CN103976909B - A kind of Herba Leibnitziae extracting solution and its preparation method and application - Google Patents
A kind of Herba Leibnitziae extracting solution and its preparation method and application Download PDFInfo
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- CN103976909B CN103976909B CN201410236191.1A CN201410236191A CN103976909B CN 103976909 B CN103976909 B CN 103976909B CN 201410236191 A CN201410236191 A CN 201410236191A CN 103976909 B CN103976909 B CN 103976909B
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- extracting solution
- herba leibnitziae
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- herba
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- 238000002360 preparation method Methods 0.000 title abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
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- -1 alkyl androstanediol Chemical compound 0.000 claims description 17
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- 239000003755 preservative agent Substances 0.000 claims description 10
- 230000002335 preservative effect Effects 0.000 claims description 10
- 238000000605 extraction Methods 0.000 claims description 9
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 claims description 8
- 229940081733 cetearyl alcohol Drugs 0.000 claims description 7
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- Cosmetics (AREA)
Abstract
The invention discloses a kind of Herba Leibnitziae extracting solution and its preparation method and application. The Herba Leibnitziae extracting solution that the present invention obtains through refining through water, its have suppression and scavenger cell metabolic process in produce a series of reactive oxygen species, thus preventing the oxidative damage of free radical mediated and the effect of stabilizing cell membrane, this characteristic makes the effect that Herba Leibnitziae extracting solution possesses antioxidation, maintains the stable hydration of horn cell, prevents Moisture factor from losing, thus delay skin aging, it is applied in cosmetics to have effect of significant moisturizing, defying age.
Description
Technical field
The present invention relates to cosmetic field, particularly relate to a kind of Herba Leibnitziae extracting solution and its preparation method and application.
Background technology
Along with the raising of people's living standard, cosmetics have become as necessary article in people's life. But people are but very high for the prescription of cosmetics, not only require effective, and require to be free from side effects. Along with the development of cosmetics industry, natural plants series products due to use safety, action temperature and, the advantage such as effect is obvious and obtain the parent of consumers in general and look at. Obtain the plant extract containing effective ingredient generally by corresponding processing, and add in cosmetics.
Plant extract in current cosmetics, mostly adopts water to carry, alcohol extraction, ultrasonic extraction, the method such as microwave extraction extract gained, and extraction process is complicated, through operations such as concentrate dryings, also to add preservative so that the shelf-life of extract is more permanent. The drawback so brought, one is waste resource, and in extraction process, solution concentrates, and generally only takes concentration fraction elite out, and most solutions then discards. This part solution is possibly together with other effective ingredient in fact, it is possible to again with, and directly discard the waste having resulted in resource.Another drawback is, adds preservative and extract no doubt can be made to obtain the longer shelf-life, but also bring sensitization source for skin simultaneously in extract.
Aging is a kind of natural law of mankind's normal activities, and skin also synchronizes aging with human body as one of the organ of human body. a series of problems at heart such as aging makes people cause anxiety, depression, feel oneself inferior. factor about skin aging is complicated, wherein representative free radical causes of senescence thinks that the reason of skin aging is: the endogenous oxygen-derived free radicals that too much exogenous free radical and internal metabolism produce causes normal cell membrane structure to be destroyed, important component in damaging cells, fibroblast and horn cell come to harm, in fibroblast, collagen protein constantly runs off, horn cell hydration disequilibrium, cell moisture evaporates in a large number, the moisture lost because of skin and nutrient substance cannot be supplemented timely, cause xerosis cutis, lose flexibility, flexibility decrease, so that there is wrinkle in skin, dry keratinization, tarnish and melanin, a series of senile symptoms such as lipofuscin excess deposition.
Therefore, select which kind of plant, how simply, safely, effectively to this plant to extract, and by the aging being applied in cosmetics delaying skin of its safety, be problem demanding prompt solution.
Summary of the invention
Based on this, present invention aim at providing a kind of Herba Leibnitziae extracting solution and its preparation method and application.
The concrete technical scheme solving above-mentioned technical problem is as follows:
The preparation method of a kind of Herba Leibnitziae extracting solution, comprises the following steps:
By Herba Leibnitziae Herb drying and crushing, install with the 800-1000 order gauze bag of sterilizing, be placed in vacuum emulsifying pot, by the weight of Herba Leibnitziae, add the deionized water of 8-12 times amount, in 90-100 DEG C of extraction, can be prepared by Herba Leibnitziae extracting solution.
