose | 0.1 |
| Add up to | 100 |
Embodiment 4 essences
Described in the present embodiment, in essence, contain Herba Saussuseae Japonicae extracting solution, the preparation method of described Herba Saussuseae Japonicae extracting solution, with reference to embodiment 1.
The component of described essence and content are in table 4:
The component of table 4 essence and content
| Composition | Percentage by weight (wt%) |
| Herba Saussuseae Japonicae extracting solution | Surplus |
| EDTA-disodium | 0.02 |
| Glycerol | 5 |
| Butanediol | 5 |
| Allantoin | 0.1 |
| Methyl hydroxybenzoate | 0.1 |
| Hamamelis virginiana extract | 2 |
| Glycyrrhizic acid dipotassium | 0.05 |
| Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate | 1 |
| Aloe vulgaris leaf extract | 2 |
| Phenoxyethanol/Sensiva SC50 | 0.5 |
| Add up to | 100 |
Embodiment 5 masks
Described in the present embodiment, in mask, contain Herba Saussuseae Japonicae extracting solution, the preparation method of described Herba Saussuseae Japonicae extracting solution, with reference to embodiment 2.
The component of described mask and content are in table 5:
The component of table 5 mask and content
| Composition | Percentage by weight (wt%) |
| Herba Saussuseae Japonicae extracting solution | Surplus |
| Glycerol | 5 |
| Butanediol | 5 |
| Propylene glycol | 3 |
| Hydroxyethyl-cellulose | 0.05 |
| Hyaluronate sodium | 0.03 |
| Carbomer | 0.15 |
| Allantoin | 0.15 |
| Beta glucan | 1 |
| Glycerol polymethacrylates/propylene glycol | 8 |
| Ovshinsky Sargassum extract | 5 |
| Hamamelis virginiana extract | 4 |
| Potassium hydroxide | 0.06 |
| Deionized water | 1 |
| 1,2-hexanediol/caprylyl glycol | 0.5 |
| Add up to | 100 |
Comparative example 1 toner/smoothing toner
The component of described toner/smoothing toner and content are in table 6:
The component of table 6 toner/smoothing toner and content
| Composition | Percentage by weight (wt%) |
| Deionized water | Surplus |
| Glycerol | 5 |
| Butanediol | 4 |
| Carbomer | 0.1 |
| Allantoin | 0.15 |
| Hyaluronate sodium | 0.06 |
| Triethanolamine | 0.1 |
| Phenoxyethanol/Sensiva SC50 | 0.3 |
| Add up to | 100 |
Comparative example 2 health breasts
The component of described health breast and content are in table 7:
Component and the content of table 7 health breast
| Composition | Percentage by weight (wt%) |
| Deionized water | Surplus |
| Methyl glucose sesquistearate | 1.3 |
| PEG-20 methyl glucose sesquistearate | 0.9 |
| Isopropyl palmitate | 4 |
| Encircle five polydimethylsiloxane/cyclohexasiloxane | 5 |
| Glyceryl stearate/PEG-100 stearate | 0.7 |
| Cetearyl alcohol | 1.2 |
| Polydimethylsiloxane | 2 |
| Methyl hydroxybenzoate | 0.2 |
| Propyl hydroxybenzoate | 0.1 |
| Xanthan gum | 0.3 |
| Propylene glycol | 5 |
| Diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate | 0.2 |
| Add up to | 100 |
Comparative example 3 nourishing cream
The component of described nourishing cream and content are in table 8:
The component of table 8 nourishing cream and content
| Composition | Percentage by weight (wt%) |
| Deionized water | Surplus |
| Cetearyl alcohol/cetearyl glucoside | 2.5 |
| Cetearyl alcohol | 1.2 |
| Glyceryl stearate/PEG-100 stearate | 1.2 |
| Encircle five polydimethylsiloxane/cyclohexasiloxane | 2 |
| Polydimethylsiloxane | 2 |
| Caprylic/capric triglyceride | 3 |
| Tocopherol (vitamin E) | 0.5 |
| Propylene glycol | 5 |
| Glycerol | 5 |
| Xanthan gum | 0.1 |
| Hyaluronate sodium | 0.02 |
| Polyacrylamide/C13-14 isoparaffin/laureth-7 | 0.7 |
| Phenoxyethanol/Sensiva SC50 | 0.5 |
| Oligofructose | 0.1 |
| Add up to | 100 |
Comparative example 4 essences
The component of described essence and content are in table 9:
The component of table 9 essence and content
| Composition | Percentage by weight (wt%) |
| Deionized water | Surplus |
| EDTA-disodium | 0.02 |
| Glycerol | 5 |
| Butanediol | 5 |
| Allantoin | 0.1 |
| Methyl hydroxybenzoate | 0.1 |
| Hamamelis virginiana extract | 2 |
| Glycyrrhizic acid dipotassium | 0.05 |
| Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate | 1 |
| Aloe vulgaris leaf extract | 2 |
| Phenoxyethanol/Sensiva SC50 | 0.5 |
| Add up to | 100 |
Comparative example 5 masks
The component of described mask and content are in table 10:
The component of table 10 mask and content
| Composition | Percentage by weight (wt%) |
| Deionized water | Surplus |
| Glycerol | 5 |
| Butanediol | 5 |
| Propylene glycol | 3 |
| Hydroxyethyl-cellulose | 0.05 |
| Hyaluronate sodium | 0.03 |
| Carbomer | 0.15 |
| Allantoin | 0.15 |
| Beta glucan | 1 |
| Glycerol polymethacrylates/propylene glycol | 8 |
| Ovshinsky Sargassum extract | 5 |
| Hamamelis virginiana extract | 4 |
| Potassium hydroxide | 0.06 |
| Deionized water | 1 |
| 1,2-hexanediol/caprylyl glycol | 0.5 |
| Add up to | 100 |
Embodiment 6 effect evaluations
One, experiment purpose
Evaluate the reparation of prepared cosmetics in the various embodiments described above and protect sensitive-skinned effect by relative analysis.
Two, experimental technique
This experiment is divided into experimental group and matched group, and wherein, experiment component is: embodiment 1-toner/smoothing toner, embodiment 2-health breast, embodiment 3-nourishing cream, embodiment 4-essence, embodiment 5-facial film; Matched group is comparative example 1-toner/smoothing toner, comparative example 2-health breast, comparative example 3-nourishing cream, comparative example 4-essence, comparative example 5-facial film, a certain commercially available essence of repairing and protecting responsive skin that has.
200 volunteers of collection sensitive skin tried out above-mentioned each product after 28 days, observed result.Wherein, women 120 people, male 80 people, maximum 30 years old age, minimal ages 15 years old, 22 years old mean age.
Described sensitive-skinned showing as: face redness, speckle, skin peeling, xerosis cutis, skin sore or skin oil and fat secretion.
Three, experimental result
The efficacy outcomes of table 11 experimental group and matched group
As known from Table 11: matched group product comparative example 1-toner/smoothing toner, comparative example 2-health breast, comparative example 3-nourishing cream, comparative example 4-essence, comparative example 5-facial film, a certain commercially available essence and experimental group product embodiments 1-toner/smoothing toner, embodiment 2-health breast, embodiment 3-nourishing cream, embodiment 4-essence, embodiment 5-facial film is red and swollen to face, speckle, skin peeling, xerosis cutis, skin sore or skin oil and fat secretion all have improvement in various degree, can find out from experimental data, experimental group product is red and swollen to face, speckle, skin peeling, xerosis cutis, the improvement degree of skin sore or skin oil and fat secretion is obviously than the height of contrast set product, this shows, the cosmetics that contain Herba Saussuseae Japonicae extracting solution have significant reparation and protect sensitive-skinned effect.
The above embodiment has only expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but can not therefore be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (10)
1. a preparation method for Herba Saussuseae Japonicae extracting solution, is characterized in that, comprises the following steps:
Herba Saussuseae Japonicae be dry, pulverize, install with 800 order gauze bags of sterilizing, be placed in vacuum emulsifying pot, by the weight of Herba Saussuseae Japonicae, the deionized water that adds 8-12 doubly to measure, in 90-100 DEG C of extraction.
2. the Herba Saussuseae Japonicae extracting solution that preparation method as claimed in claim 1 makes.
3. Herba Saussuseae Japonicae extracting solution as prepared in claim 2 has the application in the cosmetics of repairing and protecting sensitive skin effect in preparation.
4. application according to claim 3, is characterized in that, in described cosmetics, the content of Herba Saussuseae Japonicae extracting solution is 58-95wt%.
