CN103961294A - Rehmannia extracting solution as well as preparation method and application thereof - Google Patents
Rehmannia extracting solution as well as preparation method and application thereof Download PDFInfo
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- CN103961294A CN103961294A CN201410242257.8A CN201410242257A CN103961294A CN 103961294 A CN103961294 A CN 103961294A CN 201410242257 A CN201410242257 A CN 201410242257A CN 103961294 A CN103961294 A CN 103961294A
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Abstract
The invention discloses a rehmannia extracting solution as well as a preparation method and an application thereof. The rehmannia extracting solution prepared by water extraction through lots of experiments and research by the inventor has remarkable effects of resisting inflammation, eliminating swelling, promoting metabolism of skin cells and resisting ageing, due to the characteristics, the rehmannia extracting solution has the effects of repairing damaged cells and improving skin immunity, and when the rehmannia extracting solution is applied to cosmetics, the rehmannia extracting solution has remarkable effects of repairing and protecting sensitive skin.
Description
Technical field
The present invention relates to cosmetic field, particularly relate to a kind of Radix Rehmanniae extracting solution and its preparation method and application.
Background technology
Along with the raising of people's living standard, cosmetics have become necessary article in people's life.But people are but very high for the prescription of cosmetics, not only require effectively, and require to be free from side effects.Along with the development of cosmetics industry, natural plants series products due to use safety, action temperature and, the advantage such as successful welcome.Be generally to obtain by corresponding processing the plant extract that contains effective ingredient, and add in cosmetics.
At present the plant extract in cosmetics, mostly adopts the methods such as water extraction, alcohol extraction, ultrasonic extraction, microwave extraction to extract gained, and extraction process is complicated, through operations such as concentrate dryings, also to add antiseptic so that the shelf-life of extract more permanent.The drawback of bringing like this, one is waste resource, and in leaching process, solution is concentrated, generally only gets concentrated fraction elite out, and most solutions is thrown away.This part solution still can contain active component in fact, can also again utilize.Directly throw away the waste that has just caused resource.Another drawback is add antiseptic no doubt can make extract obtain the longer shelf-life, but the while to be also for skin brings sensitization source.
Sensitive skin is that current cosmetics circle personage wants a difficult problem of capturing.Cause the basic reason of responsive skin to be: Skin Cell is impaired and make the immunity degradation of skin, and stratum corneum gets thinner causes skin moisturizing degree inadequate, finally causes the barrier function of skin too weak, cannot resist environmental stimuli.Then the nerve fiber of skin is owing to being often subject to environmental stimuli, too excited, thus be easy to produce general red, heating, pruritus, twinge, the generation of the uncomfortable phenomenon such as erythema.
How simple, safety, effectively extract plant, select which kind of plant, and by being applied in cosmetics of its safety, protection sensitive skin, is problem demanding prompt solution.
Summary of the invention
Based on this, the object of the invention is to provide a kind of Radix Rehmanniae extracting solution and its preparation method and application.
The concrete technical scheme solving the problems of the technologies described above is as follows:
A preparation method for Radix Rehmanniae extracting solution, comprises the following steps:
By Radix Rehmanniae drying and crushing, with the 800-1000 order gauze bag of sterilizing, install, be placed in vacuum emulsifying pot, by the weight of Radix Rehmanniae, the deionized water that adds 8-12 doubly to measure, in 90-100 ℃ of extraction, can make Radix Rehmanniae extracting solution.
In some embodiment, the time of described extraction is 20-50min therein.
In some embodiment, by Radix Rehmanniae drying and crushing, with 800 order gauze bags of sterilizing, install therein, be placed in vacuum emulsifying pot, after having extracted, directly gauze bag is taken out, remaining solution is Radix Rehmanniae extracting solution.In the method, owing to adopting vacuum emulsifying pot, it can directly add other cosmetics adjuvants after extraction completes, and carries out Cosmetic Manufacture, and does not need to extract with special herbal extraction equipment, has saved cost; In addition, adopt the packed Radix Rehmanniae powder of gauze, extracted and directly gauze bag has been taken out afterwards, need not filter, simplification extraction process, raises the efficiency.
The Radix Rehmanniae extract that said method the makes use of can now withdrawing deposit, does not need to add antiseptic, and skin is reduced to sensitization source.In cosmetic formulations, itself is just added with antiseptic, and extract of the present invention is now carried and being added, and has avoided producing spoilage problems because of placement.
