CN103446026B - Angelica moisture-preserving water and preparation method thereof - Google Patents
Angelica moisture-preserving water and preparation method thereof Download PDFInfo
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- CN103446026B CN103446026B CN201310408654.3A CN201310408654A CN103446026B CN 103446026 B CN103446026 B CN 103446026B CN 201310408654 A CN201310408654 A CN 201310408654A CN 103446026 B CN103446026 B CN 103446026B
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Abstract
The invention relates to angelica moisture-preserving water. The angelica moisture-preserving water is prepared from the following components according to weight percent: 1%-5% of angelica extracts, 1%-5% of sodium pyrrolidone carboxylate, 0.05%-1% of hyaluronic acid, 1%-5% of glycerin, 1%-5% of propylene glycol, 0.05%-0.5% of lubrajel oil, 0.01%-1% of a preservative, 0.1%-5% of a solubilizer, 0-0.5% of essence and the balance being purified water. Meanwhile, the invention further discloses a preparation method of the angelica moisture-preserving water. The angelica moisture-preserving water has dual functions of nutrition and pharmacology, not only can preserve and supplement moisture required by skins, but also can rejuvenate and whiten skins, cannot stimulate skins and has multiple functions of improving skin conditions, maintaining beauty and keeping young after being used for a long time.
Description
Technical field
The present invention relates to cosmetics and production technology field thereof, particularly relate to a kind of Radix Angelicae Sinensis moisture retention water and preparation method thereof.
Background technology
Along with the raising of people's living standard, the market sustainable growth of cosmetics.The article of everyday use of skin protection based on astringent, has clean skin, supplements the effects such as cuticular moisture, regulation of skin acid-base value, Firm, convergence pore.Under the trend advocating back to nature now, Chinese herbal medicine class cosmetics are increasing in the market, the cry of back to nature is increasing, natural cosmetics is very be in great demand, such as the cosmetics that the medium-height grass the effective elements of the medicines such as Aloe, Radix Rhodiolae, Herba Leonuri, Flos Chrysanthemi add as nutritional labeling are commercially very popular.Radix Angelicae Sinensis is as Gansu genuine medicinal materials quality better, and resource is abundant, is just used in beauty and skin care product since ancient times.Physician to Tang Dynasty in China Sun Simiao work supplement to Thousand Golden Prescriptions in anti-ageing speckle removing, skin health-care " married woman face medicine " carried out scientific validation, therefrom filter out the highest medicine of frequency of utilization.Result shows, the function of the aqueous solution restraint of tyrosinase activity of Radix Angelicae Sinensis is very strong, the formation of energy check melanin, produces effects well, have defying age and beautification function to pigmented dermatosis such as treatment chloasma, freckle etc., contributes to people's youth is resided.Documents and materials show, effective ingredient main in Radix Angelicae Sinensis aqueous solution is ferulic acid, and medically, ferulic acid has extensive use, almost non-toxic property.Recent studies shows, ferulic acid is natural safe free radical quencher, antioxidant, skin-whitening agents and cell differentiation promoter, attention in whitening, antidotal research.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of pure natural and has the Radix Angelicae Sinensis moisture retention water of skin-active, moisturizing, moistening effect.
Another technical problem to be solved by this invention is to provide the preparation method of a kind of technique Radix Angelicae Sinensis moisture retention water simple, with low cost.
For solving the problem, a kind of Radix Angelicae Sinensis moisture retention water of the present invention, is characterized in that: it is made up of the component of following weight percentage ratio: Radix Angelicae Sinensis extract 1% ~ 5%, pyrrolidone sodium carboxylate 1% ~ 5%, hyaluronic acid 0.05% ~ 1%, glycerol 1% ~ 5%, propylene glycol 1% ~ 5%, reed fragrant plant oil 0.05% ~ 0.5%, antiseptic 0.01% ~ 1%, solubilizing agent 0.1% ~ 5%, essence 0% ~ 0.5%, surplus are purified water.