5. the application of stating according to claim 3 or 4, is characterized in that, described cosmetics are toner/smoothing toner, health breast, nourishing cream, essence or facial film.
6. a toner/smoothing toner, is characterized in that, described toner/smoothing toner comprises the component of following weight percentage ratio:
Wetting agent: 5-13wt%,
Thickening agent: 0.05-0.15wt%,
Antiinflammatory: 0.1-0.2wt%,
Nertralizer: 0.05-0.15wt%,
Antiseptic: 0.2-0.7wt%,
Herba Saussuseae Japonicae extracting solution as claimed in claim 2: surplus;
Described wetting agent is at least one in glycerol, butanediol, propylene glycol or hyaluronate sodium;
Described thickening agent is at least one in carbomer, xanthan gum or hydroxyethyl-cellulose;
Described antiinflammatory is at least one in allantoin, Flos Inulae extract or bisabolol;
Described nertralizer is at least one in triethanolamine, sodium hydroxide or potassium hydroxide;
Described antiseptic is at least one in phenoxyethanol/Sensiva SC50, DMDM beta-lactam or Kazon.
7. a health breast, is characterized in that, described health breast comprises the component of following weight percentage ratio:
Emulsifying agent: 1.5-5wt%,
Co-emulsifier: 0.8-2wt%,
Emollient: 2-8wt%,
Skinfeel regulator: 1.5-10wt%,
Thickening agent: 0.1-0.4wt%,
Wetting agent: 4-10wt%,
Antiseptic: 0.05-0.7wt%,
Herba Saussuseae Japonicae extracting solution as claimed in claim 2: surplus;
Described emulsifying agent is at least one in methyl glucose sesquistearate, PEG-20 methyl glucose sesquistearate or glyceryl stearate/PEG-100 stearate;
Described co-emulsifier is at least one in cetearyl alcohol, glyceryl stearate or triethanolamine;
Described emollient is at least one in isopropyl palmitate, caprylic/capric triglyceride or hydrogenated jojoba oil;
Described skinfeel regulator is at least one in ring five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane or vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer;
Described thickening agent is at least one in xanthan gum, hydroxyethyl-cellulose or carbomer;
Described wetting agent is at least one in propylene glycol, glycerol or butanediol;
Described antiseptic is at least one in diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate, propyl hydroxybenzoate or methyl hydroxybenzoate.
8. a nourishing cream, is characterized in that, described nourishing cream comprises the component of following weight percentage ratio:
Emulsifying agent: 3.5-6.3wt%,
Emollient: 5-10wt%,
Antioxidant: 0.2-0.8wt%,
Wetting agent: 5-15wt%,
Thickening agent: 0.05-0.15wt%,
Antiseptic: 0.3-0.7wt%,
Herba Saussuseae Japonicae extracting solution as claimed in claim 2: surplus;
Described emulsifying agent is at least one in cetearyl alcohol/cetearyl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearate, polyacrylamide/C13-14 isoparaffin/laureth-7 or methyl glucose sesquistearate;
Described emollient is at least one in ring five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane, caprylic/capric triglyceride or hydrogenated jojoba oil;
Described antioxidant is at least one that tocopherol or fan change in extract;
Described wetting agent is at least one in propylene glycol, glycerol, hyaluronate sodium, oligofructose or sorbitol;
Described thickening agent is at least one in xanthan gum or sodium carboxymethyl cellulose;
Described antiseptic is at least one in phenoxyethanol/Sensiva SC50, sodium benzoate or germall.
9. an essence, is characterized in that, described essence comprises the component of following weight percentage ratio:
Chelating agen: 0.01-0.1wt%,
Wetting agent: 5-18wt%,
Antiinflammatory: 0.05-2.5wt%,
Antiseptic: 0.3-0.66wt%,
Herba Saussuseae Japonicae extract as claimed in claim 2: surplus;
Described chelating agen is at least one in EDTA-disodium or Etidronic Acid;
Described wetting agent is at least one in glycerol, propylene glycol, Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate, Aloe vulgaris leaf extract or PEG400;
Described antiinflammatory is at least one in allantoin, Hamamelis virginiana extract, glycyrrhizic acid dipotassium or Flos Inulae extract;
Described antiseptic is at least one in methyl hydroxybenzoate, phenoxyethanol/Sensiva SC50 or Kazon.