The prepared Radix Rehmanniae extracting solution of said method has the application in the cosmetics of repairing and protecting sensitive skin effect in preparation.
In some embodiment, in described cosmetics, the content of Radix Rehmanniae extracting solution is 58-95wt% therein.
In some embodiment, described cosmetics are health breast, nourishing cream therein.
The invention provides a kind of health breast, described health breast comprises the component of following weight percentage ratio:
Emulsifying agent: 1.5-5wt%,
Co-emulsifier: 0.8-2wt%,
Emollient: 2-8wt%,
Skinfeel regulator: 1.5-10wt%,
Thickening agent: 0.1-0.4wt%,
Wetting agent: 4-10wt%,
Antiseptic: 0.05-0.7wt%,
The Radix Rehmanniae extracting solution that above-mentioned preparation method makes: surplus;
Described emulsifying agent is at least one in methyl glucose sesquistearate, PEG-20 methyl glucose sesquistearate or glyceryl stearate/PEG-100 stearate;
Described co-emulsifier is at least one in cetearyl alcohol, glyceryl stearate or triethanolamine;
Described emollient is at least one in isopropyl palmitate, caprylic/capric triglyceride or hydrogenated jojoba oil;
Described skinfeel regulator is for encircling at least one in five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane or vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer;
Described thickening agent is at least one in xanthan gum, hydroxyethyl-cellulose or carbomer;
Described wetting agent is at least one in propylene glycol, glycerol or butanediol;
Described antiseptic is at least one in diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate, propyl hydroxybenzoate or methyl hydroxybenzoate.
In some embodiment, described health breast comprises the component of following weight percentage ratio therein:
Methyl glucose sesquistearate: 1.1-1.5wt%,
PEG-20 methyl glucose sesquistearate: 0.8-1.0wt%,
Isopropyl palmitate: 3-5wt%,
Encircle five polydimethylsiloxane/cyclohexasiloxane: 4-6wt%,
Glyceryl stearate/PEG-100 stearate: 0.6-0.8wt%,
Cetearyl alcohol: 1.1-1.3wt%,
Polydimethylsiloxane: 1.8-2.2wt%,
Methyl hydroxybenzoate: 0.15-0.25wt%,
Propyl hydroxybenzoate: 0.09-0.11wt%,
Xanthan gum: 0.25-0.35wt%,
Propylene glycol: 4-6wt%,
Diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate: 0.18-0.22wt%,
Above-mentioned Radix Rehmanniae extracting solution: surplus.
The present invention also provides a kind of nourishing cream, and described nourishing cream comprises the component of following weight percentage ratio:
Emulsifying agent: 3.5-6.3wt%,
Emollient: 5-10wt%,
Antioxidant: 0.2-0.8wt%,
Wetting agent: 5-15wt%,
Thickening agent: 0.05-0.15wt%,
Antiseptic: 0.3-0.7wt%,
The Radix Rehmanniae extracting solution that above-mentioned preparation method makes: surplus,
Described emulsifying agent is at least one in cetearyl alcohol/cetearyl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearate, polyacrylamide/C13-14 isoparaffin/laureth-7 or methyl glucose sesquistearate;
Described emollient is for encircling at least one in five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane, caprylic/capric triglyceride or hydrogenated jojoba oil;
Described antioxidant is at least one that tocopherol or fan change in extract;
Described wetting agent is at least one in propylene glycol, glycerol, hyaluronate sodium, oligofructose or sorbitol;
Described thickening agent is at least one in xanthan gum or sodium carboxymethyl cellulose;
Described antiseptic is at least one in phenoxyethanol/Sensiva SC50, sodium benzoate or germall.
In some embodiment, described nourishing cream comprises the component of following weight percentage ratio therein:
Cetearyl alcohol/cetearyl glucoside: 2.3-2.7wt%,
Cetearyl alcohol: 1-1.4wt%,
Glyceryl stearate/PEG-100 stearate 1-1.4wt%,
Encircle five polydimethylsiloxane/cyclohexasiloxane: 1.8-2.2wt%,
Polydimethylsiloxane: 1.8-2.2wt%,
Caprylic/capric triglyceride: 2.8-3.2wt%,
Tocopherol: 0.4-0.6wt%,
Propylene glycol: 4-6wt%,
Glycerol: 4-6wt%,
Xanthan gum: 0.09-0.11wt%,
Hyaluronate sodium: 0.015-0.025wt%,
Polyacrylamide/C13-14 isoparaffin/laureth-7:0.6-0.8wt%,
Phenoxyethanol/Sensiva SC50: 0.4-0.6wt%,
Oligofructose: 0.08-0.11wt%,
Above-mentioned Radix Rehmanniae extracting solution: surplus.