Wherein in some embodiments, the time of described extraction is 20-50min.
Wherein in some embodiments, by Herba Leibnitziae Herb drying and crushing, installing with the 800-1000 order gauze bag of sterilizing, be placed in vacuum emulsifying pot, after having extracted, directly taken out by gauze bag, remaining solution is Herba Leibnitziae extracting solution. Owing to adopting vacuum emulsifying pot in the method, other cosmetic after extraction completes, directly can be added by it, carries out Cosmetic Manufacture, extracts without with special herbal extraction equipment, has saved cost; It addition, adopt the packed Herba Leibnitziae powder of gauze, directly gauze bag is taken out after having extracted, need not filter, simplify extraction process, improve efficiency.
Said method is simple to operation, and Herba Leibnitziae extract can now be withdrawn deposit use, does not need to add preservative, substantially reduces the sensitization source to skin. In cosmetic formulations, inherently it is added with preservative, extract of the present invention is now carried and adds, it is to avoid produce spoilage problems because of placement.
Herba Leibnitziae extracting solution obtained by said method has the application in the cosmetics of moisturizing, senile-resistant efficacy in preparation.
Wherein in some embodiments, in described cosmetics, the content of Herba Leibnitziae extracting solution is 58-95wt%.
Wherein in some embodiments, described cosmetics are nourishing cream.
The present invention provides a kind of nourishing cream, and described nourishing cream includes the component of following weight percentage ratio:
Emulsifying agent: 4.0-8.2wt%,
Emollient: 8-18wt%,
Transdermal enhancer: 0.5-2.5wt%,
Antioxidant: 0.2-0.9wt%,
Wetting agent: 12.0-20.1wt%,
Thickening agent: 0.2-0.6wt%,
Whitening agent: 1.0-2.5wt%,
Antiinflammatory, anti-sensitizer: 0.1-0.25wt%,
Preservative: 0.4-1.0wt%,
Herba Leibnitziae extracting solution as claimed in claim 2: surplus;
Described emulsifying agent is at least one in cetearyl alcohol/cetearyl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearate, C14-22 alcohol/C12-20 alkyl androstanediol or olive oil PEG7 esters;
Described emollient is at least one in ring five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane, caprylic/capric triglyceride or squalane, isopropyl myristate;
Described transdermal enhancer is at least one in tetrahydrochysene piperine, Diethylhexyl Butamido Triazon;
Described antioxidant is at least one in tocopherol or butylated hydroxytoluene;
Described wetting agent is at least one in propylene glycol, glycerol, hyaluronate sodium, reed fragrant plant glue or sorbitol;
Described thickening agent is at least one in xanthan gum, carbomer, polyacrylamide/C13-14 isoparaffin/laureth-7 or match Bick 305;
Described whitening agent is at least one in arbutin, ethylascorbyl, licoflavone;
Described antiinflammatory, anti-sensitizer are at least one of bisabolol, glycyrrhizic acid dipotassium, Lu Dingzhong;
Described preservative is at least one in phenoxyethanol/Sensiva SC50,1,2-hexanediol/caprylyl glycol, sodium benzoate, propylene glycol/Bis(hydroxymethyl)imidazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate or Kazon.
Wherein in some embodiments, described nourishing cream includes the component of following weight percentage ratio:
Emulsifying agent: 4.9-7.6wt%,
Emollient: 8.5-17.5wt%,
Transdermal enhancer: 0.5-2.0wt%,
Antioxidant: 0.2-0.8wt%,
Wetting agent: 12.0-20.1wt%,
Thickening agent: 0.2-0.5wt%,
Whitening agent: 1.2-2.5wt%,
Antiinflammatory, anti-sensitizer: 0.2-0.25wt%,
Preservative: 0.5-1.0wt%,
The Herba Leibnitziae extracting solution that above-mentioned preparation method prepares: surplus,
Described emulsifying agent is at least one in cetearyl alcohol/cetearyl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearate, C14-22 alcohol/C12-20 alkyl androstanediol or olive oil PEG7 esters;
Described emollient is at least one of polydimethylsiloxane, caprylic/capric triglyceride, squalane or isopropyl myristate;
Described transdermal enhancer is Diethylhexyl Butamido Triazon;
Described antioxidant is tocopherol;
Described wetting agent is at least one in propylene glycol, glycerol, hyaluronate sodium or sorbitol;
Described thickening agent is at least one in xanthan gum, polyacrylamide/C13-14 isoparaffin/laureth-7;
Described whitening agent is ethylascorbyl;
Described antiinflammatory, anti-sensitizer are bisabolol;
Described preservative is at least one in 1,2-hexanediol/caprylyl glycol, sodium benzoate, propylene glycol/Bis(hydroxymethyl)imidazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate.