Described Radix Angelicae Sinensis extract refers to first by after the remove impurity of fresh Radix Angelicae Sinensis medical material, chopping, then in Radix Angelicae Sinensis, add by its quality 6 ~ 12 times the ethanol that mass concentration is 60% ~ 90%, temperature be 30 ~ 90 DEG C, power be the condition of 200 ~ 500W under supersound extraction 1 ~ 3 time, each 1 ~ 2 hour, filter after merge extractive liquid, obtain filtrate, finally, by described filtrate through concentrating under reduced pressure, reclaim ethanol and get final product.
Described antiseptic refers to the one in imidazolidinyl urea, methyl parahydroxybenzoate, phenoxyethanol, germall-IS 45, DMDM Hydantoin, Bronopol.
Described solubilizing agent is the one in Tween 80, castor oil hydrogenated co-40, anhydrous sorbitol tristerin, polysorbate.
Described essence is the one of the conventional essence used in skin care item.
Described hyaluronic mass concentration is 1%.
The preparation method of a kind of Radix Angelicae Sinensis moisture retention water as above, comprises the following steps:
(1) weigh by proportioning;
(2), by after pyrrolidone sodium carboxylate, hyaluronic acid, reed fragrant plant oil, glycerol and purified water mixing, at 80 ~ 100 DEG C of temperature, heated and stirred makes it fully melt, and mixed dissolution becomes solution A phase;
(3) by after antiseptic, Radix Angelicae Sinensis extract, mixed with propylene glycol, at 80 ~ 100 DEG C of temperature, heated and stirred makes it fully melt, and mixed dissolution becomes solution B phase;
(4) add essence after solubilizing agent being heated to 30 ~ 60 DEG C, be fully uniformly mixed, be dissolved into solution C phase;
(5) add described solution C phase when described solution B being cooled to 45 DEG C mutually, fully mixing, to stir, then joined be cooled to 45 DEG C described solution A mutually in, after being fully uniformly mixed, be cooled to room temperature, preferably sterilize tinning and get final product according to a conventional method.
The present invention compared with prior art has the following advantages:
1, the present invention adopts pure Chinese herbal medicine, not containing mineral, not containing heavy metal component, and no side effects.
2, the present invention adopts Chinese herbal medicine, and wherein Chinese herbal medicine has nutrition and pharmacology dual function concurrently, and effect relaxes lastingly, meets the long-acting requirement with adding natural component of cosmetics; Simultaneously Radix Angelicae Sinensis can effective blood circulation promoting, desalination mottle, nutrition skin, increase skin elasticity, and has radiation-resisting functional.
3, the present invention has moisturizing, supplements moisture needed for skin, and Cucumber Extract, whitening, not chafe, have and improve the effect such as skin, looks improving and the skin nourishing.
4, moderate cost of the present invention, is applicable to all kinds skin and uses.
5, the inventive method is simple, easy to implement.
Detailed description of the invention
embodiment 1a kind of Radix Angelicae Sinensis moisture retention water, it is made up of the component of following weight percentage ratio (g/g): Radix Angelicae Sinensis extract 5%, pyrrolidone sodium carboxylate 5%, hyaluronic acid 0.05%, glycerol 3%, propylene glycol 5%, reed fragrant plant oil 0.4%, antiseptic 0.01%, solubilizing agent 5%, essence 0.5%, surplus are purified water.
Wherein: Radix Angelicae Sinensis extract refers to first by after the remove impurity of fresh Radix Angelicae Sinensis medical material, chopping, then in Radix Angelicae Sinensis, add by its quality 6 times the ethanol that mass concentration is 60%, temperature be 80 DEG C, power be the condition of 200W under supersound extraction 3 times, each 2 hours, filter after merge extractive liquid, obtain filtrate, finally, by filtrate through 50 DEG C of concentrating under reduced pressure, reclaim ethanol and get final product.
Antiseptic refers to imidazolidinyl urea.Solubilizing agent is Tween 80.Essence is the one of the conventional essence used in skin care item.Hyaluronic mass concentration is 1%.