A kind of Radix Rehmanniae extracting solution of the present invention and its preparation method and application has the following advantages and beneficial effect:
The present invention is through a large amount of experiment of inventor and research; draw the Radix Rehmanniae extracting solution making through water extraction; it has significant anti-inflammation detumescence and promotes skin cell metabolism and antidotal effect; this specific character makes Radix Rehmanniae extracting solution possess reparation damaged cell; improve the effect of skin immunization power, be applied to have in cosmetics significant reparation and protect sensitive-skinned effect.
The specific embodiment
Radix Rehmanniae is the tuber of scrophulariaceae rehmannia glutinosa plant, begins to be loaded in Sheng Nong's herbal classic, classifies as top gradely, is one of conventional Chinese medicine.In Radix Rehmanniae, contain polysaccharide, oligosaccharide, the compositions such as Martynoside., iridoid, it has certain pharmacological action to aspects such as immunity, blood, cardiovascular and cerebrovascular vessel, endocrine, central nervous system.There are some researches show, the obviously atrophy of aging model mouse thymus and spleen due to antagonism D-galactose of bosom Dihuang polysaccharide, even make related immune index obviously raise as thymic cortex thickness and cell number, splenic nodule and lymphocyte number, so that surpass normal level, prompting bosom Dihuang polysaccharide may be the anti-ageing main active of bosom Radix Rehmanniae tonification, and the atrophy of its antagonism aging model mouse immune organ, to strengthen immune effect may be one of anti-ageing mechanism of its tonification.In clinical practice, can be used for treating the dermatosiss such as rheumatism, rheumatoid arthritis and treatment eczema, urticaria, neurodermatitis.The just > > of < < book on Chinese herbal medicine is broken stagnant blood one deck only, seem cold and cool viscous behavio(u)r, must be without the merit of removing blood stasis with potent drugs intestinal stasis relieving, right all tumbling down strike to be flutterred, muscle blood stasis, the livid purple person that swells, mashes thick applying with the fresh Radix Rehmanniae, the detumescence of self energy blood stasis removing, the analgesic therapy of invigorating blood circulation, know that Radix Rehmanniae blood stasis removing has natural action by oneself, can not its greasy stagnant material of misidentification, and then doubt ancients' speech.Only the Tang and Song Dynasty to be to fall, all sides of removing blood stasis, without second mining with and this person, lid is also disliked its thick greasy having a surplus, eventually non-assault fortified position break through enemy lines general.The present invention makes Radix Rehmanniae extracting solution by ground ecliptic longitude water extraction, uses it for preparation and has in reparation and protection sensitive skin cosmetics.
Below with reference to specific embodiment, the present invention will be further described.
In following examples, composition title used is international cosmetic raw material name (InternationalNomenclatureCosmeticIngredient, INCI) title of defined, for example phenoxyethanol/Sensiva SC50, ring five polydimethylsiloxane/cyclohexasiloxane, glyceryl stearate/PEG-100 stearate, diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate, cetearyl alcohol/cetearyl glucoside, caprylic/capric triglyceride, polyacrylamide/C13-14 isoparaffin/laureth-7.
Embodiment 1 health breast
Described in the present embodiment, Radix Rehmanniae extracting solution is contained in health Ruzhong, and the preparation method of described Radix Rehmanniae extracting solution, comprises the following steps: 1 kilogram of Radix Rehmanniae is cleaned, dry, drying and crushing to 60 order, installs with 1000 order gauze bags of sterilizing, is tamping, be placed in vacuum emulsifying pot, the deionized water that adds 8 kilograms, in 95 ℃ of lixiviate 30min, takes out gauze bag, remaining solution, obtains Radix Rehmanniae extracting solution.