Wherein in some embodiments, described nourishing cream includes the component of following weight percentage ratio:
C14-22 alcohol/C12-20 alkyl androstanediol: 1.5-2.5wt%,
Cetearyl alcohol: 1.7-2.5wt%,
Glyceryl stearate/PEG-100 stearate: 1.7-2.5wt%,
Polydimethylsiloxane: 2.1-3.1wt%,
Caprylic/capric triglyceride: 2.1-5.1wt%,
Isopropyl myristate: 3.1-6.0wt%,
Diethylhexyl Butamido Triazon: 0.5-2.0wt%,
Squalane: 1.5-3.0wt%,
Tocopherol: 0.2-0.8wt%,
Propylene glycol: 6-10wt%,
Glycerol: 6-10wt%,
Xanthan gum: 0.1-0.25wt%,
Hyaluronate sodium: 0.01-0.06wt%,
Polyacrylamide/C13-14 isoparaffin/laureth-7:0.1-0.25wt%,
Ethylascorbyl: 1.2-2.5wt%,
Bisabolol: 0.2-0.25wt%,
Propylene glycol/Bis(hydroxymethyl)imidazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate: 0.2-0.5wt%,
1,2-hexanediol/caprylyl glycol: 0.3-0.5wt%,
Above-mentioned Herba Leibnitziae extracting solution: surplus.
A kind of Herba Leibnitziae extracting solution of the present invention and its preparation method and application has the following advantages and beneficial effect:
The present invention is through the substantial amounts of experiment of inventor and research, draw and put obtained Herba Leibnitziae extracting solution at optimum process water, its tool suppresses and produces a series of reactive oxygen species in scavenger cell metabolic process, thus preventing the oxidative damage of free radical mediated and the effect of stabilizing cell membrane, this characteristic makes the effect that Herba Leibnitziae extracting solution possesses antioxidation, maintains the stable hydration of horn cell, prevents Moisture factor from losing, thus delay skin aging, it is applied in cosmetics to have effect of significant moisturizing, defying age.
Detailed description of the invention
Herba Leibnitziae of the present invention is Compositae Gerbera plant Herba Leibnitziae, with all herbal medicine. Being born in hillside, cheuch, roadside and sylvan life thick grass, all there is distribution each provinces and regions, China north and south. Herba Leibnitziae bitter in the mouth is cold in nature, has clearing away heat-damp and promoting diuresis, removing toxic substances and promoting subsidence of swelling, cough-relieving, anastalsis. " Guizhou folk medicine ": " dispelling the wind and dampness pathogens is numb. " " Guizhou medical herbs ": " evil-wind expelling and dampness removing, cough-relieving is breathed heavily, removing toxic substances. " Herba Leibnitziae obtained through refining to obtain Herba Leibnitziae extracting solution through water by the present invention, use it in the cosmetics that preparation has moisturizing, senile-resistant efficacy.
Below with reference to specific embodiment, the present invention will be further described.
In following embodiment, described raw material is commercially available prod.
Components Name used in following example is international cosmetic raw material name (InternationalNomenclatureCosmeticIngredient, INCI) title of defined, such as C14-22 alcohol/C12-20 alkyl androstanediol, glyceryl stearate/PEG-100 stearate, caprylic/capric triglyceride, polyacrylamide/C13-14 isoparaffin/laureth-7,1,2-hexanediol/caprylyl glycol.
Embodiment 1 nourishing cream
Containing Herba Leibnitziae extracting solution in nourishing cream described in the present embodiment, the preparation method of described Herba Leibnitziae extracting solution, comprises the following steps: is cleaned by 1 kilogram of Herba Leibnitziae, dries, drying and crushing is to 100 orders, install with 1000 order gauze bags of sterilizing, be placed in vacuum emulsifying pot, add the deionized water of 12 kilograms, in 100 DEG C of lixiviate 50min, gauze bag is taken out, remaining solution, obtain Herba Leibnitziae extracting solution.