The preparation method of this Radix Angelicae Sinensis moisture retention water, comprises the following steps:
(1) weigh by proportioning;
(2), by after pyrrolidone sodium carboxylate, hyaluronic acid, reed fragrant plant oil, glycerol and purified water mixing, at 80 ~ 100 DEG C of temperature, heated and stirred makes it fully melt, and mixed dissolution becomes solution A phase;
(3) by after antiseptic, Radix Angelicae Sinensis extract, mixed with propylene glycol, at 80 ~ 100 DEG C of temperature, heated and stirred makes it fully melt, and mixed dissolution becomes solution B phase;
(4) add essence after solubilizing agent being heated to 30 ~ 60 DEG C, be fully uniformly mixed, be dissolved into solution C phase;
(5) add solution C phase when solution B being cooled to mutually 45 DEG C, fully mixing, to stir, then joined be cooled to 45 DEG C solution A mutually in, after being fully uniformly mixed, be cooled to room temperature, preferably sterilize tinning and get final product according to a conventional method.
embodiment 2a kind of Radix Angelicae Sinensis moisture retention water, it is made up of the component of following weight percentage ratio (g/g): Radix Angelicae Sinensis extract 1%, pyrrolidone sodium carboxylate 3%, hyaluronic acid 0.1%, glycerol 1%, propylene glycol 3%, reed fragrant plant oil 0.5%, antiseptic 0.1%, solubilizing agent 1%, essence 0%, surplus are purified water.
Wherein: Radix Angelicae Sinensis extract refers to first by after the remove impurity of fresh Radix Angelicae Sinensis medical material, chopping, then in Radix Angelicae Sinensis, add by its quality 12 times the ethanol that mass concentration is 70%, temperature be 40 DEG C, power be the condition of 500W under supersound extraction 1 time, each 1.5 hours, filter after merge extractive liquid, obtain filtrate, finally, by filtrate through 45 DEG C of concentrating under reduced pressure, reclaim ethanol and get final product.
Antiseptic refers to methyl parahydroxybenzoate.Solubilizing agent is castor oil hydrogenated co-40.Essence is the one of the conventional essence used in skin care item.Hyaluronic mass concentration is 1%.
The preparation method of this Radix Angelicae Sinensis moisture retention water is same
embodiment 1.
embodiment 3a kind of Radix Angelicae Sinensis moisture retention water, it is made up of the component of following weight percentage ratio (g/g): Radix Angelicae Sinensis extract 5%, pyrrolidone sodium carboxylate 4%, hyaluronic acid 0.2%, glycerol 2%, propylene glycol 5%, reed fragrant plant oil 0.3%, antiseptic 0.4%, solubilizing agent 4%, essence 0.4%, surplus are purified water.
Wherein: Radix Angelicae Sinensis extract refers to first by after the remove impurity of fresh Radix Angelicae Sinensis medical material, chopping, then in Radix Angelicae Sinensis, add by its quality 7 times the ethanol that mass concentration is 70%, temperature be 50 DEG C, power be the condition of 200W under supersound extraction 2 times, each 2 hours, filter after merge extractive liquid, obtain filtrate, finally, by filtrate through 45 DEG C of concentrating under reduced pressure, reclaim ethanol and get final product.
Antiseptic refers to phenoxyethanol.Solubilizing agent is anhydrous sorbitol tristerin.Essence is the one of the conventional essence used in skin care item.Hyaluronic mass concentration is 1%.
The preparation method of this Radix Angelicae Sinensis moisture retention water is same
embodiment 1.
embodiment 4a kind of Radix Angelicae Sinensis moisture retention water, it is made up of the component of following weight percentage ratio (g/g): Radix Angelicae Sinensis extract 4%, pyrrolidone sodium carboxylate 2%, hyaluronic acid 0.4%, glycerol 4%, propylene glycol 2%, reed fragrant plant oil 0.1%, antiseptic 0.2%, solubilizing agent 2%, essence 0.3%, surplus are purified water.