The component of described health breast and content are in Table 1:
Component and the content of table 1 health breast
| Composition | Percentage by weight (wt%) |
| Radix Rehmanniae extracting solution | Surplus |
| Methyl glucose sesquistearate | 1.3 |
| PEG-20 methyl glucose sesquistearate | 0.9 |
| Isopropyl palmitate | 4 |
| Encircle five polydimethylsiloxane/cyclohexasiloxane | 5 |
| Glyceryl stearate/PEG-100 stearate | 0.7 |
| Cetearyl alcohol | 1.2 |
| Polydimethylsiloxane | 2 |
| Methyl hydroxybenzoate | 0.2 |
| Propyl hydroxybenzoate | 0.1 |
| Xanthan gum | 0.3 |
| Propylene glycol | 5 |
| Diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate | 0.2 |
| Add up to | 100 |
Embodiment 2 nourishing cream
Described in the present embodiment, in nourishing cream, contain Radix Rehmanniae extracting solution, the preparation method of described Radix Rehmanniae extracting solution, comprises the following steps: 1 kilogram of Radix Rehmanniae is cleaned, dry, drying and crushing to 100 order, installs with 1000 order gauze bags of sterilizing, is tamping, be placed in vacuum emulsifying pot, the deionized water that adds 12 kilograms, in 100 ℃ of lixiviate 50min, takes out gauze bag, remaining solution, obtains Radix Rehmanniae extracting solution.
The component of described nourishing cream and content are in Table 2:
The component of table 2 nourishing cream and content
| Composition | Percentage by weight (wt%) |
| Radix Rehmanniae extracting solution | Surplus |
| Cetearyl alcohol/cetearyl glucoside | 2.5 |
| Cetearyl alcohol | 1.2 |
| Glyceryl stearate/PEG-100 stearate | 1.2 |
| Encircle five polydimethylsiloxane/cyclohexasiloxane | 2 |
| Polydimethylsiloxane | 2 |
| Caprylic/capric triglyceride | 3 |
| Tocopherol (vitamin E) | 0.5 |
| Propylene glycol | 5 |
| Glycerol | 5 |
| Xanthan gum | 0.1 |
| Hyaluronate sodium | 0.02 |
| Polyacrylamide/C13-14 isoparaffin/laureth-7 | 0.7 |
| Phenoxyethanol/Sensiva SC50 | 0.5 |
| Oligofructose | 0.1 |
| Add up to | 100 |
Comparative example 1 health breast
The component of described health breast and content are in Table 3:
Component and the content of table 3 health breast
| Composition | Percentage by weight (wt%) |
| Deionized water | Surplus |
| Methyl glucose sesquistearate | 1.3 |
| PEG-20 methyl glucose sesquistearate | 0.9 |
| Isopropyl palmitate | 4 |
| Encircle five polydimethylsiloxane/cyclohexasiloxane | 5 |
| Glyceryl stearate/PEG-100 stearate | 0.7 |
| Cetearyl alcohol | 1.2 |
| Polydimethylsiloxane | 2 |
| Methyl hydroxybenzoate | 0.2 |
| Propyl hydroxybenzoate | 0.1 |
| Xanthan gum | 0.3 |
| Propylene glycol | 5 |
| Diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate | 0.2 |
| Add up to | 100 |
Comparative example 2 nourishing cream
The component of described nourishing cream and content are in Table 4:
The component of table 4 nourishing cream and content
| Composition | Percentage by weight (wt%) |
| Deionized water | Surplus |
| Cetearyl alcohol/cetearyl glucoside | 2.5 |
| Cetearyl alcohol | 1.2 |
| Glyceryl stearate/PEG-100 stearate | 1.2 |
| Encircle five polydimethylsiloxane/cyclohexasiloxane | 2 |
| Polydimethylsiloxane | 2 |
| Caprylic/capric triglyceride | 3 |
| Tocopherol (vitamin E) | 0.5 |
| Propylene glycol | 5 |
| Glycerol | 5 |
| Xanthan gum | 0.1 |
| Hyaluronate sodium | 0.02 |
| Polyacrylamide/C13-14 isoparaffin/laureth-7 | 0.7 |
| Phenoxyethanol/Sensiva SC50 | 0.5 |
| Oligofructose | 0.1 |
| Add up to | 100 |
Embodiment 3 effect evaluations
One, experiment purpose
By relative analysis, evaluate the reparation of prepared cosmetics in the various embodiments described above and protect sensitive-skinned effect.
Two, experimental technique
This experiment is divided into experimental group and matched group, and wherein, experiment component is: embodiment 1-health breast, embodiment 2-nourishing cream; Matched group is a certain commercially available nourishing cream of repairing and improving responsive skin that has of comparative example 1-health breast, comparative example 2-nourishing cream.