10. a mask, is characterized in that, described mask comprises the component of following weight percentage ratio:
Wetting agent: 5-35wt%,
Thickening agent: 0.05-0.3wt%,
Antiinflammatory: 2.5-5.5wt%,
PH adjusting agent: 0.04-0.08wt%,
Antiseptic: 0.2-0.6wt%,
Herba Saussuseae Japonicae extract as claimed in claim 2: surplus;
Described wetting agent is at least one in glycerol, butanediol, propylene glycol, hyaluronate sodium, glycerol polymethacrylates/propylene glycol, Ovshinsky Sargassum extract, beta glucan or oligofructose;
Described thickening agent is at least one in hydroxyethyl-cellulose, carbomer or xanthan gum;
Described antiinflammatory is at least one in allantoin, Hamamelis virginiana extract or bisabolol;
Described pH adjusting agent is at least one in triethanolamine, potassium hydroxide or sodium hydroxide;
Described antiseptic is at least one in 1,2-hexanediol/caprylyl glycol or phenoxyethanol/Sensiva SC50.
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| CN104382837A (en) * | 2014-12-05 | 2015-03-04 | 燕之初颜如燕（厦门）生物科技有限公司 | Mask of unadulterated edible bird's nest powder and use method thereof |
| CN105748351A (en) * | 2016-03-04 | 2016-07-13 | 佛山市聚成生化技术研发有限公司 | Plant composition and application thereof |
| CN106038354A (en) * | 2016-07-11 | 2016-10-26 | 广州丹奇日用化工厂有限公司 | Emulsion containing Heitacai polysaccharide |
| CN106726988A (en) * | 2016-12-28 | 2017-05-31 | 广州市聚吉科绿色化学共性技术研究院有限公司 | A kind of beauty face-whitening-nourishing frost and preparation method thereof |
| CN107137263A (en) * | 2017-04-19 | 2017-09-08 | 北京赛尔佳人化妆品有限公司 | A kind of anti-ageing face mask liquid and preparation method thereof |
| CN109010177A (en) * | 2018-09-15 | 2018-12-18 | 梅淑婕 | A kind of preparation method of skin care compositions and facial mask with moistening effect |
| CN109260032A (en) * | 2018-09-18 | 2019-01-25 | 广州达人研选生物科技有限公司 | A kind of combined type easily tears mud film and its application method |
| CN109481322A (en) * | 2018-10-10 | 2019-03-19 | 广州雷诺生物科技有限公司 | A kind of fullerene essence cream |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104382837A (en) * | 2014-12-05 | 2015-03-04 | 燕之初颜如燕（厦门）生物科技有限公司 | Mask of unadulterated edible bird's nest powder and use method thereof |
| CN105748351A (en) * | 2016-03-04 | 2016-07-13 | 佛山市聚成生化技术研发有限公司 | Plant composition and application thereof |
| CN106038354A (en) * | 2016-07-11 | 2016-10-26 | 广州丹奇日用化工厂有限公司 | Emulsion containing Heitacai polysaccharide |
| CN106726988A (en) * | 2016-12-28 | 2017-05-31 | 广州市聚吉科绿色化学共性技术研究院有限公司 | A kind of beauty face-whitening-nourishing frost and preparation method thereof |
| CN107137263A (en) * | 2017-04-19 | 2017-09-08 | 北京赛尔佳人化妆品有限公司 | A kind of anti-ageing face mask liquid and preparation method thereof |
| CN109010177A (en) * | 2018-09-15 | 2018-12-18 | 梅淑婕 | A kind of preparation method of skin care compositions and facial mask with moistening effect |
| CN109260032A (en) * | 2018-09-18 | 2019-01-25 | 广州达人研选生物科技有限公司 | A kind of combined type easily tears mud film and its application method |
| CN109481322A (en) * | 2018-10-10 | 2019-03-19 | 广州雷诺生物科技有限公司 | A kind of fullerene essence cream |
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|---|---|
| CN103976923B (en) | 2016-07-06 |
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Effective date of registration: 20170322 Address after: 510800 Guangdong city in Guangzhou Province, Xinhua Street, Huadu District, Xinhua Industrial Zone Yongxiang road building 32-2 (plant to use) Patentee after: Guangzhou zuoduozi Cosmetics Co. Ltd. Address before: Two road 510545 in Guangdong Province, Baiyun District of Guangzhou City Land Development Zone Park No. 3 Patentee before: Guangzhou Qian Baidu cosmetics company limited |