Wherein: Radix Angelicae Sinensis extract refers to first by after the remove impurity of fresh Radix Angelicae Sinensis medical material, chopping, then in Radix Angelicae Sinensis, add by its quality 10 times the ethanol that mass concentration is 80%, temperature be 60 DEG C, power be the condition of 400W under supersound extraction 1 time, each 1 hour, filter after merge extractive liquid, obtain filtrate, finally, by filtrate through 40 DEG C of concentrating under reduced pressure, reclaim ethanol and get final product.
Antiseptic refers to Bronopol.Solubilizing agent is anhydrous sorbitol tristerin.Essence is the one of the conventional essence used in skin care item.Hyaluronic mass concentration is 1%.
The preparation method of this Radix Angelicae Sinensis moisture retention water is same
embodiment 1.
embodiment 5a kind of Radix Angelicae Sinensis moisture retention water, it is made up of the component of following weight percentage ratio (g/g): Radix Angelicae Sinensis extract 3%, pyrrolidone sodium carboxylate 1%, hyaluronic acid 0.6%, glycerol 5%, propylene glycol 1%, reed fragrant plant oil 0.2%, antiseptic 1%, solubilizing agent 3%, essence 0.2%, surplus are purified water.
Wherein: Radix Angelicae Sinensis extract refers to first by after the remove impurity of fresh Radix Angelicae Sinensis medical material, chopping, then in Radix Angelicae Sinensis, add by its quality 12 times the ethanol that mass concentration is 90%, temperature be 30 DEG C, power be the condition of 500W under supersound extraction 1 time, each 1.5 hours, filter after merge extractive liquid, obtain filtrate, finally, by filtrate through 40 DEG C of concentrating under reduced pressure, reclaim ethanol and get final product.
Antiseptic refers to germall-IS 45.Solubilizing agent is polysorbate.Essence is the one of the conventional essence used in skin care item.Hyaluronic mass concentration is 1%.
The preparation method of this Radix Angelicae Sinensis moisture retention water is same
embodiment 1.
embodiment 6a kind of Radix Angelicae Sinensis moisture retention water, it is made up of the component of following weight percentage ratio (g/g): Radix Angelicae Sinensis extract 1%, pyrrolidone sodium carboxylate 1%, hyaluronic acid 1%, glycerol 1%, propylene glycol 5%, reed fragrant plant oil 0.05%, antiseptic 0.8%, solubilizing agent 0.1%, essence 0.05%, surplus are purified water.
Wherein: Radix Angelicae Sinensis extract refers to first by after the remove impurity of fresh Radix Angelicae Sinensis medical material, chopping, then in Radix Angelicae Sinensis, add by its quality 10 times the ethanol that mass concentration is 80%, temperature be 70 DEG C, power be the condition of 300W under supersound extraction 2 times, each 2 hours, filter after merge extractive liquid, obtain filtrate, finally, by filtrate through 45 DEG C of concentrating under reduced pressure, reclaim ethanol and get final product.
Antiseptic refers to methyl parahydroxybenzoate, germall-IS45.Solubilizing agent is castor oil hydrogenated co-40.Essence is the one of the conventional essence used in skin care item.Hyaluronic mass concentration is 1%.
The preparation method of this Radix Angelicae Sinensis moisture retention water is same
embodiment 1.
embodiment 7a kind of Radix Angelicae Sinensis moisture retention water, it is made up of the component of following weight percentage ratio (g/g): Radix Angelicae Sinensis extract 2%, pyrrolidone sodium carboxylate 3%, hyaluronic acid 1%, glycerol 2%, propylene glycol 4%, reed fragrant plant oil 0.3%, antiseptic 0.6%, solubilizing agent 5%, essence 0.1%, surplus are purified water.
Wherein: Radix Angelicae Sinensis extract refers to first by after the remove impurity of fresh Radix Angelicae Sinensis medical material, chopping, then in Radix Angelicae Sinensis, add by its quality 8 times the ethanol that mass concentration is 70%, temperature be 90 DEG C, power be the condition of 500W under supersound extraction 3 times, each 1.5 hours, filter after merge extractive liquid, obtain filtrate, finally, by filtrate through 50 DEG C of concentrating under reduced pressure, reclaim ethanol and get final product.