200 volunteers of collection sensitive skin tried out above-mentioned each product after 28 days, observed result.Wherein, women 120 people, male 80 people, maximum 30 years old age, minimal ages 15 years old, 22 years old mean age.
Described sensitive-skinned showing as: face redness, speckle, skin peeling, xerosis cutis, skin sore or skin oil and fat secretion.
Three, experimental result
The efficacy outcomes of table 5 experimental group and matched group
As known from Table 5: matched group product comparative example 1-health breast, comparative example 2-nourishing cream, a certain commercially available essence and experimental group product embodiments 1-health breast, embodiment 2-nourishing cream, red and swollen to face, speckle, skin peeling, xerosis cutis, skin sore or skin oil and fat secretion all have improvement in various degree, from experimental data, can find out, experimental group product is red and swollen to face, speckle, skin peeling, xerosis cutis, the improvement degree of skin sore or skin oil and fat secretion is obviously than the height of contrast set product, this shows, the cosmetics that contain Radix Rehmanniae extracting solution have significant reparation and protect sensitive-skinned effect.
The above embodiment has only expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but can not therefore be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (7)
1. a preparation method for Radix Rehmanniae extracting solution, is characterized in that, comprises the following steps:
By Radix Rehmanniae drying and crushing, with the 800-1000 order gauze bag of sterilizing, install, be placed in vacuum emulsifying pot, by the weight of Radix Rehmanniae, the deionized water that adds 8-12 doubly to measure, in 90-100 ℃ of extraction.
2. the Radix Rehmanniae extracting solution that preparation method as claimed in claim 1 makes.
3. Radix Rehmanniae extracting solution as prepared in claim 2 has the application in the cosmetics of repairing and protecting sensitive skin effect in preparation.
4. application according to claim 3, is characterized in that, in described cosmetics, the content of Radix Rehmanniae extracting solution is 58-95wt%.
5. the application of stating according to claim 3 or 4, is characterized in that, described cosmetics are health breast, nourishing cream.
6. a health breast, is characterized in that, described health breast comprises the component of following weight percentage ratio:
Emulsifying agent: 1.5-5wt%,
Co-emulsifier: 0.8-2wt%,
Emollient: 2-8wt%,
Skinfeel regulator: 1.5-10wt%,
Thickening agent: 0.1-0.4wt%,
Wetting agent: 4-10wt%,
Antiseptic: 0.05-0.7wt%,
Radix Rehmanniae extracting solution as claimed in claim 2: surplus;
Described emulsifying agent is at least one in methyl glucose sesquistearate, PEG-20 methyl glucose sesquistearate or glyceryl stearate/PEG-100 stearate;
Described co-emulsifier is at least one in cetearyl alcohol, glyceryl stearate or triethanolamine;
Described emollient is at least one in isopropyl palmitate, caprylic/capric triglyceride or hydrogenated jojoba oil;
Described skinfeel regulator is for encircling at least one in five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane or vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer;
Described thickening agent is at least one in xanthan gum, hydroxyethyl-cellulose or carbomer;
Described wetting agent is at least one in propylene glycol, glycerol or butanediol;
Described antiseptic is at least one in diazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate, propyl hydroxybenzoate or methyl hydroxybenzoate.
7. a nourishing cream, is characterized in that, described nourishing cream comprises the component of following weight percentage ratio:
Emulsifying agent: 3.5-6.3wt%,
Emollient: 5-10wt%,
Antioxidant: 0.2-0.8wt%,
Wetting agent: 5-15wt%,
Thickening agent: 0.05-0.15wt%,
Antiseptic: 0.3-0.7wt%,
Radix Rehmanniae extracting solution as claimed in claim 2: surplus;
Described emulsifying agent is at least one in cetearyl alcohol/cetearyl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearate, polyacrylamide/C13-14 isoparaffin/laureth-7 or methyl glucose sesquistearate;
Described emollient is for encircling at least one in five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane, caprylic/capric triglyceride or hydrogenated jojoba oil;
Described antioxidant is at least one that tocopherol or fan change in extract;
Described wetting agent is at least one in propylene glycol, glycerol, hyaluronate sodium, oligofructose or sorbitol;
Described thickening agent is at least one in xanthan gum or sodium carboxymethyl cellulose;
Described antiseptic is at least one in phenoxyethanol/Sensiva SC50, sodium benzoate or germall.
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Application publication date: 20140806 |