The component of described nourishing cream and content are in Table 1:
The component of table 1 nourishing cream and content
Comparative example 1 nourishing cream
The component of described nourishing cream and content are in Table 2:
The component of table 2 nourishing cream and content
Embodiment 2 efficacy assessments
One, experiment purpose
Effect by the moisturizing of cosmetics obtained in relative analysis evaluation the various embodiments described above, defying age.
Two, experimental technique
This experiment is divided into experimental group and matched group, and wherein, experimental group is: embodiment 1-nourishing cream; Matched group is comparative example 1-nourishing cream, a certain commercially available nourishing cream with moisturizing, senile-resistant efficacy.
Collect 200 volunteers and try out above-mentioned each product 28 days, after trier uses identical gentle cleaning agent to clean face, about trier face, selected same area is as trial zone, and embodiment product is smeared in left side, the corresponding comparative example product of equivalent, observed result are smeared in right side. Wherein, women 160 people, male 40 people, max age 52 years old, minimal ages 27 years old, 41 years old mean age.
The main manifestations of described ageing skin is: cutis laxa, wrinkle, pigmentation, dry keratinization occur, coarse or skin is matt.
Three, experimental result
Result is referring to table 3.
The efficacy outcomes table of table 3 experimental group and matched group
As known from Table 3: matched group product and comparative example 1-nourishing cream, a certain commercially available nourishing cream and experimental group product embodiments 1-nourishing cream are to cutis laxa, wrinkle occurs, pigmentation, dry keratinization, coarse or skin shine all has improvement in various degree, can be seen that from experimental data, in experimental group, product is to cutis laxa, wrinkle occurs, pigmentation, dry keratinization, coarse or skin shine improvement degree is substantially high than the improvement degree of product in matched group, it can thus be appreciated that, cosmetics containing Herba Leibnitziae extracting solution have significant moisturizing, effect of defying age.
Embodiment described above only have expressed the several embodiments of the present invention, and it describes comparatively concrete and detailed, but therefore can not be interpreted as the restriction to the scope of the claims of the present invention. It should be pointed out that, for the person of ordinary skill of the art, without departing from the inventive concept of the premise, it is also possible to making some deformation and improvement, these broadly fall into protection scope of the present invention. Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (1)
1. a nourishing cream, it is characterized in that, described nourishing cream includes the component of following weight percentage ratio: emulsifying agent: 4.0-8.2wt%, emollient: 8-18wt%, transdermal enhancer: 0.5-2.5wt%, antioxidant: 0.2-0.9wt%, wetting agent: 12.0-20.1wt%, thickening agent: 0.2-0.6wt%, whitening agent: 1.0-2.5wt%, antiinflammatory, anti-sensitizer: 0.1-0.25wt%, preservative: 0.4-1.0wt%, Herba Leibnitziae extracting solution: surplus; Described emulsifying agent is at least one in cetearyl alcohol/cetearyl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearate, C14-22 alcohol/C12-20 alkyl androstanediol or olive oil PEG7 esters; Described emollient is at least one in ring five polydimethylsiloxane/cyclohexasiloxane, polydimethylsiloxane, caprylic/capric triglyceride or squalane, isopropyl myristate; Described transdermal enhancer is at least one in tetrahydrochysene piperine, Diethylhexyl Butamido Triazon; Described antioxidant is at least one in tocopherol or butylated hydroxytoluene; Described wetting agent is at least one in propylene glycol, glycerol, hyaluronate sodium, reed fragrant plant glue or sorbitol; Described thickening agent is at least one in xanthan gum, carbomer, polyacrylamide/C13-14 isoparaffin/laureth-7 or match Bick 305; Described whitening agent is at least one in arbutin, ethylascorbyl, licoflavone; Described antiinflammatory, anti-sensitizer are at least one in bisabolol, glycyrrhizic acid dipotassium, rutin; Described preservative is at least one in phenoxyethanol/Sensiva SC50,1,2-hexanediol/caprylyl glycol, sodium benzoate or propylene glycol/Bis(hydroxymethyl)imidazolidinyl urea/iodine propilolic alcohol butyl mephenesin Carbamate;
Described Herba Leibnitziae extracting solution adopts following methods to prepare: be dry, pulverize by Herba Leibnitziae Herb, loads the 800-1000 order gauze bag of sterilizing, it is placed in vacuum emulsifying pot, by the weight of Herba Leibnitziae, adds the deionized water of 8-12 times amount, in 90-100 DEG C of extraction.
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