Antiseptic refers to DMDM Hydantoin.Solubilizing agent is Tween 80.Essence is the one of the conventional essence used in skin care item.Hyaluronic mass concentration is 1%.
The preparation method of this Radix Angelicae Sinensis moisture retention water is same
embodiment 1.
Claims (2)
1. a Radix Angelicae Sinensis moisture retention water, is characterized in that: it is made up of the component of following weight percentage ratio: Radix Angelicae Sinensis extract 1% ~ 5%, pyrrolidone sodium carboxylate 1% ~ 5%, hyaluronic acid 0.05% ~ 1%, glycerol 1% ~ 5%, propylene glycol 1% ~ 5%, reed fragrant plant oil 0.05% ~ 0.5%, antiseptic, solubilizing agent 0.1% ~ 5%, essence 0% ~ 0.5%, surplus are purified water; When described antiseptic is imidazolidinyl urea, add 0.01%; When described antiseptic is methyl parahydroxybenzoate, add 0.1%; When described antiseptic is phenoxyethanol, add 0.4%; When described antiseptic is germall-IS 45, add 1%; When described antiseptic is DMDM Hydantoin, add 0.6%; Described Radix Angelicae Sinensis extract refers to first by after the remove impurity of fresh Radix Angelicae Sinensis medical material, chopping, then in Radix Angelicae Sinensis, add by its quality 6 ~ 12 times the ethanol that mass concentration is 60% ~ 90%, temperature be 30 ~ 90 DEG C, power be the condition of 200 ~ 500W under supersound extraction 1 ~ 3 time, each 1 ~ 2 hour, filter after merge extractive liquid, obtain filtrate, finally, by described filtrate through concentrating under reduced pressure, reclaim ethanol and get final product; Described solubilizing agent is the one in Tween 80, castor oil hydrogenated co-40, anhydrous sorbitol tristerin, polysorbate; Described essence is the one of the conventional essence used in skin care item; Described hyaluronic mass concentration is 1%.
2. the preparation method of a kind of Radix Angelicae Sinensis moisture retention water as claimed in claim 1, comprises the following steps:
(1) weigh by proportioning;
(2), by after pyrrolidone sodium carboxylate, hyaluronic acid, reed fragrant plant oil, glycerol and purified water mixing, at 80 ~ 100 DEG C of temperature, heated and stirred makes it fully melt, and mixed dissolution becomes solution A phase;
(3) by after antiseptic, Radix Angelicae Sinensis extract, mixed with propylene glycol, at 80 ~ 100 DEG C of temperature, heated and stirred makes it fully melt, and mixed dissolution becomes solution B phase;
(4) add essence after solubilizing agent being heated to 30 ~ 60 DEG C, be fully uniformly mixed, be dissolved into solution C phase;
(5) add described solution C phase when described solution B being cooled to 45 DEG C mutually, fully mixing, to stir, then joined be cooled to 45 DEG C described solution A mutually in, after being fully uniformly mixed, be cooled to room temperature, sterilize tinning and get final product according to a conventional method.
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| CN105796443A (en) * | 2016-05-18 | 2016-07-27 | 广州丹奇日用化工厂有限公司 | Antioxidant moisturizing lotion containing artemisia selengensis extract and preparation method of antioxidant moisturizing lotion |
| CN107951756A (en) * | 2017-12-26 | 2018-04-24 | 广州莱蔓诗生物科技有限公司 | Full-effect whitening, moisturizing, wrinkle-removing, freckle-removing and acne-removing essence and preparation method thereof |
| CN108324609A (en) * | 2018-03-13 | 2018-07-27 | 云南爱尔康生物技术有限公司 | A kind of moisture retention water of astaxanthin-containing and preparation method thereof |
| CN109453056A (en) * | 2018-11-12 | 2019-03-12 | 宁波蒙曼生物科技有限公司 | A kind of moisture saver mask liquid and preparation method thereof |
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